Spring 2012
Organic Chemistry Lab
CHML211
Lab Schedule,
Course Policies, and
Safety Information
Prerequisite/Required Materials
PREREQUISITE: Grade of “C” or better in CHM102!
REQUIRED TEXTS/SUPPLIES:
1. LAB MANUAL:
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Organic Chemistry: Chemistry 211-212 Laboratory
Manual Fall 2010 Edition—previous editions are
unacceptable
2. LAB NOTEBOOK:
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Organic Chemistry Laboratory Notebook
3. SAFETY GLASSES/GOGGLES:
–
Can be glasses or goggles, as long as they form a
complete seal around eyes!
Course Website
• http://www.uncw.edu/chem/courses/Chml211/index.htm
Lab Schedule
Monday and Thursday lab sections are on different schedules.
Please be sure you check the schedule for your lab day!
Attendance Policy
• All labs are mandatory.
• No make-up labs for any reason.
• Missed lab = zero (regardless of reason).
• Missing 3+ labs = F for course.
• Athletic events are NOT excused absences.
Grading
• Lab is graded separately than lecture!
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Quizzes (45%)
Notebook Maintenance (~10%)
Lab Reports (~35%)
Technique (~10%)
Course Grading:
– A = 90-100, B = 80-89, C = 70-79, D = 60-69, F = 59 and below.
– Plus (+) or minus (-) grades may be awarded at the discretion
of the instructor.
Lab Quizzes
• 3 lab quizzes , 3-5 experiments on each.
• Full experiment after all quizzes! Plan on staying for
the entire lab period!
• Make up quizzes will only be allowed for excused
absences.
– To have a quiz absence excused, the student must:
• Email before beginning of lab
• Bring doctor’s note
Lab Notebook
• A specific list of notebook requirements at end of
POWERPOINT presentation for each experiment.
• Pre-lab (due at beginning) and In-lab entries (due
with final lab report).
• Incomplete/missing pre-lab = no lab = ZERO
• Please be sure to refer to APPENDIX C (p. 227-230)
for formatting example!
Final Lab Reports
• In lab manual at end of each experiment.
• Due dates announced by instructor.
• Unless otherwise instructed, EACH LAB GROUP
submits one copy of the final lab report.
• Late reports = 5% penalty per day
– Once lab reports are returned to students graded, NO
MORE WILL BE ACCEPTED!
Lab Technique
• You are responsible for your own safety!
– Be prepared and familiar with safety hazards!
– Wear proper shoes and eye protection!
– Common sense and thinking are REQUIRED.
• You are responsible for cleaning up after
yourself!
– YOU. Not your lab instructor. If we clean, you pay.
Personal Electronics
• Cell phone use WILL NOT BE tolerated.
– Turn ON SILENT OR VIBRATE before lab and PUT IT
AWAY!
– YOURS rings = you leave = ZERO
– Cannot use phone as calculator during quizzes!
• Laptops and desktop computers use is allowed for
lab related activities ONLY.
• Ipod use is not acceptable in lab!
Other Issues
• Please refer to the online syllabus for
information regarding:
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Learning Outcomes
Academic Integrity
Students with Disabilities
Violence and Harassment
Safety in the Organic Lab
• Follow instructions at all times!
• Act responsibly at all times!
• No food or drinks on lab benches!
• Dress appropriately for lab!
• Come prepared! Know what you are going to do,
and what the hazards are!
• Report all accidents to the instructor, no matter
how small.
Acceptable Clothing for Lab…
• DO wear
– Goggles/safety glasses
– Closed-toe shoes
– Tie back long hair
• DON’T wear
– Sandals/flip-flops
– Jewelry
– Loose or baggy clothing
Lab Safety Equipment
Safety Shower
Eyewash
Safety Goggles/glasses
Lab Safety Equipment
Fire Extinguisher
Fume Hood
Accidents and Injuries
• Report ALL injuries to lab instructor IMMEDIATELY,
no matter how minor.
• Be aware of hazards associated with each chemical
and technique you will use in the experiment!
• Complete an Injury Report Form.
First Aid
• Eye accidents: Wash eyes in stream of water using
eyewash station for 15 minutes!
• Chemical burns: Immediately flush the affected area with
a large amount of water in the sink! Use safety shower if
necessary!
• Thermal burns: Determine the type and extent of the
burn. Take appropriate action.
– 1st degree: red skin, no blisters.
• Immerse in cold water/apply ice.
– 2nd degree: blisters.
• Immerse in cold water, then apply clean gauze.
– 3rd degree: broken skin, tissue damage.
• Cover with clean gauze. Visit the Health Center.
First Aid
• Bleeding, cuts, and abrasions:
– Clean wound with soap and warm water.
– Apply pressure with clean gauze pad until bleeding stops.
– Cover wound with bandage or clean gauze pad and secure.
• Poisoning:
– If, after contact with, inhalation of, or accidental ingestion of
a chemical, you experience discoloration of the lips, a
burning sensation in the throat, stomach cramps, nausea
and vomiting, or confusion, seek treatment IMMEDIATELY
for chemical poisoning!
UNCW Safety Contract
• READ Laboratory Rules and Guidelines (p. vii)
CAREFULLY!
• READ, SIGN, AND SUBMIT safety contract (p. xi) to
instructor!
Waste Disposal
• Waste disposal procedures are at end of the
procedure for each experiment.
• If you do not know which waste goes where,
ASK!
• NOTHING DOWN THE SINK!