Investigation on Instruments and Measurement Techniques for the Thermoelectric Properties of Materials OPTIONAL LOGO HERE Dwencel John Mamayson1, Tony V. Varghese2a, Dr. Yanliang Zhang2b, Andrew Wilson2b, Dr. Don Plumlee2b, Jacob Davlin2b 1 Science, Math and Engineering, Cosumnes River College 2a Material Science Engineering, Boise State University 2b Mechanical & Biomedical Engineering, Boise State University Objectives To study and be familiar about the operations of the current instruments and measurement techniques for measuring thermoelectric properties of materials. Method of Measurements Proposed Changes & Future Works For the Bulk-Pellet Sample Measurement Set-up: (Cross-Plane) Set-up for Bulk-Pellet Samples: The order of set-up process: • Place the sample between the Indium contact thermocouple for cold temperature (negative Seebeck voltage) on the bottom and the Indium contact thermocouple for hot temperature (positive Seebeck voltage) on the top. • Place the heater on the top of the hot temperature Indium contact. • Screw and tighten the plastic insulator for pressure application. To improve these current instruments and measurement techniques for better measurements and results. Background What is Thermoelectric Effect? • Direct conversion of temperature differences on a material’s two sides into electricity is called the “Seebeck” effect. OPTIONAL LOGO HERE • The installation of Styrofoam to the instrument: Minimized the heat losses from convection and radiation heat transfer. “Graphical Result of Ceramic Material Measurements” Set-up for Thick and Thin Film Samples: and/or • Direct conversion of electric current to temperature difference on material’s two sides is called the “Peltier” effect. • N-type and P-type of the same material are connected electrically in series and thermally in parallel to form a thermoelectric module. Application of Thermoelectric Effect: • Thermoelectric generators, TEG (also called “thermoelectric modules”) are devices that use the “Seebeck” effect to harvest waste heat. “Thermoelectric Generator for Efficient Automotive Waste Heat Recovery” TEMPLATE DESIGN © 2008 www.PosterPresentations.com The order of set-up process: • Place one side of the glass with the sample on the top of the heat sink and the other on the (hot side) module. • Place the Indium contacts for the cold and hot temperature. thermocouples on the respective sides of the sample. • Place the plain insulator piece on the top of the Indium contacts. • Place the Insulator with screws on the top of the plain insulator for pressure application. Improvements & Results The overall results showed a significant difference between the thermal conductivity of the Plain Low Temperature Co-fired Ceramic (LTCC) and the Silver Thermal Vias LTCC . “Overall Ceramic Package TEG Device Schematic with Thermal Vias” The figure shows the Silver Thermal Vias LTCC on the left and the Plain LTCC on the right . For the Thick and Thin Film Sample Measurement Set-up: In the Thick and Thin Film Measurement Set-up: In the Bulk-Pellet Sample Measurement Set-up: • The application of high thermal conductivity Silicone thermal paste between the sample and the instrument: Increased sample and set-up thermal interface conductance. Reduced measurement error due to the thermal contact resistances. • The silicone thermal conductive paste can be replace by an easier-to-clean, higher thermal conductive paste like silver paste. • The Styrofoam material cover can be replace by a better foam-like material which has lower thermal conductivity. • Fabrication of the design and then experimentation using materials with reported literature thermal properties to evaluate the accuracy. • The alteration of the insulators’ orientation and addition of glass slide (above the Indium contacts an the sample) and (blue) tape bundle to the set-up: Balanced the insulators. Abled to apply maximum pressure on both sides. Minimized the shattering of the glass-sample holder. • Build a design that has pressure variation only to the sample. • Initiate the thermal insulation idea using a foam-like material with a very low thermal conductivity. • Separate the heat sink from the module. Acknowledgement National Science Foundation; Office of Special Programs, Division of Materials Research and Research Experience for Undergraduates (REU) Program [DMR-1359344] at Boise State University.