Catalog # 36005 Lot # A083677 Ethylene Oxide Standard

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Analytical Reference Materials
Ethylene Oxide Standard
Catalog # 36005
Lot # A083677
110 Benner Circle Bellefonte, PA 16823-8812
(814) 353-1300
FOR LABORATORY USE ONLY. READ MSDS PRIOR TO USE.
RAW MATERIAL TEST INFORMATION AVAILABLE UPON REQUEST
MANUFACTURED UNDER RESTEK'S ISO 9001 REGISTERED QUALITY SYSTEM
By dshaffer at 5:32 pm, Sep 27, 2011
Page 1 of 5
110 Benner Circle
Bellefonte, PA 16823-8812
Tel: (800)356-1688
Fax: (814)353-1309
Certificate of Analysis
www.Restek.com
FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE.
Catalog No. :
36005
Lot No.: A083677
Description :
Ethylene Oxide Standard
Solvents, USP Methodethylene oxide, 500µg/ml, DMSO, 1ml/ampule
Container Size :
5
Expiration Date :
Elution Order
1
Solvent:
Pkg Amt: 5
2 mL
September 2018
Compound
Ethylene oxide
DMSO
Storage:
CAS #
> 1 mL
10°C or colder
Percent
Purity
75-21-8
99%
67-68-5
99%
2
Grav. Conc.
(weight/volume)
500.0 ug/mL
3
Grav.Uncert.
(95% C.L.; K=2)
4
+/- 6.4654 ug/mL
Column:
60m x .53mm x 3.0um
Rtx-1301 (cat.# 16088)
Carrier Gas:
helium-constant pressure 7 psi
Temp. Program:
55°C (6') to 185°C @ 20°C/min.
to 240°C @ 30°C/min.(5')
Inj. Temp:
210°C
Det. Temp:
250°C
Det. Type:
FID
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Date Passed:
27-Sep-2011
Balance:
1127510105
Manufactured under Restek's ISO 9001:2008
Registered Quality System
Certificate #FM 80397
1 Expiration date of the unopened ampule stored at the recommended storage condition is the last day of the month listed.
2A Purity and chemical identity are determined by one or more of the following techniques: GC/FID, HPLC, GC/ECD, GC/MS. Purity value is
rounded to the nearest whole number. See data pack or contact Restek for further details.
2B Compounds with a listed purity of less than 99% have been weight corrected to compensate for impurities.
2C The following types of compounds will have a listed purity of less than 99%: Aldehyde/Ketone-DNPH compounds, Bromides, Chlorides,
HCL salts, HBR salts, sulfates, hydrates, and other compounds as necessary. The listed purity is a correction factor that is equivalent
to the percentage of parent compound in the molecule. This correction factor is used to calculate the amount of compound necessary
to achieve the desired concentration of the parent compound in solution. The concentration listed on the certificate is the concentration
of the parent compound in the solution.
2D Purity of isomeric compounds is reported as the sum of the isomers. Value is rounded to the nearest whole number after summation.
3
Based upon gravimetric preparation with balance calibration verified using NIST traceable weights (seven mass levels) and/or class A
glassware used for dilutions.
4 Uncertainties determined using data for balances and glassware from measurement systems analysis methodology, raw material purity,
and, when significant, equipment tolerances or calibration results.
5A Containers are overfilled to ensure the packaged amount, as a minimum.
5B Restek supplies deactivated vials along with most standards packed in 2 mL ampules, for the handling and storage of standards. Due to space
constraints, Restek does not supply vials for larger volume ampules. Samples should be transferred into deactivated vials for handling and
storage. Restek sells DMDCS for the purpose of glassware deactivation as catalog number 31840, which includes complete instructions. Restek
will also deactivate larger volume vials from our inventory, as a custom ordered item. Contact your Restek sales or customer service
representative for details.
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Chemical Standard Batch Sheet
Lot #: A083677
Catalog #: 36005
Description: Ethylene Oxide Standard
Solvent: DMSO
Made by: Michael Maye
Tested by: Diane Shaffer
Pass
Packaged by: Joe Conway / Joe Conway
Balance Used: ARMBALPC3 XP205
Compound
Ethylene oxide
Target: 500 ug/mL
Solvent Lot: DA077
Date:
Date:
By:
Date:
Serial #:
CAS
75-21-8
Final Volume:
8/26/2011 7:48:14AM
8/26/2011 3:26:36PM
John Lidgett
8/26/2011 11:02:16AM
1127510105
500 ml
Date: 9/27/2011 1:57:35PM
No. Units: 316
Pkg Size:
Storage
Location
Lot #
Purity
VOALAB
MKBF0692
0.99
Target
Conc(ug/mL)
500.00
1 mL
Target
Actual
Calc
Conc(ug/mL)
250.00 mg
250.00 mg
500.0
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Ethylene Oxide Standard
Runs of Lot # A081427
COMPONENT Run #1 Run #2 Run #3
Ethylene oxide
274143
9/27/2011 1:54:53 PM
268458
270511
AVG
271037
STD DEV % RSD
2879
1.06
Runs of Lot # A083677
Run #1 Run #2 Run #3
287832
283576
289513
AVG
286974
STD DEV % RSD
3060
1.07
%D MEAN
-5.88
P/F
PASS
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