and Ore-testing Bureau capabilities attheNewMexico of Mines Mineral Resources NM87801 byMichael Harrs,NewMexico Bureau Resources, Socono, of Mines andMineral Introduction Many people are familiar with the New Mexico Bureau of Mines and Mineral Resourcesthrough its excellentpublications, its large collection of specimensin the mineral museum, and the annual mineral symposium. However, many of these same people do not know that the Bureau offers many other servicesto the public, including thos-e of a well-equipped metallurgy lab. The metallurgy staff is prepared to work with anyone needingtest work done on an ore. Some of the work might qualify to be done at no cost, and charges for most of the extended tests are very reasonable. The metallurgy lab offers a wide range of capabilities,including samplepreparationand ore-leaching, gravity-concentration, flotation-concentration,and firel-assay tests.When these capabilities are combined with others offered by the Bureau, such as X-ray fluorescence or wet analytical chemistry, they provide a wide spectrum of possible tests that can be performed on ore samples. Metallurgy laboratory The metallurgy lab has a well-equipped room for preparing coarse ore samples for analysis. With this equipment it is possible to prepare an ore sample to any specifiedsize down to 200mesh. Equipment includes three jaw crushers (the largest one capableof handling rock piecesup to 5 inches),a roll crusher, a rotary-disk pulverizer, and a fine-pulverizing machine. For sizing crushed or ground materials, the lab has a Gilson Testing Machine with a complete set of screensranging from 2 inches to 200 mesh. For sizing small amounts of material, the lab also has a new Rotap machine with a full set of Tyler sieves ranging from L inch to 400mesh. In addition, the lab has a Holtain air elutriator for determining the size dishibution of particles finer than 200 mesh. The met lab is well equipped to handle batch-flotation testing. The Iab has a new Denver D-12 flotation machine with a full range of flotation cells to handle samples weighihg from a few grams to two kilograms. The lab also has a Wemco flotation machine and an attrition scrubber. The lab is stocked with a wide range of flotation reagents, and specificreagentscan be ordered with advanced notice. The metallurgy lab has a two-liter Parr autoclave to carry out leaching testsunder very aggressiveconditions. Tests can be conducted at temperaturesexceeding200"Cand at pressuresof more than 500psi. Many refractory ores, which are not amenable to leaching at ambient conditions, will respond to leaching at higher temperaturesand pressures. For gravity-concentration testing the lab- oratory has a small 3' x 5' single-deckDeis- obtained by splitting a larger sample. Ore ter shaking table. Although it is recognized samples required for other tests are: Minimum ore-sample that this device may not yield the optimum requirement Typeof test results for gravity concentration, it does proFlotation 5-10pounds vide an indication of whether the ore can be Bench-scale leaching 5-10pounds treated by gravity techniques. The lab has 20-50pounds Gravityconcentration two different decks for the table, the regular leaching Large-column 200pounds deck and a Slimedeck, so that particles from be L0 mesh down to about 200 mesh can Examples of ore-testing projects tested. The projects described below are illustraThe lab also has a Bond mill for performing tive of the capability of the metallurgy lab. Bond grindability tests.The Bond test is the -Bond grindabilitytestingof a low-gradegold test standard used on a laboratory-sized ore. This test was carried out to determine sample to determine the amount of energy what the grinding costs would be for a 500required to grind the material to a given size. mine and mill. Answers are given in kilowatt hours of elec- torVday -Fluorite flotation studies.A series of flotricity per ton of ore ground. tation tests were carried out to examine the potential of a low-grade fluorite deposit to Standard ore-testing services produce commercial-grade products. This Without a doubt the most popular service work was done for a division of one of the offered by the Bureau's metallurgy lab is fire nation's largestmining companies. assayingpotential ore samples to determine --{.olumn-Ieaching testson low-grade goldore. their gold and silver content.Becauseof the These tests were carried out for a gold mine current high degree of interest in gold ores, to investigate the effectsof severalvariables the metallurgy lab conducts fire assaysnearly on the cyanide extraction of gold. The colevery week. Recently the lab upgraded its umns were 10 feet tall and had 6-inch dicapabilities by adding a new gas-fired furameters. Each contained approximately 250 naceto the assayingequipment. This furnace pounds of ore. replacesan electric furnace that had been in -N umerousgraoity-concentration studieson servicefor manv vears. golil ores. Another popirtir service offered through the metallurgy lab is testing samplesof gold Perlite-testing facility ores to determine if they are amenable to In conjunction with the met lab the Bureau treatment by gravity concentration or leach- operatesa perlite-testing facility. The facility ing. Typically this is done by cyanide leach- includes a vertical expanding furnace and ing. Testscan be conducted in almost any specialized equipment to perform a variety desired fashion from the standard "rolling of tests on the expanded perlite fractions. bottle" test, or beaker tests, to column tests Testsinclude: expanded density, brightness, used to simulate heap{eaching conditions. percent sinkers, silicacontent (by X-ray), and Leach testing can be extended to many other size-distribution determination. Recently,the applications,including leachinggold oreswith perlite facility began testing perlite sarirples solutionsother than cyanide(i.e., thiourea), as filter aids. leaching copper ores for copper recovert Analytical chemistry capabilities leaching uranium ores, etc. In addition to determining the amount of gold and silver The Bureau also has a well-equipped anthat can be extracted by leaching, tests can alytical chemistry laboratory for determining also be conducted to recover the dissolved the composition of geologic samplesas well values from solution. Recoverytests include as doing water-quality studies. The capabilcarbon adsorption, electrolytic recovery, or ities of the analytical laboratory include AA precipitation on zinc. Chargesfor thesetypes (atomic absorption spectroscopy) and ICP of tests are based on the individual project (inductively coupled plasma spectroscopy). and may vary depending on the amount of The analytical lab is also capableof performwork performed. ing the more traditional, wet chemistry determinations. Sample-size requirements Conclusion Sample-size requirements are highly dependent on the type of material being tested The New Mexico Bureau of Mines and and the testwork to be done. Fire assayscan Mineral Resourcesoffers a variety of services be performed using only a few grams of mato the public. Included in these servicesis a terial, although it would be hard to insure well-equipped metallurgy laboratory that is that such a small sample is representativeof capableof carryrng out test work on different a deposit. Typically, fire assaysare carried ores. The most requestedtest work consists out using either 29.17 grams (assayton) or of fire assaying samples to determine gold L4.5grams (half assayton) of samplethat is tr and silver content. NartMexicoGeolo3yAugust1988