T. Sawaguchi et al. / Scripta Materialia 99 (2015) 49–52 Designing Fe–Mn–Si alloys with improved low-cycle fatigue lives Takahiro Sawaguchi, Ilya Nikulin, Kazuyuki Ogawa, Kaoru Sekido, Susumu Takamori, Tadakatsu Maruyama, Yuya Chiba, Atsumichi Kushibe, Yasuhiko Inoue and Kaneaki Tsuzaki Paper6Survey Advisor : 戴子堯 Reporter : 李懋靖 Department of Mechanical Engineering & Institute of Nanotechnology, Southern Taiwan University of Science and Technology, Tainan, TAIWAN Date ﹕2015/12/29 1 Outline Introduction Design Experiment Conclusion Introduction Recently, Sawaguchi et al. proposed that Fe–Mn–Si based alloys can be used for the seismic damping of architectural constructions. Seismic metallic dampers absorb the vibrations of buildings through elastoplastic deformation;however, severe deformations cause fatigue in the damper metal. An Fe–Mn–Si-based alloy with the chemical composition of Fe–28Mn–5Cr–6Si– 0.5NbC (in wt.%) was reported to exhibit a stable damping capacity associated with reversible martensitic transformations under cyclic push–pull loading. 3 Introduction This stable deformation behaviour with enhanced fatigue properties makes such alloys highly suited for use in seismic dampers, in particular against longduration ground motion. For this purpose, we attempted to develop new Fe–Mn–Si-based alloys with enhanced low-cycle fatigue (LCF) lives,N𝑓 . 4 Design The central idea behind the design concept is the reversibility of the plasticity mechanisms characteristic of low-SFE alloys. Figure 1 illustrates schematic models of the reversible dislocation motions associated with (a, b) a deformationinduced 𝛾 − 𝜀 martensitic transformation, (c,d) deformation 𝛾-twinning and (e, f) extended dislocation gliding. 5 Design Figure 1. Schematic diagrams of the reversible group motion of the dislocations in (a, c, e) tension and (b, d, f) compression. (a, b) Deformation-induced 𝜀-martensitic transformation, (c, d) mechanical 𝛾-twinning, (e, f) extended dislocation gliding. The dashed and solid lines represent {111} planes of the 𝛾-crystal and stacking faults, respectively. 6 Experiment Table 1. Chemical compositions, the number of cycles to fatigue fracture, 𝑁f , the stress amplitude and the hysteresis energy at 𝑁f /2, ∆𝜎/2Nf/2 and ∆𝑊Nf/2 , respectively. 7 Experiment Figure 2. The composition dependence of LCF and its thermodynamic properties. (a–d) 𝑁f , (measured), (e–h) SFE (calculated) and (i–l) volume fractions (measured) of the 𝜀- and 𝛼(𝛼’)-phases before deformation (f(𝜀)INT and f(𝛼)INT) and after fatigue fracture (f(𝜀)FF and f(𝛼)FF). 8 Experiment Figure 3. Post-fatigue-fracture microstructures of the Fe–Mn–Cr–Ni–Si alloys. EBSD phase maps (step size: 0.4 𝜇m) and TEM images for (a,d) s = 0, (b, e) s = 4 and (c, f) s = 6. The areas in white and grey in the EBSD images are the 𝛾- and 𝜀-phases, respectively, and blue lines represent low-angle boundaries (misorientation ranging from 2 to 15). Cubes and hexagons in the figures represent the orientations of the 𝛾- and 𝜀-phases. 9 Conclusion In conclusion, we propose two design criteria for improving the LCF lives of Fe–Mn–Si-based alloys: first,a thermodynamic balance between 𝛾- and 𝜀-phases is essential to promote the reversible movement of Shockley partials;and secondly, a moderate planarity of dislocation motion aided by solute atoms is needed for further improvement. 10 Thanks for your attention !! 11