Analytical Reference Materials Ethylene Oxide Standard Catalog # 36005 Lot # A083677 110 Benner Circle Bellefonte, PA 16823-8812 (814) 353-1300 FOR LABORATORY USE ONLY. READ MSDS PRIOR TO USE. RAW MATERIAL TEST INFORMATION AVAILABLE UPON REQUEST MANUFACTURED UNDER RESTEK'S ISO 9001 REGISTERED QUALITY SYSTEM By dshaffer at 5:32 pm, Sep 27, 2011 Page 1 of 5 110 Benner Circle Bellefonte, PA 16823-8812 Tel: (800)356-1688 Fax: (814)353-1309 Certificate of Analysis www.Restek.com FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE. Catalog No. : 36005 Lot No.: A083677 Description : Ethylene Oxide Standard Solvents, USP Methodethylene oxide, 500µg/ml, DMSO, 1ml/ampule Container Size : 5 Expiration Date : Elution Order 1 Solvent: Pkg Amt: 5 2 mL September 2018 Compound Ethylene oxide DMSO Storage: CAS # > 1 mL 10°C or colder Percent Purity 75-21-8 99% 67-68-5 99% 2 Grav. Conc. (weight/volume) 500.0 ug/mL 3 Grav.Uncert. (95% C.L.; K=2) 4 +/- 6.4654 ug/mL Column: 60m x .53mm x 3.0um Rtx-1301 (cat.# 16088) Carrier Gas: helium-constant pressure 7 psi Temp. Program: 55°C (6') to 185°C @ 20°C/min. to 240°C @ 30°C/min.(5') Inj. Temp: 210°C Det. Temp: 250°C Det. Type: FID Page 2 of 5 Date Passed: 27-Sep-2011 Balance: 1127510105 Manufactured under Restek's ISO 9001:2008 Registered Quality System Certificate #FM 80397 1 Expiration date of the unopened ampule stored at the recommended storage condition is the last day of the month listed. 2A Purity and chemical identity are determined by one or more of the following techniques: GC/FID, HPLC, GC/ECD, GC/MS. Purity value is rounded to the nearest whole number. See data pack or contact Restek for further details. 2B Compounds with a listed purity of less than 99% have been weight corrected to compensate for impurities. 2C The following types of compounds will have a listed purity of less than 99%: Aldehyde/Ketone-DNPH compounds, Bromides, Chlorides, HCL salts, HBR salts, sulfates, hydrates, and other compounds as necessary. The listed purity is a correction factor that is equivalent to the percentage of parent compound in the molecule. This correction factor is used to calculate the amount of compound necessary to achieve the desired concentration of the parent compound in solution. The concentration listed on the certificate is the concentration of the parent compound in the solution. 2D Purity of isomeric compounds is reported as the sum of the isomers. Value is rounded to the nearest whole number after summation. 3 Based upon gravimetric preparation with balance calibration verified using NIST traceable weights (seven mass levels) and/or class A glassware used for dilutions. 4 Uncertainties determined using data for balances and glassware from measurement systems analysis methodology, raw material purity, and, when significant, equipment tolerances or calibration results. 5A Containers are overfilled to ensure the packaged amount, as a minimum. 5B Restek supplies deactivated vials along with most standards packed in 2 mL ampules, for the handling and storage of standards. Due to space constraints, Restek does not supply vials for larger volume ampules. Samples should be transferred into deactivated vials for handling and storage. Restek sells DMDCS for the purpose of glassware deactivation as catalog number 31840, which includes complete instructions. Restek will also deactivate larger volume vials from our inventory, as a custom ordered item. Contact your Restek sales or customer service representative for details. Page 3 of 5 Chemical Standard Batch Sheet Lot #: A083677 Catalog #: 36005 Description: Ethylene Oxide Standard Solvent: DMSO Made by: Michael Maye Tested by: Diane Shaffer Pass Packaged by: Joe Conway / Joe Conway Balance Used: ARMBALPC3 XP205 Compound Ethylene oxide Target: 500 ug/mL Solvent Lot: DA077 Date: Date: By: Date: Serial #: CAS 75-21-8 Final Volume: 8/26/2011 7:48:14AM 8/26/2011 3:26:36PM John Lidgett 8/26/2011 11:02:16AM 1127510105 500 ml Date: 9/27/2011 1:57:35PM No. Units: 316 Pkg Size: Storage Location Lot # Purity VOALAB MKBF0692 0.99 Target Conc(ug/mL) 500.00 1 mL Target Actual Calc Conc(ug/mL) 250.00 mg 250.00 mg 500.0 Page 4 of 5 Ethylene Oxide Standard Runs of Lot # A081427 COMPONENT Run #1 Run #2 Run #3 Ethylene oxide 274143 9/27/2011 1:54:53 PM 268458 270511 AVG 271037 STD DEV % RSD 2879 1.06 Runs of Lot # A083677 Run #1 Run #2 Run #3 287832 283576 289513 AVG 286974 STD DEV % RSD 3060 1.07 %D MEAN -5.88 P/F PASS Page 5 of 5 1/1 - 1