Developmental Regulation of DNA Replication in Drosophila melanogaster By Eugenia Agnes Park B.S., Biochemistry Washington State University Pullman, WA, 1998 Submitted to the Department of Biology in Partial Fulfillment of the Requirements for the Degree of Doctor of Philosophy in Biology At the AMASSACHUSET-S INwTyIE Massachusetts Institute of Technology OF TECHNOLOGY Cambridge, MA SEP 13 2006 S gust 2006 LIBRARIES U © 2006 Eugenia Agnes Park. All rights reserved. The author hereby grants to MIT permission to reproduce and to distribute Publicly paper and electronic copies of this thesis document in whole or in part. Signature of A uthor................. ...... ..... . ... ARCHNES ............... ......................................... Department of Biology August 17, 2006 Certified by. .. .. •..y ............. ............................................................................................ Terry L. Orr-Weaver Professor of Biology Thesis Supervisor A ccepted by ............. ... .... .............. ............... ......................................... ............ T 0 Stephen Bell Chair, Committee on Graduate Students Department of Biology Developmental Regulation of DNA Replication in Drosophila melanogaster By Eugenia Agnes Park Submitted to the Department of Biology in Partial Fulfillment of the Requirements for the Degree of Doctor of Philosophy in Biology ABSTRACT In mitotic cell cycles, the genome must be replicated fully in each cell cycle to ensure the normal complement of chromosomes. Failure to replicate chromosomes fully or a failure to limit replication to once-per-cell-cycle may lead to aneuploidy and genomic instability. Variants of the archetypal mitotic cell cycle, utilizing conserved cell cycle machinery, are employed during metazoan development to achieve different aims. Endocycles, in which the cell cycle proceeds without complete mitosis, generate polyploidy and are commonly employed to increase metabolic capacity and cell size. D. melanogasterfollicle cell gene amplification, in which bidirectional replication occurs in the absence of detectable gap phases, serves to produce large amounts of eggshell proteins and may also serve to regulate transcription. During D. melanogasterembryogenesis, mitotic cell cycles, endocycles and cell cycle exit occur concurrently. We undertook a screen to identify factors affecting developmentally regulated, variant cell cycles during D. melanogasterembryogenesis. We identified a class of mutants with apparently polyploid cells in normally diploid tissues indicating a failure to maintain mitotic cycles. In this class of mutants, we identified and characterized new mutants in pavarottiand tumbleweed, pav3CS3 and tumrn32a -2 .These mutants displayed phenotypic defects consistent with failures in cytokinesis. In particular, tum3 2a-2o displayed multinucleate cells and abnormal telophase spindles. We also describe the identification, cloning and characterization of the first cyclinE mutant to undergo aberrant gene amplification, cyclinE1 36 . We observed a novel gene amplification defect, dramatically increased replication fork progression in cyclinE'f36/cyclinEPs and cyclinE1 36/cyclinEP28 follicle cells implicating CyclinE in the regulation of replication fork speed. Thesis Supervisor: Terry L. Orr-Weaver Title: Professor of Biology To my family... and T.C. ACKNOWLEDGEMENTS I would like to thank my advisor Terry Orr-Weaver for her guidance and support. Her love for science and her integrity are inspiring. Thank you. Thanks also to the Orr-Weaver Lab, quite frankly, THE GREATEST LAB ON THE PLANET and special thanks to Tamar Resnick with whom I've had many helpful discussions. I would also like to thank my thesis committee for guidance. Thanks to David MacAlpine, Cary Lai and Steve Bell for consistently helpful and informative discussions and to my friends Eunice and Piyush who always had something interesting to say about science. Last but not least, special thanks to my little sister June who has been unflaggingly supportive. TABLE OF CONTENTS Chapter One: Introduction: The Developmental Regulation of DNA replication......................................... - Regulation of the mitotic cell cycle................................................................................8... Regulation of the endocycle...........................................................................................9 Gene amplification....................................................... ................................................ 12 Cyclin/Cdk and regulationof the Pre-ReplicationComplex............................ ... 15 R eplication Initiation................................................................................ - ............................... 16 Eukaryotic origins of replication....................................................................................16 Epigenetic determinantsof metazoan origin activity.....................................18 The Pre-ReplicationComplex......................................................................................19 A molecular mechanismfor Mcm2-7 loading at the Pre-ReplicationComplex..............20 Mechanisms of Cyclin/Cdk regulationof the Pre-ReplicationComplex........................20 The transitionto replication........................................................................................24 R eplication Elongation............................................................... - ................... .............................................. 25 Replication Fork Progression......................................................................................26 Summ ary.................................................................................................... .............................. 27 R eferences ..................................................................... ..................................... ...................... 29 Chapter Two: New mutants affecting developmentally regulated cell cycles during Drosophila embryogenesis ..................................... 37 Sum mary............................................................................................. 38 Introduction .................................................................................................................................... 46 Resu lts............................................................................................................................................ - A screenfor mutations affecting developmental cell cycle regulation.............................46 Class V mutants have large nuclei in the nervous system and epidermis................52 Characterizationand mapping of Ir8 and 3C157.......................................................55 Characterizationof 3C53 and 32a-20............................................................................58 3C53 and 32a-20 are alleles ofpavarottiand tumbleweed/RacGAP50..................61 D iscussion ................................................................................................................. - . . ........... 75 The identificationof mutants that affect developmental regulationof the cell cycle........75 New mutants that affect mitotic cell cycles in the nervous system.................................76 tum3• 2a -2 disrupts cytokinesis and shows central spindle defects........................................77 M aterials and M ethods................................................................................................................ R eferences......................................................................................................................................8 79 1 Chapter Three: The characterization of new cyclinE mutants that increase replication fork progression during gene amplification Sum m ary............................................................................................. ..................................... 85 Introduction............................................................................................... ............... ................. 86 Resu lts............................................................................................................................................9 1 - A new mutation in cyclinE that displays previously undescribeddefects in gene amplification............................................................................ .................................... 91 - cyclinEJl36 /cyclinEPz8 and cyclinEIP6/cyclinEPz8have expanded amplified regions at DAFC-66D, DAFC-30B and DAFC-34B.......................................................................94 - Increased replicationfork progression is not due to priorcell cycle defects........... 103 - Increasedreplicationfork progressionin cyclinEf36/cyclinEPz 8 follicle cells may reflect increasedreplicationfork speed.....................................................................................110 - Polyteny is intact in cyclinE"36/cyclinEPz follicle cells.....................................115 - cyclinE'f36 displays a dominant defect in replicationfork progression.......... .... 118 - Double Parkedand the MCM complex localize as double bars in cyclinEf36/cyclinEPz8 ................................ 122 follicle cells................................................................................ D iscussion...................................................................................... ........................................ 126 M aterials and M ethods......................................................... ................................................. 134 References........................................................................ ........................................ 137 Chapter Four: Conclusions and perspectives Conclusions and perspectives............................................................... References...................................................................................... ................................. ........................................ 143 152 CHAPTER ONE Introduction The Developmental Regulation of DNA Replication DNA replication is developmentally regulated during Drosophilamelanogaster development (Claycomb et al., 2002; Smith and Orr-Weaver, 1991). Endocycles, in which alternating S and G phases produce polyploidy, and replication-based gene amplification, are employed to increase tissue size and metabolic output. Drosophila endocycles occur during embryogenesis, larval development and oogenesis and are regulated by conserved replication factors. Gene amplification, in which successive replication initiation events and elongation occur in the absence of detectable gap phases, occurs during oogenesis. Drosophilafollicle cell gene amplification is employed to produce high copy numbers of chorion, or eggshell, genes (Spradling, 1981). Like endocycles, follicle cells employ conserved cell cycle regulators (Claycomb and OrrWeaver, 2005). The following chapter reviews developmental regulation of endocycles and gene amplification. In addition, current knowledge on mechanisms controlling DNA replication initiation and elongation are reviewed. Regulation of the mitotic cell cycle The archetypal cell cycle consists of G 1, S, G2 and M phases and is regulated by Cyclin/Cdk complexes consisting of a regulatory Cyclin subunit and a Cdk. Different Cyclin/Cdk complexes act in different phases of the cell cycle. In S. cerevisiae,Cyclin subunits confer phase-specificity on a single Cdk, Cdc28. The G1 Cyclins, the Clns, are required for passage through START which signifies commitment to the cell cycle and Sphase entry. The G2 Cyclins, the Clbs, act in S, G2 and M phases. Degradation of the Clbs is required for exit from mitosis (Reed, 1992). Unlike yeast, metazoans possess multiple Cdks (Sherr and Roberts, 1999; Solomon, 1993). CyclinE/Cdk2 activity is required for the G1/S transition. In mammals, CyclinA/Cdk2 regulates S-phase progression. CyclinA/Cdkl and CyclinB/Cdkl activities are required for mitosis. CyclinD/Cdk4 and CyclinD/Cdk6 mediate the convergence of growth factor signaling on the cell cycle and are thought to indirectly regulate S-phase entry by potentiating CyclinE/Cdk2 activity (Perez-Roger et al., 1999; Sherr and Roberts, 1999). Cyclin/Cdk is regulated redundantly during the cell cycle. Mechanisms for regulating Cyclin/Cdk activity include oscillatory Cyclin expression, regulatory phosphorylation, inhibition by Cyclin/Cdk inhibitors (CKI) and the targeted degradation of Cyclins. Regulation of the endocycle Endocycles consist, minimally, of discrete S and G1 phases with one round of DNA replication occurring per endocycle (Smith and Orr-Weaver, 1991). Some endocycling tissues show vestiges of mitosis ranging from chromosome condensation to nuclear divisions (Edgar and Orr-Weaver, 2001) and utilize mitotic machinery to regulate Cyclin/Cdk activity. During mitotic cycles, the APC, an E3 ubiquitin ligase, marks Cyclins for degradation by the 26S proteasome. Mutations in morula, an APC subunit, lead to ectopic spindle formation and chromosome condensation in Drosophilanurse cells undergoing endocycles, suggesting that mitotic regulators are expressed at low levels in these cells (Kashevsky et al., 2002; Reed and Orr-Weaver, 1997). APC activity may be required for establishing Drosophilaembryonic endocycles by clearing mitotic Cyclins. Mutants in an APC coactivator, fizzy-related (fzr), fail to initiate embryonic endocycles and fzr is developmentally regulated by Notch in a mitotic to endocycle switch during oogenesis (Schaeffer et al., 2004; Sigrist and Lehner, 1997). In addition, mitotic cyclin transcription is shut off during Drosophilaembryonic endocycles (Weiss et al., 1998). Together, these observations suggest that endocycles arise from downregulation of mitosis specific regulators and support the idea that endocycles are a modification of the archetypal mitotic cell cycle. Some endocycles show no vestiges of mitosis and may achieve oscillatory Cyclin/Cdk activity through means that don't involve the APC or mitotic Cyclins. Cyclin E/Cdk2 is important for mammalian endocycles. Double knockouts of the two murine isoforms of CyclinE, CCNE1 and CCNE2, die midgestation due to defects in the placenta without any apparent defects in embryos. Specifically, the trophoblast giant cells do not attain normal levels of polyploidy. This may reflect the particular importance of CyclinE/Cdk2 in regulating mammalian endocycles (Berthet et al., 2003; Geng et al., 2003; Parisi et al., 2003). In Drosophila,CyclinE is required for embryonic endocycles (Knoblich et al., 1994). cyclinE transcription corresponds with S-phase in the Drosophilaendocycling tissues and is key to developmental regulation of endocycles (Knoblich et al., 1994; Lilly and Spradling, 1996). cyclinE is not expressed in intervening gap phases, suggesting that endocycles are driven by pulses of cyclinE (Knoblich et al., 1994; Lilly and Spradling, 1996). Low CyclinE levels between pulses of cyclinE transcription are required for replication. Ectopic expression of cyclinE in Drosophilalarval endocycling tissues inhibits S-phase (Follette et al., 1998; Weiss et al., 1998). Cyclical cyclinE transcription is important for endocycles and a biphasic oscillator, consisting of the E2F1/Rbf transcription factor and the CyclinE/Cdk2 inhibitor Dacapo, has been postulated to regulate cyclinE transcription (Edgar and Orr-Weaver, 2001). In the endocycling tissues of the Drosophilaembryo, the E2F1 transcription factor regulates cyclinE expression as part of a G1/S transcriptional program (Asano and Wharton, 1999; Duronio and O'Farrell, 1994; Royzman et al., 1997). A positive feedback loop, in which CyclinE/Cdk2 hyperphosphorylates and inactivates Rbf, the E2F1 repressor, poses a mechanism for upregulating cyclinE. CyclinE activates expression of the CyclinE/Cdk2 inhibitor dacapo, which encodes a CIP/KIP family member, thereby inhibiting CyclinE/Cdk2 (de Nooij et al., 2000; Lane et al., 1996). Dacapo presents a mechanism for downregulating CyclinE protein levels by inhibiting CyclinE/Cdk2 activity allowing accumulation of hypophosphorylated Rbf, which shuts off E2F1mediated cyclinE expression. Together, these regulatory loops may define a biphasic oscillator for endocycles that ensures alternating S and G1 phases in endocycles (Edgar and Orr-Weaver, 2001). Both developmental signaling and growth signaling play key roles in endocycle progression. During Drosophilaembryogenesis, endocycles occur in a precise pattern corresponding to developmental stage (Smith and Orr-Weaver, 1991). Notch signaling is involved in the mitotic to endocycle switch in Drosophilafollicle cell endocycles and induces transcriptional changes in dacapo,fzr and string (Deng et al., 2001; Schaeffer et al., 2004; Shcherbata et al., 2004). Drosophilalarval endocycles are inhibited by nutrient deprivation (Britton and Edgar, 1998) and Ras and c-myc overexpression in mitotically proliferating cells induce growth and hasten the G1/S transition, suggesting that growth signaling also regulates the cell cycle (Johnston et al., 1999; Prober and Edgar, 2000). A study of CIn3 translation in S. cerevisiae suggests another mechanism for coupling growth to the endocycle. Cln3 mRNA carries a 5' untranslated open reading frame (ORF) that reduces the efficiency of Cln3 translation, suggesting that Cln3 protein synthesis reflects cellular ribosomal content (Polymenis and Schmidt, 1997). cyclinE mRNA carries a number of 5' untranslated ORFs and mutations in eIF4A, a translation initiation factor, confer defects in DNA replication (Galloni and Edgar, 1999). These results suggest that cyclinE may act as a growth sensor in metazoan cells. Gene amplification Gene amplification is a replication-based method for increasing the output of a gene. Replication based gene amplification occurs in Amphibians, Insects and the marine ciliate Tetrahymena thermophila.Amphibians, Tetrahymena and Pterygotan insects amplify rDNA through extrachromasomal mechanisms. Dipteran insects employ gene amplification to increase the copy number of structural genes required for egg maturation (Claycomb and Orr-Weaver, 2005). The best-characterized example of gene amplification occurs in follicle cells during Drosophilaoogenesis. During Drosophilafollicle cell gene amplification, repeated replication initiation events, occurring without detectable gap phases, generate high copy numbers of chorion genes required for eggshell formation (Spradling, 1981). These replication initiation events generate multiple tandem replication forks that move bi-directionally and generate an onion-skin structure (Fig. 1). Gene amplification occurs at a handful of genomic sites known collectively as the DrosophilaAmplicons of follicle Figure 1. Gene amplification in Drosophila follicle cells occurs by repeated replication initiation events that generate tandem replication forks moving away from a central region. Gene amplification is visualized by BrdU-incorporation at follicle cell amplicons. (A-C) BrdU incorporation in single CantonS wildtype follicle cells in stage 10B (A), stage 11 (B) and stage 13 (C) egg chambers. In stage 10B egg chambers, follicle cells show 4-6 BrdU-labeled foci corresponding to replication at follicle cell amplicons. In the example shown (A), 4 BrdUlabeled foci are evident and the major focus (arrow) corresponds to repeated replication initiation events generating bi-directional, tandem replication forks at DAFC-66D. Replication initiation and the generation of tandem replication forks in stage 10B are diagrammed to the right of (A) with BrdU-labeling shown in pink. In stage 11 (B), only DAFC-66D (arrow) continues to gene amplify. The last replication initiation events at DAFC-66D occur during this stage although replication elongation continues through stages 12 and 13. By stage 13, BrdU-labeling reveals a double bar structure at DAFC-66D (arrow). The double bar corresponds to BrdU incorporated by opposing sets of tandem replication forks - diagrammed to the right of (C) with BrdU incorporation in pink. Tandem replication forks have moved apart following cessation of replication initiation events in stage 11 prior to the start of BrdU-labeling and incorporate BrdU at distant sites. stage 10B 0-- stage 11 ~·lc~\· ~11"1~· ~I~ ~c~s CeLIIIII~ stage 13 IIIIILe ~cllrrr, Cells, or DAFC. During gene amplification replication initiation events are developmentally regulated: DAFC-66D undergoes replication initiation events in stages 10B and 11 and only replication elongation occurs from stage 12 on (Fig. 1). (Claycomb et al., 2004; Claycomb et al., 2002). Replication elongation can be visualized cytologically by BrdU-incorporation at elongating replication forks (Fig. 1) (Claycomb et al., 2002). Gene amplification is regulated by CyclinE. High CyclinE levels are thought to restrict genomic replication (Calvi et al., 1998). DAFC escape this control and conserved replication factors, components of the Pre-Replication Complex (Pre-RC) localize to the amplicons (Asano and Wharton, 1999; Austin et al., 1999; Claycomb et al., 2002; Royzman et al., 1999; Whittaker et al., 2000). Cyclin/Cdk and regulation of the Pre-ReplicationComplex Low Cyclin/Cdk activity in G of mitotic and endocycles is required for assembly of the Pre-Replication Complex (Pre-RC) at origins of replication. The Pre-RC is an assembly of the Origin Recognition Complex (ORC), Double Parked/Cdtl, Cdc6 and the Mcm2-7 complex (Dutta and Bell, 1997). Regulated assembly of the Pre-RC in G licenses origins of replication for firing in S-phase. Once-per-cell-cycle assembly enforces once-per-cell-cycle genomic replication. Cyclin/Cdk phosphorylation of the PreRC regulates nuclear compartmentalization, chromatin association, protein stability, and activity of complex members (Findeisen et al., 1999; Hendrickson et al., 1996; Ishimi et al., 2000; Labib et al., 1999). Redundant, Cyclin/Cdk dependent mechanisms for regulating Pre-RC assembly is supported by studies of re-replication in yeast in which multiple Pre-RC components must be disrupted to achieve significant re-replication (Gopalakrishnan et al., 2001; Nguyen et al., 2001). More recently, the direct binding of Cyclins to replication factors (Clb2 to Cdc6 and Clb5 to Orc6) in S. cerevisiae have presented a novel Cyclin-dependent mechanism for inhibiting Pre-RC assembly (Mimura et al., 2004; Wilmes et al., 2004). Gene amplification is different from the mitotic and endocycle in that there are no detectable gap phases. CyclinE levels are constitutively high throughout the nucleus (Calvi et al., 1998). In spite of this, the Pre-RC localizes to DAFC. Orc2, Orcl, Orc5, DUP/Cdtl and Mcm2-7 localize to amplifying foci (Asano and Wharton, 1999; Austin et al., 1999; Claycomb et al., 2002; Royzman et al., 1999; Whittaker et al., 2000) and mutations in Pre-RC components Orc2, DUP/Cdtl, and Mcm6 result in reduced gene amplification and corresponding thin eggshells (Landis et al., 1997; Schwed et al., 2002; Whittaker et al., 2000). CyclinE/Cdk2 may be locally regulated or a molecular switch may function to allow reiterative replication initiation. In addition, an ortholog of the Sphase kinase Dbf4/Cdc7, which is required for replication initiation in mitotic cells, may be required for gene amplification. Mutants in chiffon, which shows homology to the Cdc7 kinase cofactor Dbf4, displays reduced gene amplification (Landis and Tower, 1999). Replication Initiation Eukaryotic origins of replication Genetic screens for autonomously replicating sequences (ARS) led to the identification of sequence-conserved origins of replication in S. cerevisiae (Stinchcomb et al., 1979; Struhl et al., 1979). Origins of replication bind ORC, which nucleates PreRC assembly thereby defining sites of replication initiation. S. cerevisiaeorigins of replication are atypical for eukaryotes in that they consist of several well-defined sequence elements (10-20 bp) spread over an approximate 200 bp interval. The Aelement consists of the 11 bp ARS consensus sequence (ACS) and is necessary but not sufficient for origin activity. B-elements contribute to origin activity to varying degrees but as a group, are essential (Dutta and Bell, 1997). Like S. cerevisiae, S. pombe and Yarrowia lipolytica origins demonstrate ARS activity but unlike S. cerevisiae, they lack consensus sequences (Vernis et al., 1997; Vernis et al., 1999). These origins are AT rich and approximately 1 kb in size and S. pombe Orc4p carries a specialized binding domain that recognizes AT rich sequences (Chuang and Kelly, 1999). Metazoan replicators are more complicated. Generally, yeast replicators encompass a single, preferred replication initiation site or origin of replication. Metazoan origins may encompass several replication initiation sites without a predominant preferred origin of replication and range in size from 1 to 50 kb (Bielinsky and Gerbi, 2001). Comparisons of these replicators have not yielded consensus sequences or conserved sequence features. Metazoa show developmental plasticity and cell-type specificity in origin usage and this may indicate the epigenetic nature of metazoan origins (Blow, 2001). In Drosophilagene amplification at DAFC-66D, the ORC binding sites are sequence defined at ACE3 (Amplification Control Element 3) and orif3 (Austin et al., 1999). Epigenetic determinantsof metazoan origin activity Chromatin structure, including covalent modification of DNA and modifications of chromatin packaging proteins, regulate origin usage. CpG methylation inhibits replication initiation: Methylated DNA does not bind ORC in Xenopus egg extracts, CpG islands are correlated with metazoan origins, and methylase deficient cell lines show less localized replication (Delgado et al., 1998; Gilbert, 2004; Harvey and Newport, 2003a; Rein et al., 1999). In addition, chromatin structural changes such as histone acetylation affect replication initiation. In Drosophila,during follicle cell gene amplification, mutations in the histone deacetyltransferase Rpd-3 result in nuclear localization of ORC and genomic replication, suggesting that histone acetylation promotes origin usage. Consistent with this, tethering Rpd-3 or polycomb to gene amplifying origins of replication reduces replication while tethering the acetyltransferase Chameau increases replication (Aggarwal and Calvi, 2004). Transcription may promote an open chromatin configuration that is favorable for replication initiation. Numerous transcription factors affect Drosophilafollicle cell gene amplification. Mutants in E2F1, E2F2, DP, Rbfl, Myb, Mipl20 and Mipl30 lead to gene amplification defects (Beall et al., 2002; Bosco et al., 2001; Cayirlioglu et al., 2003; Royzman et al., 1999). Mutants in E2F2, Myb and Mipl30 disrupt origin specification in Drosophilafollicle cells. These mutants undergo genomic replication rather than gene amplification (Beall et al., 2004; Beall et al., 2002; Cayirlioglu et al., 2001; Cayirlioglu et al., 2003). Transcription factors may impinge on gene amplification by recruiting chromatin re-modeling factors, which influence origin usage (Aggarwal and Calvi, 2004; Bosco et al., 2001). Topological factors may also affect replication initiation. Eukaryotic replication origins are distributed in intergenic regions (Wyrick et al., 2001). Active transcription may generate negative supercoils in intergenic regions, which may play a role in origin specification. Interestingly, DrosophilaORC has been shown to bind preferentially to negatively supercoiled DNA (Remus et al., 2004). The Pre-ReplicationComplex The order of Pre-Replication Complex assembly was determined by immunodepletion experiments in Xenopus and through experiments utilizing temperature-sensitive alleles in yeast. In summary, ORC is required for Cdc6 and DUP/Cdtl binding to origins, which are required, in turn, for loading of the Mcm2-7 complex, the putative replicative helicase (Maiorano et al., 2000; Tanaka et al., 1997). Pre-RC assembly is regulated by Cyclins by Cyclin/Cdk phosphorylation and inhibitory binding by Cyclins (Mimura et al., 2004; Wilmes et al., 2004). The Pre-RC is conserved in yeast, flies, mammals, Xenopus and plants, suggesting that mechanisms for replication are conserved across eukaryotes. In addition, Pre-RC components are necessary for mitotic cell cycles, endocycles and Drosophilafollicle cell gene amplification indicating conserved mechanisms across different modes of DNA replication. A molecular mechanismfor Mcm2-7 loading at the Pre-ReplicationComplex In S. cerevisiae, ORC has been shown to bind DNA cooperatively with Cdc6 in an ATP-dependent manner (Speck et al., 2005). In Xenopus, Cdc6 is known to stabilize ORC binding to chromatin (Harvey and Newport, 2003b). In Xenopus, DUP/Cdtl localizes to origins after Cdc6 (Tsuyama et al., 2005). Cdc6 ATPase activity is ORC- and origin DNA-dependent and functions at a step prior to ORC ATP hydrolysis, which is required for Mcm2-7 loading (Bowers et al., 2004). Loss of Cdc6 ATPase activity stabilizes DUP/Cdtl at origins and prevents Mcm2-7 loading. As is the case in S. cerevisiae, ORC and Cdc6 ATPase activities are required for Mcm2-7 loading (Harvey and Newport, 2003b). These observations suggest a molecular machine that loads Mcm27 onto replication origins in an orderly manner in the following scheme: ORC and Cdc6 bind cooperatively to origins. DUP/Cdtl localizes after Cdc6 binding. ORC-Cdc6 cooperative binding triggers Cdc6 ATPase activity. ORC ATPase activity soon follows and Cdc6 ATPase activity either directly or indirectly results in re-modeling of the complex accompanied by Mcm2-7 loading and DUP/Cdtl release (Fig. 2). Mechanisms of Cyclin/Cdk regulationof the Pre-ReplicationComplex Cyclin/Cdk regulation of the Pre-RC is varied and redundant and regulates nuclear compartmentalization, chromatin binding, catalytic activity and protein stability. In Xenopus and Drosophila,high Cyclin/Cdk activity inhibits ORC binding to chromatin (Findeisen et al., 1999; Remus et al., 2005). In mammals, Cdk phosphorylation of Cdc6 at N-terminal sites exposes a nuclear export signal leading to nuclear export in S phase Figure 2. Replication initiation. In mitotic and endocycles, Pre-Replication Complex assembly at origins of replication is restricted to G1 during a period of low Cyclin/Cdk (CDK) activity. Regulation of PreReplication Complex assembly is key to once-per-cell-cycle control of DNA replication. (A) Pre-Replication Complex assembly begins with cooperative ORC and Cdc6 binding to origin DNA. DUP/Cdtl localizes after Cdc6. Sequential ATP hydrolysis by Cdc6, then ORC, leads to Mcm2-7 loading and completion of the Pre-Replication Complex (B). (C) At replication initiation, McmlO localizes. S-phase kinases Dbf4/Cdc7 (DDK) and Cyclin/Cdk (CDK) are required for localization of Cdc45, which subsequently travels with the replication fork. Sld3 is required for Cdc45 localization during replication initiation. A. Cdc6 and ORC cooperative binding ;/0, Cdc6 ATPase, ORC ATPase B. The Pre-Replication Complex ~KLJX~ DDK, CDK C. Generation of the functional helicase Duj sZ74ýý (Delmolino et al., 2001). In addition, Cdc6 degradation is signaled by ubiquitylation by the SCF/Cdc4 E3 ligase in S. cerevisiae(Perkins et al., 2001) and in vitro experiments indicate that Cdc6 degradation occurs following Cyclin/Cdk phosphorylation of Cdc6 (Elsasser et al., 1999). Pre-RC assembly is also regulated by Cyclins binding to ORC and Cdc6. Clb5 binds to and inhibits Orc6 and Clb2 binds to and inhibits Cdc6 in S. cerevisiae(Mimura et al., 2004; Wilmes et al., 2004). Cyclin/Cdk regulation of DUP/Cdtl affects chromatin binding and protein stability. CyclinA/Cdk phosphorylation has been shown to inhibit chromatin binding of human DUP/Cdtl in vitro and inhibition of Cdkl activity in murine cells leads to accumulation of dephosphorylated DUP/Cdtl onto chromatin (Sugimoto et al., 2004). In addition to chromatin localization, Cyclin/Cdk regulates DUP/Cdtl abundance. CyclinA/Cdk2 phosphorylaton of human DUP/Cdtl has been shown to promote DUP/Cdtl binding to the Skp2 F-box protein, a cofactor for the SCF E3 ligase, which has been shown to target DUP/Cdtl for proteolysis (Nishitani et al., 2006; Sugimoto et al., 2004). In Drosophila,consensus Cdk phosphorylation sites in the N-terminus of DUP/Cdtl are required for cell cycle dependent degradation and DUP/Cdtl degradation appears to be dependent on CyclinE/Cdk2 phosphorylation (Thomer et al., 2004). Cyclin/Cdk regulates chromatin binding of the MCM complex. Phosphorylation of Xenopus Mcm4 by CyclinB/Cdkl reduces its affinity for chromatin (Hendrickson et al, 1996). There is also evidence that Cdk2 phosphorylation of Mcm2 primes this subunit for phosphorylation by other kinases regulating chromatin association (Montagnoli et al., 2006). The transitionto replication Following formation of the Pre-RC, the transition to replication requires the loading of multiple factors that unwind DNA and localize DNA polymerases (Fig. 2) (Pacek et al., 2006; Wohlschlegel et al., 2002). These include McmlO, Cdc45/Sld3, th GINS complex and Dpbl1/Sld2. In Xenopus and S. cerevisiae,Mcml0O binds to origins in an Mcm2-7 dependent manner. Cdc45 localization, in turn, is dependent on Mcml0O (Sawyer et al., 2004; Wohlschlegel et al., 2002) and, in yeast, on Sld3 with which it forms a complex (Kamimura et al., 2001; Kanemaki and Labib, 2006; Nakajima and Masukata, 2002). Two other protein complexes, localize to origins at replication. These are the GINS complex and Dpbl 1/Sld2. This assembly of complexes is required for recruiting DNA polymerases. Mcml0O and Cdc45 are primarily responsible for localization of DNApola-primase (Mimura et al., 2000; Ricke and Bielinsky, 2004; Uchiyama et al., 2001; Zou and Stillman, 2000). Recruitment of DNApolE to origins requires the GINS complex and Dpbl 1/Sld2 (Takayama et al., 2003). Two S-phase kinases regulate replication initiation: Cyclin/Cdk and Dbf4/Cdc7. In Xenopus, Dbf4/Cdc7 associates with chromatin in an Mcm2-7 dependent manner prior to Cdc45 localization (Jares and Blow, 2000; Jares et al., 2004). Sequential kinase activity appears to be important for DNA replication. In a Xenopus cell-free system, exposure of chromatin to Dbf4/Cdc7 and Cyclin/Cdk2 promoted efficient DNA replication but exposure of chromatin to these kinases in the reverse order did not (Walter, 2000). Cyclin/Cdk phosphorylation may promote initiation by promoting Dpbl 1/Sld2 assembly. Mutation of all the potential Cdk phosphorylation sites of Sld2 has been shown to inhibit complex assembly and replication (Tak et al., 2006). Replication Elongation Several of the proteins involved in the transition to replication and in replication fork biogenesis travel with the replication fork. Mcml0, Cdc45, and the GINS complex have been identified at replication forks in Xenopus and S. cerevisiae (Aparicio et al., 1997; Calzada et al., 2005; Gambus et al., 2006; Pacek et al., 2006). Mutants in S. cerevisiae McmlO0 and Cdc45 show stalled replication forks (Merchant et al., 1997; Tercero et al., 2000). Recently, a Cdc45/Mcm2-7/GINS (CMG) complex associated with helicase activity was purified from Drosophilaextracts suggesting that this complex comprises the replication fork helicase (Moyer et al., 2006). Three DNA polymerases localize to the replication fork: DNApola-primase, DNApol8 and DNApolE (Garg and Burgers, 2005). DNA pola-primase possesses RNA and DNA polymerase activities and mediates priming at initiation to start leading strand synthesis and travels with the replication fork to prime lagging strand synthesis. DNApolI is thought to mediate Okazaki fragment maturation during lagging strand synthesis. DNApols is thought to perform leading strand synthesis. In addition, RPA, RFC, and PCNA are loaded. RPA consists of three subunits and is functionally homologous to E. coli SSB and binds to single-stranded DNA. PCNA is a trimeric sliding clamp that increases the processivity of DNA polymerases. RFC loads PCNA. Replication Fork Progression Replication Fork Progression (RFP) is regulated by DNA secondary structure and chromatin bound proteins. Differences in Replication Fork Speed (RFS) have been observed for cells employing different modes of DNA replication. In Drosophiladiploid cells, replication forks move at ~2.6 kb/min (Blumenthal et al., 1974). The RFS for Drosophilapolytene larval salivary glands has been measured at ~300 bp/min (Steinemann, 1981). During gene amplification, replication forks move at about ~50-100 bp/min (Spradling and Leys, 1988). These differences may be due to chromatin structure (for example, the persistence of cohesins on polytene chromosomes) or topological factors. Multiple, tandem replication forks during gene amplification may generate significant superhelical strain. At DAFC-66D, -~5 replication forks moving in the same direction are spaced -~10kb apart. RFS and RFP are also regulated by protein factors at the replication fork. Helicases are common targets for modulating RFP. Replication fork progression at normal speeds through S. cerevisiae telomeric and subtelomeric sequences requires the Rrm3p helicase, suggesting that cellular helicases have specialized functions (Ivessa et al., 2002). Not surprisingly, replication fork pausing mechanisms often target the helicase. During prokaryotic replication termination, the trans-acting factors Tus in E. coli and RTP in B. subtilis bind to and inhibit the replicative helicase (Bussiere and Bastia, 1999). In a proof-of-principle, a protein inhibitor of the replicative helicase was shown to reduce replication fork speed In E. coli, (Skarstad and Wold, 1995). Helicase activity is regulated by Cyclin/Cdk phosphorylation (Ishimi et al., 2000), and this may be an important mechanism for regulating replication fork speed. Regulation of replication fork progession may be important for gene expression. Polar intergenic Replication Fork Barriers (RFB), block replication fork progression opposing transcription at the rDNA locus of S. cerevisiae, S. pombe, mouse and Xenopus (Rothstein et al., 2000). In E. coli, head-on transcription severely inhibits replication fork progression while co-directional transcription does not, revealing the importance of coordinated transcription and replication (Mirkin and Mirkin, 2005). The interplay between DNA replication machinery and transcriptional machinery is not necessarily direct. Transcription factors may affect nucleosome arrangement or recruit chromatin remodeling machinery (Bosco et al., 2001). During Drosophilafollicle cell gene amplification, mutants in transcription factors affect replication initiation (Beall et al., 2004; Beall et al., 2002; Bosco et al., 2001; Royzman et al., 1999). Some of these mutants may affect replication fork progression. Summary The mechanisms regulating DNA replication are conserved between mitotic cell cycles, endocycles and Drosophilafollicle cell gene amplification. A period of low Cyclin/Cdk, a G1 phase, in which the Pre-RC can assemble is conserved between mitotic and endocycles. The Pre-RC is conserved during Drosophilafollicle cell gene amplification. Mechanisms for regulating replication initiation are conserved between different modes of DNA replication. Aspects of replication fork progression are likely to be conserved. Mcm2-7, Cdc45 and PCNA travel with the replication forks in mitotic cells (Claycomb et al., 2002; Loebel et al., 2000). These proteins co-localize with replication forks during gene amplification. In addition, DUP/Cdtl, co-localizes with replication forks during gene amplification. It has been postulated that DUP/Cdtl is required at the replication forks to maintain Mcm2-7 at slow-moving replication forks (Claycomb et al., 2002). We performed a screen to identify developmental regulators of mitotic and endocycles during Drosophilaembryogenesis. Three cell cycle phenomena - cell cycle exit, mitotic cell cycles and endocycles - occur concurrently during Drosophila embryogenesis. We took advantage of this period to screen for developmental regulators of S-phase using PCNA, as an S-phase marker. We identified a class of mutants that displayed large nuclei in normally diploid tissues. In this class, we identified new mutations in pavarotti and tumbleweed, pav3C53 and tum32a-20, which are required for cytokinesis. In addition, we characterized a new cyclinE mutant, cyclinElf36 , displaying increased replication fork progression during gene amplification. 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Orr-Weaver Whitehead Institute and Dept. of Biology, Massachusetts Institute of Technology, Cambridge, MA 02142 SUMMARY During Drosophilaembryogenesis, cell cycle exit, mitotic cell cycles and endocycles all occur within a narrow time span. The developmental patterning of these cell cycles are well characterized and afford a unique opportunity to study developmental regulation of the cell cycle. We screened 300 EMS mutants for developmentally uncoordinated replication by an in situ hybridization assay for PCNA transcription, a marker of the G1/S transition. We identified 30 mutants that may reflect functions in developmental signaling, G1/S transcription and DNA replication. We further characterized a class of mutants displaying large, apparently polyploid nuclei in normally diploid cells. 3C157, Ir8 and 2k32 - of which 3C157 and Ir8 are allelic - displayed large and diffuse DNA masses in isolated cells of the nervous system. 32a-20 (formerly 32a) and 3C53 displayed large nuclei in the nervous system and epidermis. We cloned these mutants and identified new alleles of tumbleweed, tum3 2a-20 , and pavarotti, pavC3 53. These mutants have defects consistent with blocks to cytokinesis. INTRODUCTION In metazoans, divergent cell cycles must be regulated accurately throughout development to build and maintain a viable organism. The G1/S/G2/M cell cycle is only one of multiple cell cycles. Variants of the archetypal cell cycle are utilized in different developmental contexts to achieve different aims. The early embryonic divisions of insects, marine invertebrates and amphibians are rapid S/M cycles. These cycles allow for speedy embryogenesis, potentially important for organisms with exposed and vulnerable embryos. Endocycles are variants of the archetypal cell cycle that lack complete mitoses but consist of discrete S and G1 phases with one round of DNA replication occurring per endocycle (Smith and Orr-Weaver, 1991). These cycles generate polyploidy and are thought to be a strategy for increasing growth and metabolic capacity without the large scale cytoskeletal rearrangements required by mitosis (Edgar and Orr-Weaver, 2001). A key requirement for all of these cell cycles is the restriction of Cyclin/Cdk activity. A window of low Cyclin/Cdk activity is required for assembly of pre-replication complexes at replication origins (Hua et al., 1997). During G1/S/G2/M cycles, Cyclin/Cdk activity remains high throughout the cell cycles except for a window in early G1 following downregulation of Cyclins A and B and preceding upregulation of CyclinE. During the early embryonic S/M cycles of Xenopus, nuclear compartmentalization restricts Cyclin/Cdk activity (Blow and Laskey, 1988). Some endocycling tissues show vestiges of mitosis ranging from chromosome condensation to nuclear envelope breakdown (Edgar and Orr-Weaver, 2001) and utilize mitotic machinery to achieve low Cyclin/Cdk activity. Mutations in morula, an APC subunit, lead to ectopic spindle formation and chromosome condensation in Drosophilanurse cells suggesting that regulators of mitosis are expressed at low levels in these cells (Kashevsky et al., 2002; Reed and Orr-Weaver, 1997). To modulate activity, Cyclin/Cdk complexes are regulated on many levels including oscillatory Cyclin expression, regulatory phosphorylation, inhibition by Cyclin/Cdk inhibitors (CKI), and through targeted degradation of Cyclins. Developmental signaling plays a key role in regulating different cell cycles. In Drosophila,Notch signaling mediates a mitotic to endocycle switch in ovarian follicle cells, and no less than 36 pattern formation genes are involved in the developmental regulation of mitotic cell cycles during embryogenesis (Deng et al., 2001; Edgar et al., 1994; Keller Larkin et al., 1999; Schaeffer et al., 2004; Shcherbata et al., 2004). Drosophilaembryogenesis provides an elegant example of developmental regulation of the cell cycle. Cell cycle exit and three different cell cycles - S/M, S/G2/M and S/G occur dynamically in a 6 hour time span (Fig. 1). Cycles 1-13 consist of rapidly alternating S and M phases and are nuclear divisions that occur more or less synchronously in a common cytoplasm. Cycles 14-16, the postblastoderm divisions, consist of S, G2 and M phases. These divisions (S/G2/M) occur in mitotic domains in which cells differentiating into the same tissue undergo mitosis synchronously and at the same developmental time (Foe et al., 1993). Following cycle 16, the embryonic epidermis exits the cell cycle while cells of the developing nervous system continue to undergo mitotic cycles. Also following cycle 16, the developing larval tissues initiate endocycles consisting of S and G phases and continue these through embryogenesis and larval development resulting in highly polytene tissues. Embryonic endocycles occur in spatiotemporal domains reminiscent of the mitotic domains of the postblastoderm divisions (Fig. 2) (Smith and Orr-Weaver, 1991). Figure 1. Diagram of variant cell cycles utilized during embryogenesis. Following fertilization, cell cycles 1-13 are syncitial divisions that occur synchronously in a common cytoplasm. These rapid S/M cycles correspond to stages 1-8 of embryonic development. By cycle 14, cellularization is complete and a gap phase is added coincident with a requirement for zygotic string/CDC25transcription. Cycles 14-16 (the postblastoderm divisions) consist of S/G2/M phases and occur in mitotic domains in which groups of cells differentiating together undergo mitoses at different times. The dorsal epidermis undergoes cycles 14, 15, and 16 in stages 9, 10 and 11 respectively. Following cycle 16, the epidermis exits the cell cycle in stages 11 and 12 (not shown). The developing nervous system continues to cycle mitotically while the endodomains, or developing larval tissues, initiate S/G endocycles in stage 11. Shown in the image is a stage 12 embryo (anterior is to the left) in situ hybridized with antisense riboprobe against PCNA, which is expressed at G1/S, to visualize the nervous system (NS) and the endodomains (ENDO). 1-13 Syncytial Divisions M 4 14-16 Postblastoderm Divisions G2 M! S M G2 17 Endo Cell Cycle 17 Mitotic Cell Cycle I CNS ENDO \\ Figure 2. Embryonic endocycles in the larval tissues occur in developmentally regulated spatiotemporal domains. (A-F) Endocycle domains are shown in color at the developmental stage in which they undergo DNA replication (figure taken from Smith & Orr-Weaver, 1991). Gray shading indicates larval tissues not undergoing DNA replication in a given developmental stage. (A) As the germband begins to retract in stage 11, the salivary gland undergoes the first detectable endocycle S-phase 3 hours after the last mitosis (green). (B) During germband retraction in stage 12, the anterior and posterior midgut (am and pm) undergo DNA replication (red) along with isolated large nuclei between am and pm (red dots). (C) During dorsal closure in stage 13, DNA replication continues in the anterior and posterior midgut (red). The hingut undergoes DNA replication (hg, yellow) and shortly thereafter the Malpighian tubules initiate DNA replication 4.5 hours after the last mitosis (mt, purple). (D) During head involution in stage 14, replication continues in the anterior and posterior of the midgut (red), hindgut (yellow) and Malpighian tubules (purple). In addition, a 2 nd round of DNA replication initiates in a stripe in the central region of the midgut (mg, blue). (E) In stage 15 with the first constriction of the sac-like central midgut, the stripe of replicating tissue expands anteriorly and posteriorly (blue) and a group of dorsally located cells extending along the posterior part of the embryo undergoes DNA replication (pink). (F) In stage 16 as the midgut convolutes, replication extends throughout the midgut (blue) and continues in the dorsally located cells (pink). A P vi ml A L ~KJ~j LI)I F dc IF ~CCLL/LI Transcriptional regulation is key to developmental control of the cell cycle. The mitotic domains of the postblastoderm divisions arise from the zygotic transcription of string/CDC25phosphatase, an activator of Cdkl that regulates the G2/M transition (Edgar et al., 1994; Edgar and O'Farrell, 1990). String (stg) transcription occurs in pulses anticipating mitoses in each mitotic domain. Epidermal cell cycle exit requires developmentally coordinated changes in the transcriptional regulation of three genes. cyclinE transcription is downregulated. fizzy-related (fzr), an APC co-activator related to S. cerevisiae Cdhl, is transcriptionally upregulated. dacapo (dap), a CIP/KIP family CyclinE/Cdk2 inhibitor, is also transcriptionally upregulated (de Nooij et al., 1996; Knoblich et al., 1994; Lane et al., 1996; Sigrist and Lehner, 1997). Perturbation of any of these transcriptional regulatory events leads to a complete additional round of cell division. Embryonic endocycles coincide with pulses of cyclinE andfzr transcription (Knoblich et al., 1994; Sigrist and Lehner, 1997). Transcription of cyclinE andfzr occurs in a spatiotemporal pattern mirroring endocycle S-phases and expression of both genes is required for endocycle S-phase (Knoblich et al., 1994; Sigrist and Lehner, 1997). The periodic transcription of cyclinE is clearly important for endocycles, as continuous ectopic expression of cyclinE inhibits S-phases (Sauer et al., 1995). fzr transcription is probably required to reduce mitotic Cyclin/Cdk activity (Reed and Orr-Weaver, 1997; Sigrist and Lehner, 1997). The complex developmental control of cell cycle regulators is almost certainly due to complex promoters that contain modular cis-elements. The cyclinE and string promoters span 10 kb and 15 kb respectively (Edgar et al., 1994; Jones et al., 2000). Tissue-specific elements have been defined in the promoters of cyclinE, string and dacapo and multiple developmental cues are likely to converge on these promoters (Deng et al., 2001; Edgar et al., 1994; Jones et al., 2000; Meyer et al., 2002; Schaeffer et al., 2004). In addition to stg, cyclinE,fzr, and dap, an E2F regulated G1/S transcriptional program is developmentally regulated during embryogenesis (Asano and Wharton, 1999; Duronio and O'Farrell, 1994; Duronio and O'Farrell, 1995; Royzman et al., 1997; Whittaker et al., 2000). This program precedes S-phase in the endodomains. Developmentally coordinated E2F mediated transcription is required for normal endocycle S-phase (Duronio et al., 1998; Royzman et al., 1997). This program includes PCNA (DNA polymerase processivity factor), RNR1 and RNR2 (ribonucleotide reductase subunits), Double Parked(a replication initiation factor), Orcl (a component of the replication initiator complex) and cyclinE (Asano and Wharton, 1999; Duronio and O'Farrell, 1994; Royzman et al., 1997; Whittaker et al., 2000). To better understand the relationships between variant cell cycles during development, we undertook a screen to identify regulators of mitotic cycles and endocycles during embryogenesis. We screened 300 EMS-mutagenized 3 "dchromosome lines (Moore et al., 1998) and recovered 26 mutants falling into 5 phenotypic classes reflecting functions in transcriptional regulation and developmental regulation of Sphase. In addition, we identified a class of mutants in which normally diploid cells became polyploid, suggesting functions that distinguish mitotic cycles from endocycles during development. Amongst these, we cloned mutations in pavarotti, encoding a kinesin-like protein, and tumbleweed, encoding a Rho-family GAP. RESULTS A screenfor mutations affecting developmental cell cycle regulation To recover mutations altering developmental cell cycle regulation during embryogenesis, we looked for alterations in the pattern of expression of PCNA, a component of the G1/S transcriptional program. PCNA is expressed in the mitotically proliferating nervous system and endocycling larval gut, allowing examination of both tissues. Previously, Irena Royzman and Allyson Whittaker screened 700 EMS mutagenized 3rd chromosome lines, from a collection of mutagenized lines generated in the laboratory of Ruth Lehmann (Moore et al., 1998), for aberrant PCNA expression in the interest of identifying developmental regulators of G1/S transcription (Moore et al., 1998; Royzman et al., 1997). We were primarily interested in identifying developmental regulators of DNA replication using PCNA expression as a marker of DNA replication and screened an additional 300 lines from the collection. Embryos were collected from heterozygous flies, aged 8-15 hr, and in situ hybridized using a PCNA riboprobe as described previously (Royzman et al., 1997). Heterozygous embryos carried a Ubx-lacZ transgene. Homozygous embryos were detected by absence of lacZ expression, as detected by in situ hybridization with a lacZ riboprobe. We recovered 26 mutants falling into 5 phenotypic classes (Table 1, Fig. 3). In addition, we included three mutants isolated by Irena Royzman and Allyson Whittaker as they fit our phenotypic classes. Class I consisted of 6 mutants that failed to downregulate PCNA mRNA in the anterior and posterior midgut in stage 14 embryos (Table 1, Fig. 3D). Mutants in cyclinE and dup display a block to replication and fail to downregulate the G1/S transcriptional program in the endodomains (Sauer et al., 1995; Whittaker et al., 2000). Class I mutants Table 1. Mutants recovered from a screen for regulators of developmental cell cycle specificity. In situ hybridization with PCNA antisense riboprobe of EMS-mutagenized homozygous mutant embryos identified 30 alleles falling into five phenotypic classes. Class V mutants showed large cells in the CNS. Of these, 3C53, 3C157, Ir8, 2k32 and 32a (marked with v5 displayed large nuclei corresponding are mapped to the 2 nd to large cells. (II) and (III) indicate that alleles and 3 rd chromosomes respectively. (?) indicate that the allele has not been mapped to a chromosome, * indicates mutants belonging to two phenotypic classes. ** were isolated by I. Royzman and A. Whittaker. Additional phenotypic descriptions are given under comments. Italics indicate description of PCNA expression in tissues abbreviated as follows: AM/PM - anterior and posterior midgut, MG - central midgut, HG - hindgut, MT - Malpighian tubules, ENDO - all endodomains (AM/PM, MG, HG and MT), CNS - central nervous system, VNC - ventral nerve cord. Class I Ectopic PCNA expression in endodomains. Class II Small brain and aberrant PCNA expression in endodomains. Class III Reduced PCNA expression in CNS. No PCNA expression in MG. Class IV Reduced PCNA expression. Class V Large cells CNS Allele No. 3C22 (III) 3C37 (III) 3C92 (III) 3C225 (III) 3C240 (III) 3C241 (?) * 3Cll (III) 3C41 (III) 3C137 (III) 3C187 (III) 3C44 (III) 3C83 (III) 3C87 (III) 3C165 (III) * 3C168 (III) 3C249 (III) 3C115 (III) 3C118 (III) 3C148 (III) 3C]74 (?) 3C175 (?) 3C210 (III) * 3C143 (III) 3C23 (III) V3C53 (III) V'3C157 (III) 3C165 (III) * 3C207 (?) 3C210 (III) * 3C241 (?) * VIr8 (III) ** '2k32 (III) ** 1v32a (II) ** Comments AM/PM in stage 14. AM/PM in stage 14. AM/PM in stage 14. Reduced MG. AM/PM in subset of stage 14. Reduced MG. AM/PM in stage 14. No MG. AM/PM in stage 14. Large cells CNS. AM/PM in stage 14. No HG or MT. HG and MT domains small. MG in all stages. No HG or MT. HG and MT domains small. AM/PM in stage 14. AM/PM in stage 14. AM/PM in stage 14. AM/PM in stage 14. Large cells CNS. AM/PM in subset of stage 14. AM/PM in stage 14. AM/PM low ENDO low. CNS low. ENDO low. ENDO low. AM/PM, MG low. Large cells CNS. Large cells VNC. VNC disorganized. AM/PM in stage 14. Large cells CNS. AM/PM, MG low. Large cells CNS. AM/PM in stage 14. Large cells CNS. Figure 3. PCNA expression phenotypes of select mutants recovered from a screen for regulators of developmental cell cycle specificity. Mutant embryos were in situ hybridized with PCNA and lacZ antisense riboprobes. Homozygotes were detected by absence of lacZ expression from an Ubx-lacZ transgene on a balancer chromosome. (A, B) CantonS wildtype (WT) stage 13 and 14 embryos are shown. (A) In stage 13, PCNA expression is seen in the nervous system (*), anterior and posterior midgut (arrowheads), hindgut and Malpighian tubules (arrows) corresponding to DNA replication in these tissues. (B) In stage 14, PCNA expression is evident in a stripe in the central midgut (**) corresponding to 2 nd round DNA replication in this tissue. PCNA expression in the anterior and posterior midgut is downregulated (arrowheads). (C, D) Class I mutant 3C37 stage 13 and 14 embryos are shown. (C) In stage 13, PCNA is expressed appropriately in the anterior and posterior midgut, hindgut and Malpighian tubules. (D) In stage 14, PCNA inappropriately persists in the anterior and posterior midgut (arrowheads). (E, F) Class II mutant 3C11 stage 13 and 14 embryos are shown. Class II mutants display small brains (*) suggestive of proliferative defects. (E) In stage 13, PCNA is expressed in anterior and posterior midgut (arrowheads) but the hindgut and Malpighian tubules are not evident (arrows). (F) In stage 14, PCNA expression persists inappropriately in anterior and posterior central midgut (arrowheads). (G, H) Class III mutant 3C44 stage 13 and embryo with terminal phenotype are shown. (G) In stage 13, 3C44 displays reduced PCNA expression in the nervous system (*) relative to wildtype. (H) In stage 14, homozygotes fail to express PCNA coinciding with the 2 nd round of replication in the central midgut (**). o (j efd Q (with the exception of 3C241, which has not been mapped to a chromosome), are on the 3" chromosome whereas cyclinE and dup are located on the 2 nd chromosome. Although CyclinE and DUP may directly participate in G1/S transcript downregulation, we favor the model that completion of S phase signals this event and that CyclinE and DUP act indirectly by blocking S phase progression. We expect that Class I mutants either block DNA replication or affect components of an active, cell-cycle dependent signaling mechanism for G1/S transcript downregulation. These mutants may affect replication factors. Class II mutants had small brains and failed to downregulate transcripts in the midgut (Table 1, Fig. 3E-F). These mutants affected both the nervous system and endodomains, suggesting conserved function between mitotic cycles and endocycles. 3C41 and 3C187 specifically affected ectoderm-derived tissues - the central nervous system, hindgut and Malpighian tubules. The hindgut and Malpighian tubules are ectoderm derived unlike the midgut, which is mesoderm derived (Skaer, 1993). 3C41 and 3C187 may be ectoderm specific whereas 3C11 and 3C137, which affect both the central nervous system and the midgut, are more likely to affect cell cycle regulators. Class III mutants displayed reduced PCNA expression in the nervous system and a failure to downregulate PCNA expression in the anterior and posterior midgut (Table 1, Fig. 3G-H). Failure to downregulate PCNA in the midgut is reminiscent of cyclinE and dup mutants in which replication is blocked (Sauer et al., 1995; Whittaker et al., 2000). Again, neither cyclinE nor dup are on the 3 r chromosome. All Class III mutants map to the 3 rd chromosome. We expect that Class III mutants block DNA replication. Like Class I mutants, Class III mutants may affect replication factors. Class IV consists of 7 mutants that displayed reduced PCNA expression in the endodomains or in the case of 3C118, in both endodomains and the nervous system (Table 1). This phenotype suggests defects in G1/S transcription. These mutants may encode transcription factors. Class V mutants displayed large cells in the nervous system (Table 1, Fig. 4). 10 mutants displayed this phenotype. Three belonged to other classes besides Class V. These mutants are described further in the following section. Class V mutants have large nuclei in the nervous system and epidermis We were interested in examining how mitotic cycles and endocycles are distinctively regulated in a developmental context. Ten Class V mutants displayed large cells in the nervous system in our primary screen. Since cell size is linked to ploidy (Edgar and Orr-Weaver, 2001), we expected these mutants might enumerate the developmental mechanisms by which mitotic cycles are converted to endocycles in either functional or pathological ways. We conducted a secondary screen on Class V mutants to examine DNA content in the large cells. We stained 8-15 hr embryos from each mutant line with the DNA dye DAPI and confirmed large nuclei in the nervous system of 5 of these mutants (Table 1, Fig. 4). The remaining mutants in this class may have large cells reflective of increased cell size and not increased ploidy. 3C53 and 32a displayed large nuclei throughout the nervous system while Ir8, 3C157 and 2k32 displayed large, diffuse DNA masses in isolated cells in the nervous system (Fig 4). We conducted complementation tests on the Figure 4. Class V mutants display large, apparently polyploid nuclei in normally diploid cells. Class V embryos (stages 12-14) were DAPI stained and examined for large nuclei. Of the ten mutants initially identified as having large cells, five mutants displayed large nuclei in the ventral nerve cord of the central nervous system as shown here. (A) CantonS wildtype control, (B) 3C53, (C) 32a, (D) 2k32, (E) 3C157, and (F) Ir8. Scale bar is 5 ptm. (B, C) 3C53 and 32a showed large nuclei (arrowheads) throughout the nervous system. (D-F) 2k32, 3C157 and Ir8 showed large, diffuse DNA masses (arrowheads) in a subset of nuclei. 3" chromosome mutants, 3C53, Ir8, 3C157 and 2k32 and determined Ir8 and 3C157 to be allelic. Characterizationand mapping of Ir8 and 3C157 Ir8 and 3C157 displayed isolated large and diffuse DNA masses in the vicinity of the ventral nerve cord (Fig. 4E-F). Ir8 displayed a more pronounced phenotype than 3C157 suggesting Ir8 is the stronger allele. To determine if these diffuse DNA masses displayed characteristics of mitosis, we performed tubulin and phosphohistone H3 antibody staining (Fig. 5). Although we were not able to discern mitotic spindles with tubulin antibody staining, we found that the large and diffuse DNA masses were phosphohistone H3 positive (Fig. 5). Phosphohistone H3 localized to irregularly shaped and irregularly condensed DNA masses indicating that in Ir8 and 3C157, phosphohistone H3 does not strictly coincide with condensed DNA as observed in normal mitoses. These observations suggest that Ir8 and 3C157 disrupt functions in chromatin dynamics, perhaps chromosome condensation. The large nuclei phenotype may be due to defects specific to nervous system development or may be a consequence of the timing of the onset of zygotic regulation of the cell cycle. The central nervous system develops via lineage specification of cells generated by asymmetric divisions of neuroblasts. These divisions result in the generation of both neurons and glial cells that provide support functions (Goodman and Doe, 1993). To determine if Ir8 and 3C157 affect specific lineages, we performed ELAV antibody staining on Ir8 and 3C157 embryos. ELAV is a pan-neuronal marker (Robinow and White, 1988). The pattern of ELAV antibody staining did not strictly correspond with Figure 5. Ir8 and 3C157 polyploid nuclei retain aspects of mitosis. (A-I) Large, diffuse DNA masses in 3C157 stage 12 embryos are phosphohistone H3 positive. Arrowheads indicate diffuse, poorly condensed regions that are phosphohistone H3 positive. The first column (A, D, G) shows anti-phosphohistone H3 staining. The second column (B, E, H) shows DAPI staining. The third column (C, F, I) shows merged channels with anti-phosphohistone H3 in red and DAPI in blue. Scale bar is 10 [tm. phospho H3 3C157 3C]57 DNA phospho H3 DNA large nuclei - some large nuclei were ELAV positive while others were not - suggesting polyploidy in neuronal and non-neuronal cells (Fig. 6). We favor the explanation that the large nuclei in Ir8 and 3C157 are due to misregulation of the cell cycle and that the nervous system specificity of the defects are due to perseverance of the maternal contribution. To determine the lethal stage of Ir8/3C157transheterozygotes, we placed Ir8 and 3C157 in trans to a balancer carrying an actin-GFPtransgene. We crossed these strains and collected embryos over a 24 hour period examining 25 larvae for transgene expression. All larvae were GFP positive suggesting that Ir8/3C157transheterozygotes are embryonic lethal or that larvae fail to hatch. We deficiency mapped Ir8 and 3C157 with 70 deficiencies deleting portions of the 3" chromosome but failed to identify a deficiency uncovering the large nuclei phenotype. We undertook meiotic mapping and mapped the large nuclei phenotype to the genetic interval between h and cu. Characterizationof 3C53 and 32a-20 3C53 and 32a-20, a recombinant of 32a, affected cells more or less uniformly throughout the nervous system suggesting a general defect in mitotic cell cycles. These mutants also appeared to have large cells in the epidermis. This phenotype suggested either (1) defects during cycles 14-16 of the epidermis or (2) unrestricted DNA replication in the period following cycle 16 when epidermal cells exit the cell cycle. We eliminated unrestricted DNA replication as a potential mechanism by examining BrdUlabeled stage 12 embryos. Mutations that affect cell cycle exit result in abundant Figure 6. Some large DNA masses in Ir8 homozygous embryos do not stain for ELAV - a neuronal marker. Stage 13 embryos were stained with monoclonal rat anti-ELAV (Developmental Hybridoma Studies Bank) and DAPI. The ventral nerve cord at mid-embryo are shown and the scale bar in panel (A) is 5 lpm. Sibling embryos of genotypes Ir8/CyO or CyOICyO were used as control. (A-C) anti-ELAV and DAPI staining of a sibling control embryo. (D-F) anti-ELAV and DAPI staining of an Ir8 homozygous embryo. The ventral nerve cord as defined by ELAV staining is disorganized in Ir8 (D) but not in a sibling control (A). Large DNA masses are evident at the periphery of the ventral nerve cord (arrow and arrowhead). Arrowheads in panels D, E, F point to a large DNA mass that is seemingly ELAV negative while arrows in panels D, E, F point to a large DNA mass that is seemingly ELAV positive. 59 replication in the dorsal epidermis at this stage (Lane et al., 1996; Sigrist and Lehner, 1997). Both 3C53 and 32a-20 exited the cell cycle appropriately, suggesting that the large nuclei in the epidermis were due to defects during cycles 14-16 (Fig. 7). In order to examine mitoses, we performed tubulin antibody staining on 3C53 and 32a-20 homozygotes. We detected abnormal mitotic spindles associated with polyploid nuclei in the vicinity of the ventral nerve cord of stage 12 embryos (Fig. 8). Spindles in 3C53 homozygotes appeared depleted of astral microtubules and displayed intensely stained clumps of tubulin at spindle poles. In addition, some nuclei lacked spindles but were decorated with tubulin clumps. 32a-20 homozyotes displayed less severe spindle defects than 3C53. Spindles were more intact albeit morphologically abnormal - fat and carrying tubulin clumps. The spindle defects suggested that 3C53 and 32a-20 might affect determinants of spindle morphology. 3C53 and 32a-20 are alleles of pavarottiand tumbleweedlRacGAP50C respectively Next, we deficiency mapped 3C53 and 32a-20. 3C53 was placed in trans to a collection of 70 deficiencies deleting segments of the 3" chromosome. Of these, Df(3L)GN24 and Df(3L)GN50, failed to complement the large nuclei phenotype. These overlapping deficiencies delete the polytene salivary gland cytological intervals 63F47;64C13-15 and 63E1-2;64B17 respectively. We examined the candidate genes falling into this region and given the spindle defects seen in 3C53 homozygotes, identified pavarotti (pav), a kinesin-like protein previously demonstrated to play a role in cytokinesis, as a good candidate for 3C53 (Adams et al., 1998). We obtained an allele of pavarotti,pavB200, and determined that this allele fails to complement both lethality and Figure 7. The dorsal epidermis of 32a and 3C53 homozygous mutant embryos exits the cell cycle successfully. In stage 12 of embryonic development, the dorsal epidermis exits from the cell cycle following the postblastoderm mitotic divisions. Mutants in fzr and dap fail to exit the cell cycle as indicated by robust BrdU-labeling of dorsal epidermal cells (Lane et al., 1996; Sigrist and Lehner, 1997). 32a (B) and 3C53 (D) homozygous mutant embryos and sibling control embryos (A and C) were labeled with BrdU. Stage 12 sibling control embryos (A and C) are not labeled with BrdU in the dorsal epidermis (yellow arrows). BrdU-labeled cells to either side of non-labeled domains are in the peripheral nervous system, which are undergoing mitotic divisions. 32a and 3C53 homozygous embryos (B and D respectively) were identified by the presence of large nuclei in the nervous system and epidermis. Yellow arrows in B and D point to dorsal epidermal domains, which are not BrdU-labeled, indicating successful cell cycle exit in the dorsal epidermis. Figure 8. 3C53 and 32a-20 homozygotes display abnormal mitotic spindles associated with polyploid nuclei in the nervous system. Images in the first column (A, D, G, J, M) are stained with anti-tubulin. Images in the second column (B, E, H, K, N) are stained with DAPI. Images in the third column (C, F, J, L, O) show anti-tubulin in red and DAPI in blue. The scale bar shown in panel A is 5 [tm. (A-C) Spindle in nervous system of CantonS wildtype stage 12 embryo is shown. (D-J) Spindles in nervous system of stage 12 3C53 embryos are shown. (D-F) 3C53 homozygote shows a spindle with depleted astral and interpolar microtubules. (G-J) 3C53 homozygote shows disorganized clumps of microtubules associated with a nucleus. (J-0) Fat and wide spindles in 32a-20 homozygote stage 12 nervous system. CantonS 3C53 32a-20 the large nuclei phenotype in trans to 3C53. Therefore, 3C53 is an allele of pavarottiand 3 3 . henceforth we designate the allele pavCS We meiotically mapped 32a to the genetic interval between the genes pr and cu and recovered a recombinant chromosome, which we designated 32a-20. We tested 50 deficiencies in this region and identified Df(2R)CX1 as the sole deficiency producing the large nuclei phenotype in trans to 32a-20. We identified a candidate interval containing approximately 100 genes and further limited the candidate interval by male recombinational mapping of the mutation (Preston and Engels, 1996; Preston et al., 1996). We were able to map 32a-20 to an interval containing about 10 genes. Among these genes, tumbleweed (tum), formerly known as racGAP50C,a Rho family GTPase required for cytokinesis (Zavortink et al., 2005), was an attractive candidate. We sequenced the coding region of tum and identified a Leu to His substitution in a conserved residue in the GAP catalytic domain box II (Fig. 9). We expect that the LA64H substitution is the critical mutation in our allele, which we designated tumrn32a20 Pav, a kinesin-like protein, and Tum, a Rho family GAP, are conserved proteins with homologs in C. elegans, humans and mice. Pav and Tum, and their orthologs in other organisms, interact directly, co-localize throughout the cell cycle, are functionally interdependent and are required for cytokinesis (Kuriyama et al 2002, Hirose et al. 2001, Mishima et al. 2002, Jantsch-Plunger et al. 2000, Raich et al. 1998, Somma et al. 2002, Adams et al, 1998, Zavortink and Saint, 2005). Both Pav and Tum are required for the formation of the central spindle, a bundled microtubule structure that arises in anaphase and persists through telophase. The central spindle is required for successful cytokinesis in mammalian cells, C. elegans and Drosophila(Straight and Field, 2000). Figure 9. Tum32a 2 0 carries a L464H substitution in a conserved residue in the GAP catalytic domain. Tum is a 625 residue protein that has coiled-coil (blue box) and Cysteine-rich domains (green box). Tum interacts with Pav and Pbl, and binding domains are at the N-terminus (Somers and Saint 2003). Tum has a GAP catalytic domain characteristic of Rho family GAP. tum 3 2a-20 is a new mutant that carries an L464H substitution in box II of the GAP catalytic domain (red box). Catalytic dead transgenic constructs carry small deletions in GAP domain box I. The two other known Tum mutants are truncated due to nonsense mutations. tumDHS is truncated at residue 195 while tumAR 2 is truncated at residue 470 (Jones and Bejsovec 2005). ?,0 Itt cri S Ho C) c6 I HL CTr I I Li Li I To determine if pav3C53 and tum 32 a-20 block cytokinesis, we stained embryos with antibodies directed against the nuclear and cell membranes and a DNA dye. We observed binucleate cells at high frequency in the dorsal epidermis of tumrn32a -20 stage 12 embryos (Fig. 10D-I). In this stage, the dorsal epidermis has just completed the last postblastoderm division and is exiting from the cell cycle. Binucleate cells were not observed in the dorsal epidermis of pav3CS3. We did, however, observe large DNA masses suggestive of polyploidy (Fig. O1N). Cytokinesis defects have been described in pav mutants previously (Adams et al., 1998). Our inability to identify binucleate cells could indicate a defect prior to cytokinesis or an early block to cytokinesis in which multinucleate cells subsequently fuse. It is possible that multinucleate cells are most abundant following the initial cytokinesis defect. We were unable to examine the earliest postblastoderm division affected by pav3CS3 with certainty. Although heterozygotes were positively marked with a balancer carrying Ubx-lacZ, we found that transgene expression could not be detected with confidence until stage 12. We believe that tum 3 2a-20 embryos first exhibit a cytokinesis defect in the dorsal epidermis in cycle 15. This assertion is based on the presence of multipolar spindles in dorsal epidermal cells undergoing cycle 16 (Fig. 11D-F). In addition to multipolar spindles, we observed abnormal central spindles in telophase cells (Fig. 11J-O). We observed a telophase cell with no central spindle (Fig. 11J-L) and a single, poorly defined central spindle (Fig. 11M-O). We did not detect these defects in 48 spindles examined in control embryos. In a quantification of 31 and 48 spindles in tum 32a -20 and heterozygous sibling embryos respectively, we found the two abnormal anaphase/telophase spindles (Fig. 11J-O) occurring at a frequency of 6% in turn32a-20 , whereas 21% of spindles in heterozygous sibling embryos showed central spindles in telophase. However, we examined few late anaphase/telophase spindles. These results, however, are consistent with defects in central spindle assembly preceding a block to cytokinesis in tum"32 a-2 Figure 10. tumrn ""2 2o and pav3 cs3 display defects consistent with disrupted cytokinesis. Stage 12 embryos stained with anti-lamin, anti-phosphoTyrosine, and YOYO-1 DNA dye. Dorsal epidermal cells were imaged. The first column (A, D, G, I, L), shows antilamin staining. The second column (B, E, H, K, M), shows anti-phosphoTyrosine staining. The third column (C, F, I, L, N), shows merged channels with anti-lamin in blue, anti-phosphoTyrosine in red and YOYO-1 in green. The first row (A-C), shows dorsal epidermal cells in yw control embryos. Single nuclei (green) shown in (C) are enveloped by nuclear lamin shown in (A) and phosphoTyrosine shown in (B). (D-I) 32 turn -2 ° embryos have binucleate cells in the dorsal epidermis. Arrowhead in (F) points to the junction between two closely appositioned nuclei where nuclear lamin is localized in (D) but arrowhead in (E) points to the same junction and no phosphoTyrosine is evident. However, phosphoTyrosine in (E), envelopes both nuclei, indicating that this is a binucleate cell. Arrowheads in (G-I) point to a similar junction between two nuclei. Arrow in (I) points to a large DNA mass that may have arisen from nuclear fusion following a failure in cytokinesis. (J-N) pav3C 53 display large DNA masses, arrow in (N), which may result from cytokinesis failure. We also observed small nuclei, arrowhead in (L) suggestive of aneuploidy. yell//ow white ,,,3 2a-20 aV3C53 Figure 11. tum r "" display spindle defects in the dorsal epidermis. All images were taken in the dorsal epidermis of stage 11/12 embryos. anti-tubulin is in red and YOYO-1 DNA dye is in green. (A-C) yw control metaphase spindle. (D-F) tum3 2a -20 multipolar spindle in metaphase. (G-I) yw control telophase cell with a tightly- bundled central spindle evident between separating DNA masses. (J-L) shows an unusual spindle in tum 32a-20 . Distance between nuclei suggest that this cell may be in telophase cell and has failed to assemble a central spindle. (M-O) A central spindle with poor microtubule bundling in turn32a-20 . (A, D, G, J, M) anti-tubulin. (B, E, H, K) YOYO-1 DNA dye. (C, F, I, L) merge. Tubulin yellow white yellow white t'/ ?32a-20 1 DNA Tubulin DNA DISCUSSION The identificationof mutants that affect developmental regulationof the cell cycle In our screen for regulators of cell cycle specificity during development, we identified 30 mutants falling into five phenotypic classes. We were particularly interested in identifying factors that distinguish mitotic cycles from endocycles in this developmental context. Transcriptional regulation is clearly a motif in developmental cell cycle specification. The Notch signaling pathway is known to impinge on the transcription of key regulators during the mitotic to endocycle switch of follicle cells during Drosophila oogenesis. string and dacapo are downregulated while fizzy-related is upregulated (Deng et al., 2001; Edgar et al., 1994; Jones et al., 2000; Meyer et al., 2002; Schaeffer et al., 2004). The E2F transcription factor is known to regulate cyclinE transcription during embryogenesis but regulation is tissue-specific and other transcription factors are likely to play variable roles in different tissues undergoing different types of cell cycle (Royzman et al., 1997; Sauer et al., 1995). Class III and IV mutants displayed reduced GI/S transcripts in the CNS, endodomains or both and may prove useful in identifying additional transcription factors responsive to developmental signaling. Class I and III mutants failed to downregulate PCNA expression in the endodomains. This defect is reminiscent of mutants in cyclinE and dup, which display an early S-phase block (Knoblich et al., 1994; Whittaker et al., 2000). We excluded cyclinE and dup as candidates because these genes are located on the 2 nd chromosome whereas Class I and III mutants (with the exception of 3C241) map to the 3 rd chromosome. Although Cdk2 maps to the third chromosome, hemizygous mutants in Cdk2 are larval lethal and display no embryonic defects, suggesting that Class I and III mutants are not likely mutants in Cdk2 (Lane et al. 2000). Class I and III mutants may affect replication factors based on their phenotypic similarity to mutants in cyclinE and dup. These mutants may be useful for examining G1/S transcript downregulation. cyclinE and dup mutants fail to downregulate G1/S transcripts in the endodomains, suggesting that S-phase progression is required for G1/S transcript downregulation. CyclinE and DUP are both critical for replication initiation - an immediate early block to S-phase - leaving the question as to the timing of transcript downregulation with respect to S-phase open. Class I and III mutants may block S-phase at later points. Unlike Class III mutants, Class I mutants specifically affect the endodomains. Developmentally regulated fzr and cyclinE expression are required for endocycles (Knoblich et al., 1994; Sigrist and Lehner, 1997). In addition, transcription of mitotic cyclins must be turned off (Weiss et al., 1998). Class I mutants may affect developmental regulation of transcriptional events required for endocycles. Alternatively, the CNS may display normal G1/S transcription due to the perdurance of maternal products in this tissue. New mutants that affect mitotic cell cycles in the nervous system We believed that Class IV mutants that showed signs of polyploidy in normally diploid tissues would either enumerate the ways in which the canonical cell cycle is modified to yield endocycles or elucidate the developmental signals that maintain mitotic cell cycles at a time during which endocycles initiate. Two mutants in this class, 3C53 and 32a-20 (formerly 32a), were identified to be alleles of pavarotti, a MKLP-1 family member, and tumbleweed, a Rho family GTPase activating protein. 2k32, 1r8 and 3C157 (of which 1r8 and 3C157 are allelic), displayed isolated large nuclei in the nervous system. The large isolated nuclei seen in 2k32, Ir8 and 3C157 suggested two possibilities: the mutants affect regulation of cell division specific to nervous system development; or the mutants affect mitotic cell cycle regulators and the maternal contribution is sufficient to drive cell division until late embryonic development when only the nervous system is proliferating. Examination of Ir8 and 3C157 indicated that large nuclei occur in both neuronal and non-neuronal cells. This observation indicates a lack of cell type specificity. We observed phosphohistone H3 localization to poorly condensed DNA, suggesting that Ir8 and 3C157 may affect chromatin dynamics. We favor the explanation that Ir8 and 3C157 disrupt mitotic functions and that any potential tissue and cell type specificity is due to the perdurance of maternal products in conjunction with the developmental timing of cell divisions in the nervous system (Salzberg et al., 1994). tum 3 2a20 disrupts cytokinesis and shows central spindle defects We observed multinucleate cells in tum 32a -20 indicating a block to cytokinesis (Fig. 10). Our observations are consistent with prior work indicating that tum is required for cytokinesis (Zavortink et al., 2005). In addition, we detected central spindle defects in tum 3 2 -2 a-20: turn a 0 32 displayed weak central spindles (Fig. 11) and the frequency of central spindles in tum32a-20 was reduced. Similar central spindle defects were observed for tumrn"", an allele that is truncated due to a nonsense mutation at Arg195 and lacking the GAP catalytic domains (Fig. 10) (Zavortink et al., 2005). The phenotypic similarity between tum32a-20 and tumDHr 5 suggests compromised catalytic activity in turn32a- 20. I addition, the location of the substitution mutations in the GAP catalytic domain of tum"32a 20 may portend loss of GAP catalytic activity. Tum catalytic activity appears to be required for cytokinesis. Transgenic expression of Tum catalytically dead mutants carrying small deletions known to abolish catalytic activity, Tum AVE and TurnmAYRL, failed to rescue the central spindle defect of tum"DHS (Zavortink et al., 2005). Unlike the two known loss-of-function alleles, tumrnDHS and turnm2 (Fig. 10), tum 32a-20 is a full-length protein and unlike the catalytically dead transgenic rescue constructs, TurnmIE and TumAYRL (Fig. 10), we expect that tum 32 a-20 retains physiological expression patterns. The fact that Tum32 -20 is a full-length protein is important because Tum affects Pav protein stability (Zavortink et al., 2005). Tum 32~ 02 is more likely than TumDH 15 and TumAr 2 to retain native structure. In addition, the deletions in TumDH 15 and TumAR2 may remove as yet undefined regulatory domains or disrupt protein structure. tum3 2a-2 0 is potentially useful for dissecting the different roles of Tum - stabilization of Pav and catalytic activity. Zavortink and colleagues report that only the Pav interaction domain and not GAP catalytic activity is required for Pav stabilization (Zavortink et al., 2005). However, they stabilized Pav levels by overexpressing the catalytically dead constructs, TurnmIE and TurnAYRL, and the effects on Pav stability may be indirect. MATERIALS AND METHODS Genetic screen 2 nd chromosome mutants were isolated by Irena Royzman and Allyson Whittaker (Royzman et al., 1997). 3" chromosome mutants were provided by R. Lehmann (Moore et al., 1998). The genetic screen was carried out as described previously (Royzman et al., 1997). Cytological analysis and microscopy In situ hybridization was carried out with digoxigenin-labeled RNA probes exactly as described previously (Royzman et al., 1997). Antibody stainings were performed as described previously (Dej et al., 2004). YL1/2 and YOL1/34 (Sera Lab) anti-tubulin antibodies were used. Anti-phosphohistone H3 (Upstate Biotechnology) was used at 1:250. Anti-DmOLamin (Gruenbaum et al., 1988) was used at 1:200 and antiphosphoTyrosine (Zymed) was used at 1:100 with methanol fixation. DNA stains were performed with DAPI at 10 [tg/mL or YOYO-1 at 1:2000 (Molecular Probes). AntiDm0Lamin was obtained from Paul Fischer (SUNY at Stony Brook) and all secondary antibodies were from Jackson Immunoresearch. Images of multinucleate cells and epidermal spindle defects were collected using a Zeiss Axiovert 100 M Meta confocal microscope with LSM510 software. A Zeiss Axiophot microscope with Plan-Neofluar 20x, Plan-NeoFluar 25x Inn Korr, or PlanNeoFluar 40x oil objectives were used to collect images with a SPOT RT CCD camera and software. Mapping and Sequencing Chromosome II and III deficiency kits and pavB 20 0 (Adams et al., 1998) were from the Bloomington Stock Center. We performed male recombinational mapping (Chen et al., 1998) using EP2383, EP2423,EP2041, EP2407, EP2054 and EP993. Sequencing of tum 32a-20 was performed as described previously (Dej et al., 2004). DNA from 10 embryos was purified and exons were sequenced on both strands and compared to the Drosophilagenome sequence Release 2. REFERENCES Adams, R.R., A.A. Tavares, A. Salzberg, H.J. Bellen, and D.M. Glover. 1998. pavarotti encodes a kinesin-like protein required to organize the central spindle and contractile ring for cytokinesis. Genes Dev. 12:1483-94. Asano, M., and R.P. Wharton. 1999. E2F mediates developmental and cell cycle regulation of ORC1 in Drosophila. 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Strumpf, L. Tsai, and H.J. Bellen. 1994. Mutations affecting the pattern of the PNS in Drosophila reveal novel aspects of neuronal development. Neuron. 13:269-87. Sauer, K., J.A. Knoblich, H. Richardson, and C.F. Lehner. 1995. Distinct modes of cyclin E/cdc2c kinase regulation and S-phase control in mitotic and endoreduplication cycles of Drosophila embryogenesis. Genes Dev. 9:1327-39. Schaeffer, V., C. Althauser, H.R. Shcherbata, W.M. Deng, and H. Ruohola-Baker. 2004. Notch-dependent Fizzy-related/Hecl/Cdhl expression is required for the mitoticto-endocycle transition in Drosophila follicle cells. Curr Biol. 14:630-6. Shcherbata, H.R., C. Althauser, S.D. Findley, and H. Ruohola-Baker. 2004. The mitoticto-endocycle switch in Drosophila follicle cells is executed by Notch-dependent regulation of G1/S, G2/M and M/G1 cell-cycle transitions. Development. 131:3169-81. Sigrist, S.J., and C.F. Lehner. 1997. Drosophila fizzy-related down-regulates mitotic cyclins and is required for cell proliferation arrest and entry into endocycles. Cell. 90:671-81. Skaer, H. 1993. The Alimentary Canal. In The Development of Drosophila melanogaster.Vol. 2. M. Bate and A. Martinez Arias, editors. Cold Spring Harbor Laboratory Press, Plainview, New York. 941-1012. Smith, A.V., and T.L. Orr-Weaver. 1991. The regulation of the cell cycle during Drosophila embryogenesis: the transition to polyteny. Development. 112:9971008. Straight, A.F., and C.M. Field. 2000. Microtubules, membranes and cytokinesis. Curr Biol. 10:R760-70. Weiss, A., A. Herzig, H. Jacobs, and C.F. Lehner. 1998. Continuous Cyclin E expression inhibits progression through endoreduplication cycles in Drosophila. Curr Biol. 8:239-42. Whittaker, A.J., I. Royzman, and T.L. Orr-Weaver. 2000. Drosophila double parked: a conserved, essential replication protein that colocalizes with the origin recognition complex and links DNA replication with mitosis and the down-regulation of S phase transcripts. Genes Dev. 14:1765-76. Zavortink, M., N. Contreras, T. Addy, A. Bejsovec, and R. Saint. 2005. Tum/RacGAP50C provides a critical link between anaphase microtubules and the assembly of the contractile ring in Drosophila melanogaster. J Cell Sci. 118:538192. CHAPTER THREE The characterization of new cyclinE mutants that increase replication fork progression during gene amplification Eugenia A. Park, David M.MacAlpine and Terry L. Orr-Weaver Whitehead Institute and Dept. of Biology, Massachusetts Institute of Technology, Cambridge, MA 02142 Eugenia A. Park performed all of the immunolocalization, microscopy, flow cytometry and quantitative real-time PCR for this work. For Drosophila2L tiling array experiments, Eugenia Park prepared probes and hybridized arrays and assisted in scanning arrays. David MacAlpine scanned arrays and analyzed data. SUMMARY We have identified the first cyclinE mutants to display aberrant gene amplification during Drosophilaoogenesis. cyclinEuz36/cyclinEPzs and cyclinE'f6 /cyclinEP28 are the first mutants to display increased replication fork progression in gene amplification, demonstrating an absence of CyclinE independent Replication Fork Barriers (RFBs) during this process. The rate of oogenesis is normal in cyclinEl'f6 /cyclinEP 8 ovaries, suggesting that increased replication fork progression is due to increased replication fork speed. These results implicate CyclinE in the regulation of replication fork speed. Double Parked (DUP) and the Mcm2-7 complex showed localization to the double bar cytological feature, corresponding to bi-directional replication forks, leaving open the possibility that CyclinE/Cdk2 regulation of DUP and Mcm2-7 may affect replication fork progression. INTRODUCTION The regulation of replication fork progression is important for varied biological processes such as DNA damage checkpoint responses, gene expression and replication termination (Rothstein et al., 2000). Replication fork progression is regulated, in part, by factors found at the replication fork. PCNA, the DNA polymerase processivity factor, is a key component of the active replication fork. It is known to interact with two of three polymerases that localize to the replication fork, DNApol8 and DNApols (Garg and Burgers, 2005). Additionally, biochemical approaches to determining components at stalled eukaryotic replication forks have identified DNApola-primase, Mcm2-7, Cdc45, Mcml0, GINS, Mrcl and Tofl proteins among others at stalled replication forks (Calzada et al., 2005; Pacek et al., 2006). DNA polct is involved in lagging strand synthesis during replication elongation. The Mcm2-7 complex is the putative replicative helicase that travels with replication forks (Aparicio et al., 1997; Labib et al., 2000). Cdc45, Mcml 0 and GINS are three other replication factors (Aparicio et al., 1999; Gambus et al., 2006; Merchant et al., 1997; Moyer et al., 2006; Seki et al., 2006; Takayama et al., 2003; Tercero et al., 2000; Wohlschlegel et al., 2002). Mrcl and Tofl act as sensors and effectors in replication checkpoint pathways. They stabilize stalled forks during checkpoint responses and regulate replication fork progression during normal DNA replication (Szyjka et al., 2005; Tourriere et al., 2005). Replicative helicases generally promote replication fork progression. In E. coli, a protein inhibitor of the replicative helicase reduces replication fork speed (Skarstad and Wold, 1995). Replication fork progression at normal speeds through S. cerevisiae telomeric and subtelomeric sequences requires the Rrm3p helicase (Ivessa et al., 2002). In addition, replication fork pausing mechanisms often target the helicase. During prokaryotic replication termination, the trans-acting factors Tus in E. coli and RTP in B. subtilis bind to and inhibit replicative helicase (Bussiere and Bastia, 1999). Replication fork progression may be regulated at the level of competing helicases. At the S. cerevisiae rDNA locus, the DNA helicase Piflp maintains replication fork pausing while Rrm3p promotes replication fork progression (Ivessa et al., 2000). Helicases are also regulated by phosphorylation. The Mcm2-7, the putative eukaryotic replicative helicase, is a multisubunit complex that is phosphorylated at multiple sites on Mcm2 by S-phase kinases Cdc7 and Cdk2 and ATR kinases (Montagnoli et al., 2006). The Cdc7 phosphorylation sites negatively regulate chromatin association of Mcm2, and phosphorylations at these sites are stimulated by Cdk2 phosphorylation, suggesting that sequential phosphorylation by multiple kinases modulates Mcm2-7 activity (Montagnoli et al., 2006). CyclinB/Cdkl phosphorylation of Mcm4 restricts chromatin association (Hendrickson et al., 1996). CyclinA/Cdk2 phosphorylation has been shown to restrict Mcm4,6,7 subcomplex helicase activity (Ishimi et al., 2000). In addition, p27Kipl, the CyclinE/Cdk2 inhibitor, binds to Mcm7 and inhibits initiation of DNA replication (Nallamshetty et al., 2005). Replication fork progression is also regulated by factors that do not localize to replication forks. Replication fork barriers (RFBs) have been identified in prokaryotes, yeast and metazoans (Rothstein et al., 2000). RFBs in prokaryotes and yeast consist of DNA sequence elements that bind trans-acting factors to impose a block to replication fork progression. Replication terminator sequences in E. coli and B. subtilis, Ter, bind Tus and RTP respectively. In prokaryotic replication termination, RFBs colocalize replication forks with replication termination machinery such as topoisomerase, which is important for the decatenation of circular chromosomes (Zechiedrich and Cozzarelli, 1995). In S. pombe, the Rtsl sequence element binds the Swil/Swi3 complex, Tofl and Mrcl homologs, and acts as a polar RFB to ensure the directional replication of the mat] locus (Lee et al., 2004). This directional replication induces strand-specific mating type switching by inducing an imprint in the next round of replication (Dalgaard and Klar 2000, 2006). Swil/Swi3 also binds at the imprint site and pauses replication forks (Dalgaard and Klar, 2000; Lee et al., 2004). Like Tofl and Mrcl, Swi 1 and Swi3 are required for stabilization of stalled forks and activate replication checkpoint signaling (Noguchi et al., 2004). Not all barriers to replication fork movement are protein/DNA units. Homopurine/homopyrimidine sequences have been shown to pause replication forks thereby slowing replication fork progression (Rao, 1994; Rao, 1996; Rao et al., 1988). The regulation of replication fork progression may be important for gene expression. RFBs are found in the rDNA loci of S. cerevisiae, S. pombe, mouse, Xenopus and humans (Rothstein et al., 2000). In S. cerevisiae, S. pombe, mouse and Xenopus, polar intergenic RFBs block replication fork progression opposing transcription (Brewer and Fangman, 1988; Brewer et al., 1992; Gerber et al., 1997; Hernandez et al., 1993; Kobayashi et al., 1992; Linskens and Huberman, 1988; Lopez-estrano et al., 1998; Lucchini and Sogo, 1994; Sanchez et al., 1998; Wiesendanger et al., 1994). In E. coli, head-on transcription severely inhibits replication fork progression while co-directional transcription does not, revealing the importance of coordinated transcription and replication (Mirkin and Mirkin, 2005). The Tetrahymena rDNA locus shows a co- directional bias in replication fork pausing, suggesting that even co-directional transcription and replication may be refractory to replication fork progression (MacAlpine et al., 1997). This may be due to nucleosomal rearrangements required for transcription. Follicle cell gene amplification during Drosophilaoogenesis is a useful system for studying DNA replication. During gene amplification, replication occurs from defined origins of replication utilizing conserved cell cycle machinery. The visualization of replication factor localization and DNA synthesis by BrdU incorporation is easy to perform. In addition, replication initiation events occur from well-defined, isolated origins of replication, allowing for the examination of replication elongation by cytological methods. During gene amplification, multiple, tandem replication forks move outwards from origins of replication at five genomic loci known as the DrosophilaAmplicons of Follicle Cells - DAFC-7F,DAFC-30B, DAFC-34B, DAFC-62D and DAFC-66D (J. Kim and T. Orr-Weaver, unpublished results), (Claycomb et al., 2004; Spradling, 1981). These replication forks amplify genomic regions containing eggshell constituents to high copy numbers (Claycomb et al., 2002; Delidakis and Kafatos, 1989; Spradling, 1981) and gene amplification is required for eggshell formation. The study of female-sterile mutants affecting gene amplification and eggshell formationindicate that cell cycle machinery is conserved during gene amplification. Females mutant for mcm6, dup/Cdtl, orc2, and chiffon, which shows homology to dbf4, a specificity factor for the S-phase kinase Cdc7, produce eggs with thin eggshells due to reduced gene amplification (Landis et al., 1997; Landis and Tower, 1999; Schwed et al., 2002; Whittaker et al., 2000). In addition, localization studies show that replication factors Orcl, Orc2, Orc5, DUP/Cdtl, Cdc45, the MCM complex and PCNA localize to amplicons (Asano and Wharton, 1999; Austin et al., 1999; Claycomb et al., 2002; Loebel et al., 2000; Royzman et al., 1999; Whittaker et al., 2000). The examination of female-sterile mutants, have identified genes required for replication initiation, amongst these are components of the Pre-Replication Complex and a putative co-factor for an S-phase kinase, chiffon. In addition, the cis-acting elements which regulate the location of replication initation events, by binding the ORC Complex, have been identified (Austin et al., 1999). Although the cis-acting elements, replication factors and regulatory kinases regulating replication initiation during gene amplification are characterized, little is known about the factors regulating replication elongation during gene amplification. Cis-acting elements regulating replication elongation have not been defined but such elements may be important for coordinating replication and transcription during gene amplification. No genetic studies unmasking replication factors involved in elongation have been forthcoming, possibly due to pleiotrophic effects on replication initiation. We have characterized the first mutants known to increase replication fork progression during gene amplification. In addition, these are the first mutants in cyclinE 28 to display gene amplification defects. cyclinElf36/cyc1inEPzs and cyclinElf36/cycinEP follicle cells display increased replication fork progression, demonstrating the lack of stringent RFBs and implicating CyclinE in the control of replication fork progression. RESULTS A new mutation in cyclinE that displayspreviously undescribeddefects in gene amplification cyclinE'116 is an EMS allele that was isolated from a screen for regulators of the G 1/S transcriptional program (Royzman et al., 1999; Royzman et al., 1997; Whittaker et al., 2000). This allele is lethal in trans to Df(3L)TE35DI that deletes cyclinE and 1 3 6 is cyclinEPzS, a P-element allele. In trans to cyclinEP z,' a P-element allele, cyclinEf sterile. In trans to cyclinEP28, a hypomorphic EMS allele, cyclinE*36 is semi-sterile. 6 /cyclinEPz cyclinEfP 8 and cyclinE' 36a/cyclinEP28 mutant follicle cells display cytological defects consistent with increased replication fork progression. The double bar structure is seen in follicle cells of BrdU-labeled stage 12 and 13 egg chambers and corresponds to gene amplification at DAFC-66D (Calvi and Spradling, 2001; Claycomb et al., 2002). There is strong evidence that the double bar structure (Fig. 1B) corresponds to tandem replication forks moving bi-directionally away from a central origin of replication (Claycomb et al., 2002). The gap distance between bars reflects the distance traveled by replication forks after termination of replication initiation events in stage 11 but prior to the start of BrdU-labeling (Claycomb et al., 2002). cyclinEPf36cyclinEPz8 and 13 6/cyclinEP28 cyclinE• mutant follicle cells had double bars in stage 13 egg chambers that appeared to have increased gap distances relative to a CantonS wildtype control (Fig. lA). We confirmed that the double bars corresponded to gene amplification at DAFC66D in cyclinEf36 /cyclinEZ8 mutant follicle cells by performing BrdU/FISH co-labeling using a DAFC-66D specific FISH probe (Fig. 1C). Figure 1. Double bars corresponding to replication at DAFC-66D are distantly P spaced in cyclinEf'/cyclinE" mutant follicle cells. (A) cyclinEf36/cyclinEPZ8 follicle cells have BrdU-labeled double bars with larger gap distances than those seen in CantonSfollicle cells. Stacked confocal images of BrdUlabeled double bars in stage 13 egg chambers were deconvolved (left column) and rendered into 3D projections (right column). The CantonSfollicle cell double bar has a gap distance of 300 nm while the cyclinElf 6/cyclinEPZ8 follicle cell double bar has a gap distance of 700 nm. (B) The double bar corresponds to bi-directional replication occurring at DAFC-66D. Multiple, tandem replication forks incorporate BrdU (red shade) as they move outwards. The gap distance (bracketed line) is the distance between the BrdU-labeled bars. (C) The double bars seen in cyclinEf3l6/cyclinEP 8 (red) correspond to DAFC-66D as visualized by FISH using a DAFC-66D specific probe (green). The scale bar is 2 Rm. I Iil ~----~c ~---21 ~L---~311 ~s~-L, c~s~ To confirm that gap distances were increased in cyclinEl3 6/cyclinEPz 8 , we deconvolved stacked confocal images and rendered 3D projections to accurately measure the distance between bars (Fig. lA). We measured gap distances in 10 double bars each for cyclinE13 6/cyclinEPz 8 and an OregonR wildtype control (Table 1). The average gap distance for OregonR follicle cells was 0.38 t 0.06 Rm. For cyclinEJ'6/cyclinEPz 8 follicle cells, the average gap distance was 0.54 _ 0.13 tm. OregonR follicle cells showed gap distances ranging from 0.30 to 0.50 [m while cyclinEP36/cyclinEP 8 mutant follicle cells showed gap distances ranging from 0.30 to 0.80 [tm. This phenotype is mosaic. Within one egg chamber, we found one double bar with a gap distance of 0.30 and another with a gap distance of 0.70. We conclude that the gap distances between bars is increased in cyclinE'f36/cyclinEPz8 mutant follicle cells relative to OregonR follicle cells. This phenotype is consistent with increased replication fork progression. 8 and cyclinE'13 6/cyclinEPz 8 have expanded amplified regions at cyclinE'-*6/cyclinEPz DAFC-66D, DAFC-30B and DAFC-34B We expected that increased replication fork progression would coincide with an expanded amplified region at DAFC-66D. We performed quantitative real-time PCR on genomic DNA purified from cyclinEP36/cyclinEPZ8 stage 13 egg chambers and determined fold amplification at DAFC-66D in 10 kb intervals (Fig. 2A). Our results showed that the 6/cyclinEPzS follicle cells extends 100 kb to amplified region at DAFC-66D in cyclinEf3 either side of the amplified maximum (Fig. 2A), whereas in OregonR wildtype control follicle cells, the amplified region extends 50 kb to either side of the amplified maximum (Fig. 2A). For cyclinE'36 cyclinEP28 follicle cells, we observed that the amplified region at Table 1. GAP distances in cyclinE''I6cyclinEra and CantonS follicle cell double bars. Gap distances were measured for 10 BrdU-labeled double bars in CantonS and cyclinElf36/cyclinEP8 follicle cells. Distances were measured from 3D projections of deconvolved confocal images and are given in pm. The mean gap distance of ten double bars is given with standard deviation as error. Double bar 1 2 3 4 5 6 7 8 9 10 Mean CantonS 0.3 0.5 0.4 0.4 0.4 0.4 0.4 0.3 0.3 0.4 0.38 t 0.06 8 cyclinElf36/cyclinEzP 0.8 0.6 0.6 0.3 0.7 0.6 0.3 0.5 0.3 0.7 0.54 ± 0.13 Figure 2. The DAFC-66D amplified region is increased two-fold in cyclinEl6 I/cyclinEP'Z and cyclinE'6/cyclinEP2 8 mutant follicle cells. Quantitative real-time PCR was used to determine fold amplification at DAFC-66D. Fold amplification (Y-axis) was determined at 10 kb intervals surrounding the amplified maximum at 0 kb (X-axis). (A) Amplification profiles were determined for cyclinE'P6 /cyclinEPZ8 (blue and yellow) and OregonR (pink) stage 13 egg chambers. Two independent DNA preps (trial 1 and trial 2) were used for cyclinEl36/cyclinEPz8 (blue and 6 /cyclinEPz 8 yellow). (B) Partial amplification profiles were determined for cyclinE /P (blue), cyclinE'f 36/cyclinEP2 8 (orange) and OregonR (pink) stage 13 egg chambers. In both (A) and (B), the amplified region is doubled in cyclinEln 6 /cyclinEPz 8 and cyclinE'f6 /cyclinEP28 stage 13 egg chambers relative to the wildtype control. Errors are the standard deviation of the sample. A 70 60 50 40 -.0 PC Is wo 10 0 -80 -100 D -40 OregontR -- cyclinE, I 6/cyclinEPz -C1 -60 -20 0 20 Distance (kb) 8 trialI 40 60 80 100 cyclinE/3 6/CyClinEPZ 8 trial2 rr\ 3u 45 40 a 35 o 30 S25 20 4 15 10 5 0 '0 10 -i OregoniR 20 -.- 30 cyclin 40 50 60O Distance (kb) 6 /cyclnEPz 8 70 80 -- cyclinE 69/cyclinE 90 28 100 DAFC-66D extends 100 kb to the right of the amplified maximum (Fig. 2B). We also observed that while the amplified maximum in cyclinE'l6/cyclinEPz8 and P 2 8 follicle cells is comparable to OregonR follicle cells (25-30 fold cyclinE'9 6/cyclinE amplified), suggesting that replication initiation events are intact in these cyclinE mutants. The slope of drop-off in flanking regions may be gentler in cyclinE'f36 /cyclinEPz 8 2 8 follicle cells (Fig. 2B), indicating that replication forks are and cyclinE'~6/cyclinEP farther apart and that the rate of replication initiation events is reduced in cyclinE'f36/cyclinEPz8 and cyclinE'f36/cyclinEP28 follicle cells. To examine additional amplicons, we performed genomic DNA microarray experiments using the Drosophila 2L tiling array with sequences from Chromosome 2L. In addition, this array carried a 250 kb genomic segment surrounding DAFC-66D on Chromosome 3. DAFC-30B and DAFC34B are located on Chromosome 2L. We hybridized the Drosophila2L tiling array (MacAlpine et al., 2004) with probe made from flow-sorted 16C follicle cell nuclei. 2C embryonic DNA was used to synthesize a reference probe. Array experiments were performed in triplicate and dyes swapped in one experiment. Results were Loess normalized and plotted as the log base 2 ratio of enrichment on the Y-axis and chromosomal position of the array feature on the X-axis (Fig. 3A). We examined array features corresponding to DAFC-30B, DAFC-34B and DAFC66D. Plots were smoothened by taking the moving average of 15 continguous features and overlaid (Fig. 3B). Our results indicate that amplified regions are broader at DAFC6/cyclinEPz 30B and DAFC-34B in cyclinEfP 8 follicle cells relative to OregonR (Fig. 3A and B). We found that in OregonR follicle cells DAFC-30B was amplified over a 160 kb region (Fig. 3B). In cyclinE' 6/cyclinEPz8 mutant follicle cells, DAFC-30B was amplified Figure 3. Amplified regions at DAFC-30B and DAFC-34B are increased two-fold in 6 cyclinE"P cyclinE'J3 and cyclinE'P6 IcyclinEP 28 mutant follicle cells. Drosophila2L tiled arrays were hybridized with labeled follicle cell 16C DNA and labeled embryonic 2C DNA as reference. (A) Scatter plot for the length of chromosome 2L. X-axis is chromosome position and Y-axis is the log 2 ratio of enrichment. Peaks corresponding to gene amplification at DAFC-30B and DAFC-34B are broader in cyclinEJP6/cyclinEP 8 follicle cells than in OregonR follicle cells. Peaks are significant to P.0.01. (B) High resolution plots for OregonR (solid line) and cyclinEf36/cyclinEPz 8 (dashed line) at DAFC-30B, DAFC-34B and DAFC-66D, were smoothened by finding the moving average of 15 contiguous data points. 100 R ~ · r= ·N h;l O 01 · 8 9 · · 17 Z 00 vr vr ~ci 0j U, I$) rcl 0 -e . U, 0 0c 9'E O'W 'Z 0Z 5'1 0"1 e.* 0; 0 o~ c :c It . . . I . . I - - I', Il,. •1 - m I i I 0 V luaUqaijtua PloJ 2o3 OOp Q 0' OZ LiT 5 Julumq3)laU21 u7u' 07u3 pIlo4 *p1 over a 300 kb region (Fig. 3B). In OregonR, DAFC-34B was amplified over a 100 kb region (Fig. 3B). In cyclinEf-6/cyclinEPzs, DAFC-34B was amplified over a 200 kb region (Fig. 3B). The amplified regions for DAFC-30B and DAFC-34B were doubled in cyclinEf36/cyclinEPz8 relative to the wildtype control. This is consistent with the doubling in amplified region seen for DAFC-66D as assayed by quantitative real-time PCR (Fig. 2). The Drosophila2L tiling array included a 250 kb region surrounding DAFC-66D and for OregonR, the amplified region was about 120 kb (Fig. 3B). We were not able to detect the non-amplified endpoints for cyclinEf3 6/cyclinEP8 but the expanded amplified region appears to be greater than 250 kb (Fig. 3B). The increased amplification levels seen in regions flanking the maximum are consistent with an expanded amplified region relative to OregonR (Fig. 3B). Our microarray experiments indicated that in OregonR follicle cells, DAFC-30B is amplified over a 160 kb region and that DAFC-66D is amplified over a 120 kb region (Fig. 3B). This differs from the approximate 100 kb amplified regions for DAFC-30B and DAFC-66D detected by quantitative real time PCR (Claycomb et al., 2004; Claycomb et al., 2002). The expanded amplified regions that we observed for DAFC-30B and DAFC66D suggest that microarrays are more sensitive for detecting lower copy number DNA. Alternatively, the smoothing algorithm used in the high resolution plots (Fig. 3B) may affect the boundaries of the amplified regions. Maximum amplification levels at DAFC66D determined by the tiled microarray differed significantly from values obtained by quantitative real-time PCR. As assayed by tiled microarray, DAFC-66D is amplified 8fold in both cyclinE'f6/cyclinEPz8 and OregonR follicle cells (Fig. 3B). whereas quantitative real-time PCR indicates about 30-fold amplification in both of these 102 populations (Fig. 2B). These differing values may reflect the limitations of the tiled microarray for quantifying high copy number DNA. Given the results from quantitative real-time PCR and 2L tiling array experiments, we conclude that amplified regions for DAFC-66D, DAFC-30B and DAFC-34B are expanded in cyclinEn36/cyclinEPZ8 and cyclinE'36/cyclinEP28 mutant follicle cells. These results are consistent with increased replication fork progression. Increased replicationfork progression is not due to prior cell cycle defects. Follicle cells undergo developmentally regulated cell cycles during egg chamber development. During stages 1-6, follicle cells proliferate mitotically. In stages 7-9, follicle cells undergo endocycles. In stage 10A, follicle cells exit endocycles and in stage 10B, follicle cells initiate synchronous gene amplification. Perturbations to these prior cell cycle events could explain the increased replication fork progression that we 8 observed in cyclinEf3 6/IcyclinEPz and cyclinE~f36 /cyclinEP28 mutant follicle cells. Premature initiation of gene amplification would give replication forks more time to travel. To determine if follicle cell endocycles were perturbed in cyclinE36/IcyclinEPZ8 females, we performed flow cytometry on DAPI-stained follicle cell nuclei isolated from whole ovaries. Normally, follicle cells undergo three rounds of DNA replication generating a ploidy of 16C. A final endocycle generating 32C ploidy is presumed to occur in a subset of cells, possibly the dorsal anterior cells (Lilly and Spradling, 1996). Follicle cell nuclei isolated from whole ovaries and stained with DAPI generate a flow cytometry profile with five peaks corresponding to ploidies of 2C, 4C, 8C, 16C and 32C 103 (Fig. 4A). cyclinEf36 /cyclinEPz 8 mutant follicle cells undergo three endocycles generating 4C, 8C and 16C peaks, but may fail to undergo a complete fourth endocycle to generate a 32C peak (Fig. 4A). Alternatively, a 32C peak may be obscured in cyclinElf36/cyclinEPz8 follicle cells (Fig. 4A). In OregonR, most follicle cells are 16C, as evidenced by the prominent 16C peak relative to the 2C, 4C and 8C peaks (Fig. 4A). In cyclinE-f 6/cyclinEPz8 , a greater proportion of follicle cells are 2C, 4C and 8C, as indicated by the greater size of these peaks relative to the 16C peak (Fig. 4A). Also in cyclinEf36/cyclinEPz8 , a larger fraction of follicle cells have intermediate ploidies indicative of a larger fraction of cells undergoing S-phase (Fig. 4A). This is evident from the enlarged areas between 4C and 8C, 8C and 16C peaks and also between the 16C peak and a possibly obscured 32C peak (Fig. 4A). We conclude that endocycles are delayed in cyclinElf 6/cyclinEPz 8 follicle cells, possibly due to prolonged S-phases. 6/cyclinEPZ8 follicle cells replicated genomic DNA to the To determine if cyclinEJn same extent as OregonR follicle cells, we calculated DNA indices for cyclinEf36/cyclinEPz8 and OregonR follicle cell nuclei analyzed by flow cytometry (Table 2). The DNA index is a ratio of the mean fluorescence of a population of cells stained with a stoichiometrically binding DNA dye to that of a reference population stained in the same tube. The DNA index normalizes for sample-to-sample differences in staining. We determined DNA indices for 4C, 8C and 16C peaks (and also the 32C peak in OregonR). 6/cyclinEPz 8 follicle cell nuclei. in reference to the 2C peaks for OregonR and cyclinEfP The DNA indices calculated for cyclinEf36/cyclinEPz8 follicle cell nuclei were not significantly different from those calculated for OregonR follicle cell nuclei (Table 2). 104 Figure 4. The expanded amplified region at DAFC-66D is not due earlier cell cycle defects. (A) Follicle cell endocyles are delayed and have prolonged S-phases in cyclinE'f36/cyclinEPz8 females. Follicle cell nuclei were isolated from OregonR and cyclinE'f36 /cyclinEPz 8 ovaries, stained with DAPI and their ploidies determined by flow cytometry. Fluorescence intensity is given on X-axis on a logarithmic scale. Y-axis indicates cell count. In OregonR, 2C, 4C, 8C, 16C and 32C ploidies are evident in five peaks. Note that the majority of cells have a ploidy of 16C as evidenced by the prominence of this peak. In cyclinEf36 /cyclinEPZ8 , a greater proportion of cells are 2C, 4C, and 8C as evidenced by the prominence of these peaks relative to the 16C peak. The 32C peak may be obscured by S-phase nuclei. S-phase cells (the population between peaks) are enriched. (B) Confocal images running the depth of the nucleus were collected and stacked to produce 2D images used to quantify BrdU-foci in StlOB. X-axis is the number of BrdU foci/nucleus. (gen) indicates genomic replication. Y-axis is the percentage of cells falling into the categories given on the X-axis. The distributions of follicle cells for cyclinE'136/cyclinEPZ 8 (magenta) and CantonS (teal) are indistinguishable (p=0.46), suggesting that synchronous gene amplification initiates properly in cyclinEP6/cyclinEPz 8 follicle cells. (C) Quantitative real-time PCR of stage 10B (blue), 11 (pink), and 13 (yellow) cyclinEf36/cyclinEPz 8 follicle cells in a region flanking the DAFC-66D maximum indicates that replication forks have not progressed beyond 40 kb in stage 10B and 11 egg chambers (arrowhead). Thus, replication forks travel 60 kb between stages 11 and 13 (*). X-axis is distance from amplification maximum in kb. Y-axis is fold amplification. 105 JS S uo!qu;U!Idunm PIOa Table 2. DNA indices for OregonR and cyclinE'f36cyclinEP' follicle cell nuclei. DNA indices were tabulated from three independent experiments. Purified follicle cell nuclei were DAPI-stained and analyzed by flow cytometry to determine ploidies (Fig. 2A). Mean absorbance/fluorescence was determined for 2C, 4C, 8C, 16C and 32C peaks. The DNA index was calculated by finding the ratio of mean fluorescence of 4C, 8C, 16C and 32C peaks to the mean absorbance/fluorescence of the 2C peak (4C/2C, 8C/2C, 16C/2C, 32C/2C). Each DNA index (4C/2C, 8C/2C, 16C/2C, 32C/2C) was determined in three independent experiments. Mean DNA index and standard deviation as error from three independent determinations of DNA index is given. The 32C/2C DNA index was not determined (ND) for cyclinElf36 /cyclinEPz8 due to the absence of a clear 32C peak (Fig. 3A). 107 4C/2C OregonR 1.71 ± 0.03 cyclinEf3 6 /cyclinEPZ8 1.81 ± 0.02 8C/2C 16C/2C 2.87 ± 0.11 5.08 ± 0.13 2.96 ± 0.10 5.10 ±_0.12 32C/2C 8.67 ± 0.66 ND We conclude that cyclinE"6/cyclinEPs8follicle cells replicate DNA fully during the endocycles. To determine if cyclinElf 36/cyclinEPz8 follicle cells exit endocycles with the appropriate developmental timing, BrdU-labeled nuclei were quantified in stage 10A egg chambers by which time endocycles normally are complete and follicle cell nuclei do not display nuclear BrdU-labeling (Calvi et al., 1998). In cyclinElf36/cyclinEPz8 , 2.8% of 531 follicle cell nuclei in nine egg chambers displayed nuclear BrdU-labeling whereas in OregonR, 2.7'% of 732 follicle cell nuclei in ten egg chambers displayed nuclear BrdUlabeling. In spite of endocycle delays, cyclinE'f3 6 /cyclinEPz8 follicle cells replicate their DNA fully as indicated by DNA indices (Table 2) and terminate endocycles with the appropriate developmental timing in stage 10A as indicated by our quantification of nuclear BrdU-labeling. To determine if synchronous gene amplification initiates at the appropriate developmental time and not earlier (which might result in increased replication fork progression), we quantified BrdU foci in stage 10B egg chambers in cyclinE'f3 6/cyclinEPz8 and OregonR follicle cells (Fig. 4B). We counted 394 cyclinEhf 36/cyclinEPz8 follicle cells in 6 egg chambers and 510 OregonR follicle cells in 8 egg chambers. 36/cyclinEP• 8 follicle cells displayed 4.8 BrdU foci/nucleus on average while cyclinE~f OregonR follicle cells displayed 4.7 BrdU foci/nucleus (Fig. 4B). We applied the Wilcoxon Rank Sum test to determine if the two distributions (Fig. 4B) were significantly different, and determined a P-value of 0.426, indicating that cyclinE1f36/cyclinEPz 8 follicle cells are not significantly different from OregonR follicle cells in the number of BrdU 109 foci/nucleus in stage 10B. We conclude that synchronous gene amplification initiates 8 with the appropriate developmental timing in cyclinE1P6/cyclinEPz follicle cells. Gene amplification at DAFC-66D initiates during follicle cell endocycles. Gene amplification during endocycles results in about 4 fold amplification by stage 10A (Calvi et al., 1998). Therefore, abnormal gene amplification occurring during endocycle Sphases in cyclinEf36/cyclinEPz 8 follicle cells (Fig. 4A) may account for increased replication fork progression in cyclinEP36/cyclinEPz8 follicle cells. We determined DAFC66D amplification profiles for cyclinElf6 /cyclinEPz 8 follicle cells in stage 10B,11 and 13 egg chambers to measure replication fork progression after the onset of synchronous gene amplification in stage 10B. We found that replication forks travel 40 to 60 kb between stages 11 and 13 (Fig. 4C). Previous work indicates that in OregonR, replication forks travel 10 to 20 kb between stages 11 and 13 (Claycomb et al., 2002). We conclude that gene amplification occurring during endocycles is not responsible for increased replication fork progression in cyclinEf3 6/cyclinEP" 8 follicle cells. Increasedreplicationfork progression in cyclinE/f36cyclinEP8 follicle cells may reflect increasedreplicationfork speed Increased replication fork progression may result from developmental delays during oogenesis. Normally, replication elongation occurs during stages 10B, 11, 12 and 13 (Claycomb et al., 2002). If these stages are prolonged, replication forks may travel farther given more time. We assayed egg-laying rates to determine the time required for oogenesis in cyclinEf36/cyclinEPZ8 females. Females generally have two ovaries each containing 16 egg-producing units known as ovarioles. We dissected and counted 110 ovarioles in cyclinE'f3 6 /cyclinEPz 8 and heterozygous sibling ovaries. 798 ovarioles in 52 1 36 cyclinE/cyclinE] /cyclinEPz 8 ovaries and 492 ovarioles in 32 heterozygous sibling ovaries were counted. We determined that cyclinE'f36 /cyclinEPz8 females have 15.3 t 1.8 ovarioles per ovary while heterozygous sibling females have 15.4 _ 2.1 ovarioles per ovary where the errors are the standard deviations of the samples. We concluded that cyclinE1f36/cyclinEPz8 ovaries have the same number of ovarioles per ovary as heterozygous sibling ovaries. To approximate the duration of oogenesis, we assayed the number of eggs produced in a 24hour period at maximum fecundity (Fig. 5A). Newly hatched females were collected over a period of 24 hours, and 30 females were placed in an egg collection chamber with OregonR males. Eggs were collected over a 24-hour period and counted for 12 days. The rate of egg production reached a maximum around day 7 for both cyclinE'f36/cyclinEPZ 8 and heterozygous sibling control females (Fig. 5A). Both cyclinEf3 6/cyclinEP8 and heterozygous sibling females produced about 20 eggs in a 24-hour period at maximum fecundity (Fig. 5A). Since each female has about 30 ovarioles (15 ovarioles per ovary), this measure indicated that an ovariole produces an egg in approximately 36 hours in both cyclinE'f36/cyclinEPz 8 and control females. This measure is intermediate to the 12-hour duration calculated using a similar method and the minimal 63.5 hours calculated by Lin and Spradling (Lin and Spradling, 1993; Spradling, 1993). Based on the results that (1) cyclinE'f36/cyclinEPz8 and control females are comparable in terms of the number of ovarioles per ovary and (2) that egg-laying rates are comparable over an extended period (Fig. 5A), we concluded that the time required for egg chamber maturation is not dramatically different in cyclinEf3 6/cyclinEPr8 females relative to a sibling control. 111 Figure 5. Increased replication fork progression is not due to developmental delays in oogenesis. (A) Egg-laying rates were determined by quantifying the number of eggs laid by 30 females in a 24-hour period. Per female egg-laying rate is on the Y-axis as a function of fly age in days on X-axis. Egg-laying rates for cyclinEf36/cyclinEPz8 females (blue) and sibling females (pink) peak at day 6 at about 20 eggs/day. (B) Egg chamber stages were quantified between at day 7. Apparently apoptotic egg chambers with pyknotic nuclei, are given as "A" on X-axis. Frequency of occurrence is on Y-axis. 673 cyclinEuf3 6/cyclinEPZ8 egg chambers (teal) and 494 sibling egg chambers (magenta) were counted with the standard deviation in egg chamber frequency in 4 ovaries as error. 112 A 25 20 F ,10 5 0 d4 d5 d6 d7 d8 d9 dl0 Day of egg collection -.- cyclinEIAP6/cyciAnEFZ8 B dll d12 -&-sibling control 0.25 0.2 0.15 S0.10.05 0 '2/3 4 5 6 7 8 9 10A 10B 11 12 -0.05 Egg chamber stage z Scycycc6/ CYC n£ 8 Msibling control 13 14 A To assess whether there are stage-specific delays in egg chamber development, we quantified egg chambers in cyclinEf36/cyclinEPz8 and heterozygous sibling ovaries (Fig. 5B) at maximum fecundity (d7 in Fig. 5A). We counted 673 egg chambers in 4 cyclinE'f6 /cyclinEPz8 ovaries and 494 egg chambers in 4 sibling control ovaries. We did not observe dramatic differences in the frequency of stage 2 through stage 5 egg chambers between cyclinEa36/cyclinEPz8 and sibling control females (Fig. 5B). During these stages, follicle cells are undergoing mitotic divisions. In addition, we did not observe dramatic differences in the frequencies of stage 7 and 8 egg chambers during which follicle cells are undergoing endocycles (Fig. 5B). We did see an appreciable difference in the frequency of stage 9 egg chambers during which follicle cells are undergoing their final endocycles (Fig. 5B). Stage 9 egg chambers occurred at a frequency of 6% in cyclinEPf36cyclinEPz8and 2% in sibling control ovaries. Interestingly, enrichment of stage 9 egg chambers in cyclinEf36 /cyclinEPz ovaries corresponded to increased S-phase length in the terminal endocycles as detected by ploidy analysis of follicle cells (Fig. 4A) and may reflect a developmental delay coupled to a cell cycle defect. The frequencies of gene amplification stages (10B, 11, 12 and 13) were similar in cyclinE16/IcyclinEPz8 and control ovaries (Fig. 5B). We saw a slight elevation in the frequency of stage 10B egg chambers in cyclinEf3 6/cyclinEPz8 ovaries, suggestive of increased time spent in this stage. We do not think that increased replication fork progression in cyclinEf36/cyclinEPz8 follicle cells is due to increased duration of stage 10B, since we have shown that replication forks progress about 60 kb between stages 11 and 13 (Fig. 4C). We conclude that the developmental timing of oogenesis is not altered 8 females. Our results suggest significantly in cyclinEf36/cyclinEýP that increased 114 replication fork progression in cyclinE'f3 6/cyclinEP 8 is not due to developmental delays in oogenesis. Polyteny is intact in cyclinElf 36 /cyclinEPz8 follicle cells Our results suggest that increased replication fork progression in cyclinE'f3 6/cyclinEPZ8 follicle cells is due to increased replication fork speed and not due to developmental delays that prolong the period of gene amplification. Polyteny affects replication fork speed (Steinemann, 1981). As such, we thought that increased replication fork progression in cyclinE'f3 6/cyclinEPr8 and cyclinE'f36/cyclinEP28 follicle cells might be due to defects in polytene chromosome structure. To determine if polyteny is maintained in cyclinE1f36/cyclinEP 8 follicle cells, we performed BrdU/FISH co-labeling experiments using FISH probes directed against DAFC-66D (Fig. 6A-D). We found that polytene chromosome structure is largely intact in cyclinE1f 36/cyclinEPz8 mutant follicle. In general, in cyclinEf 361/cyclinEPz 8 follicle cells, we saw one DAFC-66D FISH focus per cell that looked qualitatively similar to DAFC-66Dfoci in the sibling control (Fig. 6A and C). This observation suggested that polyteny is maintained for the 3 rd chromosome in cyclinE'f36/cyclinEPz8 follicle cells. We quantified BrdU and DAFC-66D FISH foci in 424 sibling control and 290 cyclinE'f36/cyclinEP=8 follicle cells to determine if the frequency of follicle cells displaying multiple DAFC-66D FISH foci or no FISH foci, both consistent with loss of polyteny, is increased in cyclinE'f36/cyclinEPz 8 follicle cells (Fig. 6E-F). In all cases, we found that DAFC-66D FISH foci were coincident with BrdU-labeled foci. In all cases with one DAFC-66D FISH focus/nucleus, the DAFC-66D FISH focus was coincident with the 115 Figure 6. Polytene chromosome structure is intact in cyclinE'1 6/cyclinEýa follicle cells. BrdU/FISH co-labeling was performed on cyclinElf 36/cyclinEPz 8 and sibling control ovaries using a DAFC-66D specific FISH probe. (A-D) Projections of stacked confocal images of follicle cells in stage 12 egg chambers. (A, C) DAFC-66D FISH. (B, D) DAFC-66D FISH in green and BrdU in red. (E and F) Stacked confocal images were used to quantify the number of BrdU-labeled foci/nucleus (X-axis) with number of nuclei falling into each category on the Y-axis. The number of nuclei showing one, two and no FISH foci in each category on the X-axis are shown in red, blue and yellow, respectively. 116 Q ci 40, o0 am W 00 r0o z".. ,•. -- 8 C '-O q .tiamN .-iaqmnN 0 oý 00 0 t- 0 0D W 0 a p!alJN .jIaq•lnN 0 -D emN 0 55- ( largest BrdU-*labeled focus in the nucleus (Fig. 6A-D). In cyclinE'f3 6/cyclinEPz 8 follicle cells, 2.9% (8/290) of follicle cells in stage 12 egg chambers showed two DAFC-66D FISH foci and 0.3% (1/290) showed no DAFC-66D FISH foci (Fig. 6F). In sibling control follicle cells, 1.2% (5/424) of follicle cells in stage 12 egg chambers showed two DAFC-66D foci and 0.2% (1/424) showed no DAFC-66D FISH foci (Fig. 6E). Although the occurrence of two FISH foci/nucleus is higher in cyclinElf3 6 /cyclinEPz 8 follicle cells (2.9%) than sibling control follicle cells (1.2%), we believe that polyteny is intact in cyclinE'f3 6/cyclinEPz8 follicle cells. 6 of the 8 nuclei displaying two BrdU FISH foci/nucleus were found in one of six cyclinEf3 6/cyclinEPz 8 egg chambers examined. We cannot, however, exclude the possibility that increased replication fork progression is due to aberrant polytene chromosome structure. cyclinE'ý 6 displays a dominant defect in replicationfork progression We sequenced the coding region of cyclinE'136 and identified a G to E substitution mutation (Fig. 7A). This amino acid substitution is not present in an isogenic line. The G to E substitution occurs in the 5 th residue N-terminal to the MRAIL hydrophobic patch, suggesting that the mutation may affect CyclinE/Cdk2 substrate recognition (Furstenthal et al., 2001; Schulman et al., 1998). We wished to determine whether increased replication fork progression was a gain-of-function or loss-of-function phenotype. We performed MPM2 antibody staining on cyclinElf3 6/cyclinEPz 8 mutant follicle cells. Localization of MPM2 to subnuclear foci is known to reflect CyclinE activity (Calvi et al., 1998). We were unable to detect any differences in intensities of subnuclear foci between cyclinEf36 /cyclinEPz8 and OregonR 118 Figure 7. cyclinE' l 6 displays a dominant phenotype. (A) cyclinE'f36 is a G to E substitution mutant in a non-conserved residue 5 residues removed from the MRAIL substrate recognition motif. (B) Quantitative real-time PCR at DAFC-66D was performed on stage 13 egg chamber DNA as described previously. Xaxis is distance from amplification maximum in kb. Y-axis is fold amplification. Df(2L)TE35D1/+ (brown) did not show a pronounced broadening of the amplified region suggesting that increased replication fork progression is not a loss-of-function phenotype. This was true of cyclinE 2 8/+ (pink), cyclinEPZB/+ (blue). cyclinEf36/+ (yellow) showed a slight broadening of the amplified region relative to other cyclinE mutant heterozygotes and OregonR (black), indicating that cyclinE*36 is a dominant mutant. 119 A .*•9* * * .* *.*** * •******9* C.elegans D. rerio M- musculus THVMERHPHL QPKMRAILLD WLIEVCEVYK TRVMERHPNL QPKMRAILLD WLMEVCEVYK D. melanogaster ISMLEQHPGL QPRMRAILLD WLIEVCEVYK EHFLQRHPLL QARMRAVLLD WLMEVCEVYK Gly to Glu B 50 45 40 a 35 30 20 ; 15 10 5 0 '10 20 30 - cyclin£E28/CyO -+"OregonR 40 50 60 Distance (kb) cyclin£AEf 6/CyO -- cyclinEPz 8/CyO 70 80 90 100 -- DJ2L)7£35DI/CyO controls, suggesting that any changes in CyclinE activity are beyond the limit of detection by this assay (data not shown). To determine if increased replication fork progression is recessive or dominant, we performed quantitative real time PCR on stage 13 egg chamber DNA to establish amplification profiles for cyclinE'f36/+, cyclinEPz8 /+ and cyclinEP28 /+egg chambers (Fig. 7B). To determine the loss-of-function phenotype, we examined Df(2L)TE35D1/+, which lacks one copy of cyclinE. Df(2L)TE35D1/+ stage 13 egg chambers displayed a small increase in fold amplification relative to OregonR stage 13 egg chambers at 20 kb, 30 kb, 40 kb and 50 kb from the amplification maximum (Fig. 7B). However, the differences were small (about 5 units fold amplification at any point). cyclinEP8s/+ displayed an amplification profile very similar to Df(2L)TE35D1/+ and cyclinEP28/+ follicle cells displayed an amplification profile very similar to OregonR follicle cells (Fig. 7B). cyclinE'f36/+ follicle cells, however, displayed considerable differences in fold amplification relative to OregonR at 20 kb, 30 kb and 40 kb (about 15 units fold amplification difference at each point - Fig. 7B). At 50 kb, the difference dropped down to about 7 units fold amplification and at 60 kb to about 5 units fold amplification. In cyclinE'f3 6/+, the slope of the drop-off in amplification levels has a noticeable shoulder near the amplification maximum (Fig. 7B), indicating that the last replication forks initiated from DAFC-66D travel farther in cyclinE'f36/+ follicle cells relative to all of the other heterozygous mutants described and the OregonR control. At 25-fold amplification levels, OregonR and cyclinEP28/+ replication forks have traveled about 10 kb. Df(2L)TE35DI and cyclinEP8 /+ replication forks have traveled about 15 kb. cyclinE1f36/+ have traveled about 30 kb (Fig. 7B). Thus, the phenotype of increased replication fork 121 progression is dominant in cyclinE'36 /+. We cannot distinguish whether this dominant effect is a dominant loss-of-function or a dominant gain-of-function phenotype. Double Parkedand the MCM complex localize as double bars in cyclinEP6/IcyclinEPZ 8 follicle cells The MCM complex localizes to replication forks and is the presumptive replicative helicase in eukaryotes (Aparicio et al., 1997; Calzada et al., 2005; Gambus et al., 2006; Ishimi, 1997; Labib et al., 2000; Moyer et al., 2006). During gene amplification, MCM subunits and Double Parked (DUP), the DrosophilaCdtl homolog, localize to replication forks (Claycomb et al., 2002). DUP is a known target of CyclinE/Cdk2 (Thomer et al., 2004) and DUP is required for MCM complex localization to replication forks (Claycomb). DUP and MCM chromatin localization is regulated by Cyclin/Cdk phosphorylation (Hendrickson, Thomer, Masai?) (Masai et al., 2000; Montagnoli et al., 2006). To determine if increased replication fork progression in cyclinEf36/cyclinEPZ8 follicle cells is due to altered chromatin localization of DUP and MCM complex, we performed in situ localization studies to examine DUP and MCM complex localization to replication forks. We observed localization of DUP and MCM subunits to double bars at reduced levels (Fig. 8). In cyclinE36/IcyclinEPz 8 follicle cells, we saw MCM localized, at reduced levels, to double bars with increased gap distances, relative to an OregonR wildtype control (Fig. 8K-N). MCM double bars with increased gap distances in cyclinEjf36/cyclinEPf8 follicle cells are consistent with increased replication fork progression. In addition, in cyclinElf36/cyclinEPZ 8 follicle cells, we saw DUP localized, at 122 Figure 8. Dup and MCM subunits localize to double bars in cyclinE' 6 /cyclinEra follicle cells. cyclinEJ6 I/cyclinEPz8 and OregonR ovaries were stained with anti-Dup (A-F) or antiMcm2-7 (G-N). (A-F) confocal imaging of Dup double bars showing single confocal images and projections, in which single confocal images taken at different depths are stacked on top of each other, for representative double bars. Single images and projections are marked in figure. (G-N) show anti-Mcm2-7 in red and YOYO-1 in green with single images and projections as marked. Arrows in (A-N) point to double bars. Scale bar is 1 [tm 123 OregonR 8 36/cyc2nEPz cyc1njEJcI DUP OregonR MCM P1,0jection P z8 cychnE/jEf 6/cyc/n£E reduced levels, to double bars. Although gap distances in these double bars appeared to be slightly increased in cyclinEl3 6/cyclinEPz 8 follicle cells, gap distances were not increased as dramatically as seen for MCM double bars in cyclinEft36/cyclinEPz8 follicle cells. These observations may indicate that DUP becomes uncoupled from replication forks and that this uncoupling correlates with increased replication fork progression in cyclinE'f36/cyclinEP8 follicle cells. Alternatively, these MCM and DUP localization phenomena may occur in different subsets of cells. We found MCM and DUP double bars in a small fraction of follicle cells examined and these subsets might not overlap. In addition, measurement of gap distances in BrdU-labeled double bars indicates a range of 3 6/cyclinEPz8 follicle cells (Table 1). Given replication fork progression defects in cyclinE'f the generally reduced localization of MCM and DUP to double bars in cyclinE'fS6/cyclinEPz8 follicle cells, we conclude that increased replication fork progression is not due to increased localization of DUP and the MCM complex to replication forks. In addition, we conclude that MCM complex localization to double bars with increased gap distances is consistent with increased replication fork progression. 125 DISCUSSION We have characterized the first mutants known to affect replication fork progression during gene amplification. cyclinEl3 6/cyclinEPz8 and cyclinE'~36/cyclinEP28 follicle cells displayed increased replication fork progression as evidenced by increased gap distances in BrdU-labeled double bars and expanded amplified regions for DAFC30B, DAFC-34B, and DAFC-66D as assayed by quantitative real-time PCR and comparative genomic hybridization (CGH) of the Drosophila2L tiling array. These mutants result in a dramatic two-fold increase in replication fork progression at DAFC30B, DAFC-34B and DAFC-66D. Our results demonstrate that gene amplification is not regulated by Replication Fork Barriers (RFBs). We cannot exclude the possibility that CyclinE is essential to sitespecific RFB function during gene amplification. CyclinE may regulate RFB function by regulating trans-acting factors or by modulating replication fork sensitivity to sitespecific RFBs by regulating replication fork components. Mutations in replication factors that compromise replication initiation during gene amplification result in thin eggshells (Landis et al., 1997; Landis and Tower, 1999; Schwed et al., 2002; Whittaker et al., 2000). Replication fork progression has not been examined in any mutants affecting gene amplification replication initiation and it is questionable whether examining replication elongation in the context of impaired replication initiation is informative or even possible. The cyclinE' 6 allele is unusual in that it is highly specific to replication elongation. In cyclinElf6/cyclinEPz 8 and cyclinE1 f36/cyclinEP28 follicle cells, DAFC-66D is amplified (at maximum) to levels 126 comparable to wildtype (Fig. 2B) and as we have shown, the cell cycle events leading up to gene amplification are minimally perturbed in cyclinEfl 6/cyclinEPz8 follicle cells. The functional significance of actively restricting replication fork progression during gene amplification is yet unclear. We examined the eggshells of eggs laid by cyclinE'f•6 cyclinEP'z females by Scanning Electron Microscopy. Follicle cell footprints, dorsal appendages, micropyle and operculum looked completely normal, indicating that increased replication fork progression does not disrupt eggshell formation (Fig. 9). Although we were unable to detect eggshell defects, cyclinEP6/cyclinE• '8 and cyclinEf36/cyclinEP28 females were sterile and semi-sterile respectively, suggesting that limiting replication fork progression during follicle cell gene amplification may be important for egg viability. Although we cannot exclude the possibility that reduced 2 8 females is due to viability of eggs laid by cyclinEf3l/cyclinEPz8 and cyclinE~6/cyclinE" effects in other tissues, an intriguing possibility is that misregulated replication fork progression disrupts the expression of genes important for egg viability. In wildtype, at DAFC-66D, replication forks travel 20 kb at most between stages 11 and 13 (Claycomb et al., 2002). In cyclinE3'6/cyclinEPz 8 , replication forks at DAFC-66D travel 60 kb between stages 11 and 13 (Fig. 4C). These active replication forks may impede gene expression during late stages. An expedient explanation for increased replication fork progression is that developmental delays increase the time spent in gene amplification. The prevailing view regarding replication fork progression during gene amplification is that bi-directional replication occurs until follicle cells slough off in stage 14 of egg chamber development (Claycomb and Orr-Weaver, 2005; Spradling and Leys, 1988). The primary locus for 127 Figure 9. Embryos laid by cyclinE'/ 61cyclinE e females have normal looking eggshells. Embryos were collected from cyclinE3 6I/cyclinEPz8 and sibling control females and visualized by scanning electron microscopy. 6 embryos were examined for each sample and representative images are shown. Scale bar is 100 jim. Follicle cell footprints (arrow), dorsal appendages (arrowhead) and micropyle (*) look normal in eggs laid by 6 /cyclinEPz 8 relative to those laid by a sibling females. cyclinE** 128 regulation is thought to be replication initiation, which is under developmental control. Following replication initiation events, slow-moving replication forks travel at about 50 to 100 bp/min (Claycomb et al., 2002; Spradling and Leys, 1988). In this model, the elapsed time between replication initiation events of gene amplification (occurring largely in stages 10B and 11 at DAFC-66D) and follicle cell removal in stage 14, determines the span of gene amplification. We did not detect any delays in oogenesis in cyclinE'16/cyclinEPz8 ovaries, suggesting that increased replication fork progression in cyclinEJP6 /cyclinEPz8 follicle cells is not due to a prolonged period between the onset of gene amplification and the sloughing off of follicle cells in stage 14 egg chambers. Increased replication fork progression might result from disrupted polytene structure. We conclude that increased replication fork progression in cyclinElf36/cyclinEPz8 36 P 28 follicle cells is not due to disrupted polyteny. Replication fork and cyclinE'1 /cyclinE speed is, in part, dependent on higher order DNA structure and increased replication fork speed in cyclinE3 6 . Polyteny affects replication fork speed. Measurements of replication fork speed indicate that while replication forks move at ~2.6 kb/min in Drosophila diploid cells, replication fork speed is an order of magnitude lower in Drosophila polytene larval salivary glands at ~300 bp/min. This order of magnitude difference may be due to protein/DNA complexes specific to polytene chromosomes. Prior to gene amplification, follicle cells undergo endocycles resulting in polytene chromosomes, which are maintained during gene amplification (Calvi and Spradling, 2001). The polytene structure of follicle cell chromosomes could serve as a major determinant of replication fork progression during gene amplification. 130 Increased replication fork progression is a dominant phenotype conferred by cyclinE1 36 . This mutant allele carries a Gly to Glu substitution five amino acids removed from the MRAIL hydrophobic patch. The MRAIL hydrophobic patch interacts with cognate RXL sequences and is important for Cyclin/Cdk substrate specificity (Loog and Morgan, 2005), inhibition of Cyclin/Cdk by CIP/KIP inhibitors (Wohlschlegel et al., 2001) and chromatin localization of Clb5 in S. cerevisiaeand CyclinE in Xenopus via interaction with RXL motifs in Orc6 and Cdc6, respectively (Furstenthal et al., 2001; Wilmes et al., 2004). The proximity of the Gly to Glu substitution found in cyclinE f36 to the MRAIL hydrophobic patch suggests that this mutation disrupts CyclinE/Cdk2 or CyclinE binding to replication factors. We are unable to predict, however, whether the Gly to Glu substitution increases or decreases CyclinE activity and we did not detect appreciable changes in CyclinE protein levels by in situ antibody staining of 8 and cyclinE'6/cyclinEP 28 ovaries (data not shown). cyclinEf~6/cyclinEPz CyclinE may directly regulate replication fork progression by covalently modifying replication fork components. In particular, we thought that the cyclinElf36 phenotype of increased replication fork progression might be due to altered CyclinE/Cdk2 regulation of DUP/Cdtl and the Mcm2-7 complex. Both DUP/Cdtl and Mcm2-7 are known to localize to double bars at DAFC-66D (Claycomb et al., 2002). In cyclinE'f36 /cyclinEPz 8 follicle cells, we observed DUP/Cdtl and Mcm2-7 localizing to double bars at reduced levels (Fig. 8). Although reduced localization to double bars is counterintuitive to increased replication fork progression, these proteins may be localized in excess and CyclinE/Cdk2 regulatory phosphorylation is complex. MCM subunits exist as multiple phosphoisoforms 131 that are cell cycle dependent (Young and Tye, 1997), Cyclin/Cdk phosphorylation is most clearly established for Mcm2 and Mcm4. While hyper-phosphorylation by CyclinB/Cdkl reduces chromatin affinity in both and Xenopus and human cells (Fujita et al., 1998; Hendrickson et al., 1996), complete dephosphorylation abolishes chromatin binding in Xenopus (Pereverzeva et al., 2000). Phosphorylation of Mcm4 by CyclinA/Cdk2 has been shown to inhibit Mcm4,6,7 helicase activity in human cells (Ishimi et al., 2000). The effects on Mcm2-7 localization may be downstream of DUP/Cdtl localization. DUP/Cdtl has previously been shown to be required for Mcm2-7 localization during gene amplification (Claycomb et al., 2002). Ectopic overexpression of a DUP phosphoacceptor mutant dominantly inhibits replication elongation at DAFC-66D (Thomer et al., 2004), suggesting that DUP phosphorylation by CyclinE/Cdk2 promotes replication elongation. Thus, reduced CyclinE activity would be expected to reduce replication fork progression, suggesting that CyclinEf '36 has increased activity. The 1 possibility remains that increased replication fork progression in cyclinEV 6 mutants is due to altered CyclinE/Cdk2 regulation of DUP/Cdtl and MCM2-7 complex at the replication fork. Increased replication fork progression seen in cyclinEV36/cyclinEPz 8 and 28 follicle cells demonstrates plasticity in replication fork speed during cyclinE1 0/cyclinEP gene amplification. This plasticity may be functional. Previously, amplified regions for DAFC-30B (Claycomb et al., 2004), DAFC-34B (J. Kim and T. Orr-Weaver, unpublished results) and DAFC-66D (Claycomb et al., 2004; Claycomb et al., 2002; Spradling and Leys, 1988) were determined to be ~100 kb in span with replication forks predicted to travel -50 kb to either side of confined replication initiation sites. Our results by 132 comparative genomic hybridization of the Drosophila2L tiling array indicate greater variability with DAFC-30B amplifying a 160 kb region, DAFC-34B amplifying a 100 kb region and DAFC-66D amplifying a 120 kb region. Replication fork speed may be regulated variably at the different amplicons perhaps to meet the varying demands of transcription at these amplicons. In addition, replication fork speed may be regulated variably in different subsets of cells in response to developmental cues. 133 MATERIALS AND METHODS Quantitative Real-Time PCR Quantitative realtime PCR was performed using primer sets spanning 50 kb on either side of ACE3 (denoted as distance 0) at 10-kb intervals and primers to a nonamplified intergenic region on chromosome arm 3R (located approximately 25 kb upstream of the DNApola locus) as described previously (Claycomb et al., 2002). Primer sets spanning 60 - 100 kb on either side of ACE3 were generated as described previously (Claycomb et al., 2002) and supplied by GeneLink. In Fig. 2, three ten-fold dilutions of stage 1-8 ovary DNA were used as standard. Relative fluorescence was measured for each sample in relation to the standard curves and standard deviations of triplicate reactions were calculated by the ABI Prism 7000 software. Fold amplification was calculated by dividing the relative fluorescence of the amplicon site by the relative fluorescence for the nonamplified intergenic region near DNApola. Error is the standard deviation of the ratio A/C = (FA/FC)*{[(SA/FA)A2 + (SC/FC)A2]}. A, amplicon locus; C, control locus; FA, relative fluorescence for amplicon locus, FC, relative fluorescence of control locus; SA, standard deviation for amplicon locus; SC, standard deviation for control locus. Flow cytometry and DNA index Follicle cell nuclei were isolated as described previously and stained with DAPI (Lilly and Spradling, 1996). Flow-sorting and ploidy analyses were performed on a MoFlo flow cytometer (Dako, Fort Collins, CO) at the M.I.T. Flow Cytometry Core Facility. An Argon Ion laser was tuned to multi-line UV with a 450/22 bp filter. 16C nuclei were collected for DNA microarray experiments. For the calculation of DNA indices, ploidy analyses were performed in three separate experiments. 2C, 4C, 8C, 16C, and 32C peaks 134 were gated and the mean of total fluorescence intensity calculated. DNA indices were found by dividing the mean of total fluorescence for the 4C, 8C, 16C, or 32C peaks by the mean of total fluorescence for the 2C peak within the same sample. Error is standard deviation. Drosophila2L tiling array Drosophila2L tiling arrays were kindly provided by David MacAlpine and Steven Bell (M.I.T., Cambridge, MA). DNA from 16C follicle cells and embryonic DNA for reference was purified as previously described (Claycomb et al., 2004). DNA was labeled, slides hybridized and data analyzed as previously described (MacAlpine et al., 2004). To calculate p-values, total data points were used to model the normal distribution. Experiments were performed in triplicate with one dye-swap. Sequencing Sequencing was performed as described previously using genomic DNA from 8 embryos for each sequencing run (Dej et al., 2004), cyclinE coding regions were sequenced with two-fold coverage and the mutation was sequenced with four-fold coverage. An isogenic strain was sequenced in parallel and the Gly to Glu substitution was not present in this strain. Cytology Anti-DUP and anti-MCM2-7 antibody staining was performed on whole ovaries as previously described (Claycomb et al., 2002). YOYO-1 (Molecular Probes) was used to 135 stain DNA at 1:2000. BrdU/FISH co-labeling was performed as previously described (Claycomb et al., 2004). Imaging was performed using a Zeiss Axiovert 100 M Meta confocal microscope with LSM510 software. Excitation of YOYO-1 and rhodamine dyes used the 488 and 543 nm lasers respectively. Deconvolution was carried out using Huygens2.3-professional (Scientific Volume Imaging). 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Mcm2 and Mcm3 are constitutive nuclear proteins that exhibit distinct isoforms and bind chromatin during specific cell cycle stages of Saccharomyces cerevisiae. Mol Biol Cell. 8:1587-601. Zechiedrich, E.L., and N.R. Cozzarelli. 1995. Roles of topoisomerase IV and DNA gyrase in DNA unlinking during replication in Escherichia coli. Genes Dev. 9:2859-69. 141 CHAPTER FOUR Conclusions and perspectives 142 CONCLUSIONS & PERSPECTIVES We observed increased replication fork progression in cyclinE' 6 mutants, which correlates with reduced DUP and Mcm2-7 co-localization to sites of replication initiation (data not shown) and to replication forks. We favor the model that CyclinE/Cdk2 regulates DUP and Mcm2-7 at the replication fork to mediate fork progression. Changed chromatin configuration and topological parameters are alternative explanations. In the following chapter, we note the alternative models and delineate the reasons why we have excluded them. To conclude the chapter, we discuss CyclinE/Cdk2 regulation of DUP and Mcm2-7 and propose future experiments investigating a possible role for CyclinE/Cdk2 in regulating replication fork progression via DUP. Chromatin structure FISH with DAFC-66D and DAFC-7F specific probes, and BrdU-labeled foci indicated that follicle cell polytene chromosome structure, defined previously by these methods (Calvi and Spradling, 2001), is maintained in cyclinEJP6/cyclinEPZ 8 follicle cells. However, altered chromatin structure may not manifest as loss of polyteny. Cohesins, histone modifications, or other protein complexes defining chromatin structure may be disrupted in cyclinEf36 mutants. We performed anti-acetylhistone H4 (Lys5) (Upstate Biotechnology), staining on 6 /cyclinEPz cyclinEfn3 8 28 ovaries. Anti-acetylhistone H4 (Lys 5) and cyclinEf36/cyclinEP localizes to DAFC-66D during gene amplification (G. Bosco, unpublished results). Acetylated histone H4 increases gene amplification (Aggarwal and Calvi, 2004), suggesting that this histone modification promotes replication, perhaps by promoting an 143 open chromatin configuration (Aggarwal and Calvi, 2004). Anti-acetylhistone H4 (Lys5) 6/cyclinEPzs and cyclinE'f3 6/cyclinE•2 8 follicle cells, similar to localized to foci in cyclinE'13 a wildtype control, suggesting that replication fork progression defects are not due to alterations in H4 acetylation (data not shown). We were not able to detect altered chromatin structure by in situ antibody staining with anti-acetylhistone H4 (Lys5). Additional antibodies specific for histone modifications are commercially available and several have been tested for specific localization in follicle cells (G. Bosco, unpublished results). Many of these produced pan-nuclear staining in the follicle cells. More interesting localization patterns may be uncovered by washing the samples with high salt buffer to remove non-chromatin bound fractions. This approach was taken to unmask specific Mcm2-7 localization to follicle cell amplicons (Claycomb et al., 2002). Cohesin localization to follicle cell chromosomes has not been characterized. However, antibodies to Drosophilacohesin subunits Rad21 (Lee et al., 2005) and Smcl (Dorsett et al., 2005; Thomas et al., 2005) exist and cytological studies may prove an expedient route to examine cohesin localization in cyclinElf36/cyclinEP8 and cyclinE'f 36/cyclinEP2 8 follicle cells. Increaseddistance between replicationforks in cyclinE'36/cyclinEPz8 and cyclinE'f36/cyclinE P28follicle cells Increased replication fork progression may be due to topological factors, such as the helical strain generated by multiple, tandem replication forks. In OregonR wildtype follicle cells at DAFC-66D, replication forks are ~10 kb apart (Spradling and Leys, 1988). This inter-replication fork distance is calculated by determining the number of 144 replication initiation events (equal to the number of replication forks moving tandemly in one direction) and dividing the interval amplified by these amplification forks by the number of replication forks. For example, DAFC-66D is amplified ~30 fold by our measure, consistent with the results of J. Claycomb and colleagues (Claycomb et al., 2002). ~30 fold amplification corresponds to 5 replication initiation events and therefore 5 replication forks moving in one direction spread over a 50 kb interval, which indicates replication fork spacing of -~10 kb in wildtype. Since the amplified region is doubled at DAFC-66D in cyclinEf36/cyclinEPzs and cyclinEf'6 /cyclinEP28 follicle cells, and amplification levels at the maximum are not diminished, this suggests that replication forks are spaced ~20 kb apart. However, these values are approximate since replication forks may not be distributed uniformly. CyclinE/Cdk2 is required for replication initiation (Knoblich et al., 1994). As such, we would like to note that a potential mechanism for increased replication fork progression seen in cyclinEIf36 mutants would result from a defect in replication initiation. Decreased replication initiation rates would allow replication forks to travel farther between origin firings. The resulting increased distance between replication forks could relieve superhelical strain allowing replication forks to travel faster. We do not think this is a likely mechanism given that fold amplification is not decreased at DAFC-66D in cyclinE"36 mutants. In addition, in wildtype, relatively small differences are seen in replication fork progression among the follicle cell amplicons. Replication forks progress ~50 kb for DAFC-30B, DAFC-62D and DAFC-66D although these amplicons are amplified 4-, 3.5- and 30-fold respectively (Claycomb et al., 2004; Claycomb et al., 2002). If the topological strain generated by tandem replication forks affects replication 145 fork speed, we would expect a correlation between the number of replication initiation events and replication fork progression. Regulation of DUP and Mcm2-7 at replicationforks Increased replication fork progression in cyclinEJP6/cyclinEP8 and cyclinE'f36/cyclinEP28 follicle cells may be due to aberrant CyclinE/Cdk2 regulation of the protein machinery at the replication fork. Both DUP and Mcm2-7 localize to double bars (Claycomb et al., 2002). During gene amplification, Mcm2-7 localization to double bars requires unimpaired DUP function, suggesting that DUP (which is required along with Cdc6 for Mcm2-7 loading at the Pre-Replication Complex) is involved in maintaining Mcm2-7 at slow-moving replication forks (Claycomb et al., 2002; Spradling and Leys, 1988). Thomer et al. have described gene amplification defects for DUP mutants incapable of undergoing CyclinE/Cdk2 phosphorylation (Thomer et al., 2004). Overexpression of an N-terminal deletion (C-DUP) greatly increases BrdU-incorporation at gene amplifying foci, whereas overexpression of an N-terminal phosphomutant lacking N-terminal Cdk2 phosphorylation consensus sequences (DUP 10(A)) inhibits gene amplification completely. Of particular interest, overexpression of DUP 10(A) inhibited gene amplification at DAFC-66D during developmental stages when DAFC-66D is undergoing replication elongation only, suggesting that CyclinE/Cdk2 is required for replication fork progression. Amplification parameters (maximum amplification and amplification profile) have not been determined under conditions of C-DUP overexpression and it is unclear whether increased BrdU-incorporation at gene 146 amplifying foci is due to increased replication initiation or increased replication fork progression. C-DUP lacks potential ubiquitylation sites regulating DUP degradation (Nishitani et al., 2006; Senga et al., 2006). Thomer et al. have shown that CyclinE/Cdk2 activity is required for DUP degradation, and that the N-terminus is necessary and sufficient for DUP degradation in follicle cells, suggesting that CyclinE/Cdk2 phosphorylation of DUP at the N-terminus promotes DUP degradation (Thomer et al., 2004). DUP localizes to replication forks during gene amplification and failures to degrade DUP may have consequences at replication forks. Although DUP is required for Mcm2-7 localization to double bars (Claycomb et al., 2002), this observation may reflect an earlier requirement for DUP in loading the MCM complex, perhaps during replication initiation. The role of DUP, at replication forks during gene amplification, is not yet clear. We observed reduced localization of DUP to double bars, indicating that DUP localization to double bars is not limiting for replication fork progression. We also observed reduced localization of Mcm2-7 to double bars in cyclinEf36/cyclinEPz 8 follicle cells. Given that helicases generally promote replication fork progression, our observation suggests that Mcm2-7 localization is not limiting for replication fork progression. In general, Cyclin/Cdk activity inhibits Mcm2-7 chromatin localization (Findeisen et al., 1999; Fujita et al., 1998; Hendrickson et al., 1996) and reduced localization of Mcm2-7 to double bars may indicate that cyclinEf3 6 is a gain-offunction mutant. We do not think this is the case. Normally, nuclear CyclinE levels are high during gene amplification. Reduced Mcm2-7 localization at double bars in cyclinE•36/cyclinEPz8 follicle cells does not reflect total Mcm2-7 chromatin localization, which may more accurately reflect CyclinE/Cdk2 activity. Total chromatin localization 147 6 /cyclinEPz 8 follicle cells. We saw nuclear Mcm2-7 may, in fact, be increased in cyclinEf31 localization in a small fraction of cyclinEl 36 /cyclinEP s follicle cells (Fig. 1A). Normally, Mcm2-7 localizes to foci corresponding to gene amplification at DAFC-66D (CantonSin Fig. 1A). Increased ectopic replication seen in cyclinEf36/cyclinE•z8 and 3 6/cyclinEP2 8 follicle cells (Fig. 1B) is consistent with more widespread Mcm2-7 cyclinE"f localization. Calvi et al. postulated that high nuclear CyclinE levels are important for restricting genomic DNA replication during gene amplification (Calvi et al., 1998). If CyclinE inhibits nuclear Mcm2-7 chromatin localization and replication fork progression at follicle cell amplicons, our results are consistent with reduced CyclinE activity in cyclinEI36 mutant follicle cells. Future Experiments Our results suggest that cyclinEf36 is a loss-of-function allele. We would like to confirm that CyclinE/Cdk2 activity is reduced in cyclinE'f36 mutants. CyclinE/Cdk2 activity could be determined by performing in vitro kinase assays using H1 as a target. We will immunoprecipitate kinase using anti-DUP which has been shown to pull down functional Cdk2 (Thomer et al., 2004). Alternatively it may be necessary to immunoprecipitate from lines expressing UAS:6Xmyc:CDK2 using anti-Myc, given that CyclinE'f36 may interefere with DUP binding. Overexpression of the N-terminal truncation of DUP (C-DUP) leads to increased gene amplification. It has not been determined whether this effect is due to increased replication initiation or elongation. We would be interested to know whether replication fork progression is increased in these mutants, and if so, what the effect of C-DUP 148 Figure 1. cyclinE"/IcyclinEvafollicle cells display nuclear Mcm2-7 localization consistent with more BrdU-labeled sites throughout nucleus. PanelA: cyclinE'P6 /cyclinEPz8 follicle cells (D-F) displayed nuclear Mcm2-7 localization as visualized by anti-Mcm2-7 staining (A, D) and DNA staining with YOYO-1 (B, E) in stage 12 egg chambers. In a CantonS wildtype control (A-C), Mcm2-7 localizes to a single major focus corresponding to replication at DAFC-66D. (C, F) merge with antiMcm2-7 in red and YOYO in green. Antibody staining was performed as in Chapter 3. Panel B: Confocal images of BrdU-incorporation in stages 11 and 13 in CantonS, 2 8 follicle cells. Imaging was performed as cyclinElf36/cyclinEPz8 and cyclinE'36/cyclinEP described in Chapter 3. (C) cyclinE'f36/cyclinEPz 8 and (E) cyclinEf36/cyclinEP28 follicle cells display punctate BrdU-labeled spots throughout the nucleus in stage 11 correlating with more widespread Mcm2-7 localization in cyclinEf36/cyclinE"8 follicle cells. (A) CantonS control with 1 BrdU focus/nucleus. (B, D, F), In stage 13 egg chambers, 28 CantonS, cyclinE'I36/cyclinEPZS and cyclinEf36/cyclinEP follicle cells display BrdU- labeled double bars corresponding to replication elongation at DAFC-66D. 149 Mcm2-7 merge DNA CantonS cyc/inEI P 6/cychnE Z8 B stage 11 CantonS 28 cycn/i '1 6/cycalnE' stage 13 6/cyclinEPz 8 or cyclinE* 3 6/cyclinEP28 background. These expression is in a cyclinEf3 experiments would begin to address whether CyclinE regulates replication forks through DUP. C-DUP lacks potential ubiquitylation sites regulating DUP degradation (Arias and Walter, 2006; Nishitani et al., 2006; Senga et al., 2006) and increased gene amplification may be due to persistence of DUP in the cell. In addition, the N-terminus may carry other, as yet unmapped, regulatory domains. A Cdk phosphomimetic DUP mutant would be informative for determining how CyclinE regulates DUP because it would more specifically address CyclinE regulation of DUP. 151 REFERENCES Aggarwal, B.D., and B.R. Calvi. 2004. 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