CHM 2046L: CHEMISTRY II LAB Summer 2015 Instructor: Contact: Department: Katya Nacheva, PhD nacheva.katya@spcollege.edu (or through MyCourses) Natural Science Meg Delgato, PhD, Academic Chair John Chapin, Dean COURSE INFORMATION: Course Description: This lab will involve hands-on investigations of topics including kinetics, chemical equilibria, buffer systems, redox reactions, and qualitative analysis. Course Corequisite: The corequisite for this course is General Chemistry and Qualitative Analysis II (CHM 2046). Please note that students who withdraw from lecture or lab must withdraw from the appropriate corequisite course. REQUIRED TEXTBOOK & OTHER RESOURCE INFORMATION: Textbook: General Chemistry II Laboratory Manual, Custom Ed., Slowinski, et al. ISBN-13: 9781285886428 Other Required: Bound composition style notebook. The pages must be stitched, not glued, into the binding and have no perforations. It can either be lined like notebook paper or have a grid like graph paper. ATTENDANCE POLICY: Attendance will be taken at every lab meeting. Tardiness is not acceptable. If you miss my discussion at the beginning of lab, you will miss important explanations, and therefore would be unsafe in the lab. Under no circumstances will you be admitted to lab if you are more than 10 minutes late, and you will be considered absent for that lab meeting. Attendance must be reported for the first two weeks of the semester. If you are not attending this class during this time, you will be automatically dropped from the course. The college-wide attendance policy is included in the “Addendum to the Syllabus”, which should be read at the following web address: http://www.spcollege.edu/central/asa/addendum.htm. At the 60% mark in the semester, students will be evaluated for active participation in the course. If you have missed three or more lab meetings, you will fail to meet my criteria for active participation and will be withdrawn and given a “WF” for the course. PLEASE NOTE: The lecture and the lab are co-requisites. If you withdraw from lecture, you must also withdraw from the lab. If you withdraw from the lab, you must also withdraw from the lecture. The last day to withdraw with a "W" is June 26, 2015. Failure to do drop before the drop date will result in you receiving a final grade of "F." NOTE: instructors are NOT able to withdraw students. TESTING / GRADING POLICY: The following weights will be given to assignments: 1. 2. 3. 4. 5. You will have unannounced quizzes at the beginning of some lab periods. If you are late to lab and miss the quiz, you will receive a zero for that quiz grade. Quizzes cannot be made up. However, your one lowest quiz score will be dropped. Your overall quiz average will count for 20% of your overall grade. You may use your lab notebook (not lab manual) as a reference for any quiz. Each week you will turn in data, calculations and ASA assignment. This will count as your weekly lab report. Again, if you miss a lab, you will receive a zero for that lab report grade. Lab reports cannot be made up. Your one lowest lab report grade will be dropped. Your overall report average will count for 40% of your overall grade. Your lab notebook will be graded at the end of the semester and will count for 10% of your final grade. The lab exams (midterm and final) will count together for 30% of your overall grade. 10% may be deducted from each lab report score for failure to follow experimental procedures and safety rules. Always wear your goggles and clean up your glassware and station when you have finished with your experiment. You can calculate your grade as follows: Quizzes Reports Lab notebook Final Your letter grade will be: A 90 – 100 % B 80 – 89 % Percentage of Overall Grade 20 40 10 30 C 70 – 79 % D 60 – 69 % F < 60 % REQUIRED ASSIGNMENTS EACH WEEK: 1- Read the introductory material pertaining to each experiment BEFORE the scheduled lab. 2- In your own words, write a detailed procedure for the lab in your lab notebook (BEFORE coming to lab). You should be able to follow the procedure from your lab notebook. 3- You will also need to complete your lab “report”, which includes your data and calculations and the advanced study assignment (ASA) from your lab manual. These reports are to be handed in before your next lab and will be graded for accuracy and precision. Special Accommodations If you wish to receive special accommodations as a student with a documented disability, please make an appointment with the Learning Specialist on this campus (712-5789). If you have a documented hearing loss, please contact the Program for the Deaf at 791-2628 (V/TDD). If you will need assistance during an emergency classroom evacuation, it is imperative that you speak with you campus Learning Specialist immediately about arrangements for your safety. CAMPUS SAFETY AND SECURITY: For information on campus safety and security policies please contact 727-791-2560. For information on sexual offenders on your campus please contact campus security or the associate provost office or for general information go to the State of Florida website at http://www3.fdle.state.fl.us/sopu/index.asp. CLASSROOM BEHAVIOR: The following behavior may warrant dismissal from: Regular use of profanity in lab, talking or texting on your cell phone during lab, leaving lab repeatedly to talk or text on your cell phone, arriving to lab more than 10 minutes late, drinking or eating in lab, wearing shoes that do not cover your entire foot (including your heels), and/or not following safety rules (such as wearing your goggles). Please be safe and respectful at all times while in the lab room. References: Please refer to the appendices in your lab manual for a review of measurement, significant figures, graphing, etc. Resources: I will be available during office hours to answer any questions you have. Also, there are (FREE) tutors in FA 154 which can help you at times when I may not be available. For nonacademic resources, please see http://www.spcollege.edu/hec/hus/resources.htm CHM 2046L Lab Schedule - Session I, Spring Semester 2015 Week/Date Topic Experiment 1. May 18 Check-In/Introduction/Safety 1 2. May 20 Rates of Chemical Reactions I: The Iodination of Acetone 2 3. May 25 4. May 27 Memorial Day Rates of Chemical Reactions I: The Iodination of Acetone (cont.) 2 Determination of the Equilibrium Constant 4 Properties of Systems in Equilibrium— Le Chateler's Principle 3 7. June 8 Determination of the Hardness of Water I 5 8. June 10 Determination of the Hardness of Water I 5 9. June 15 pH--Buffers and Their Properties 6 10. June 17 pH--Buffers and Their Properties (cont.) 6 11. June 22 Qualitative Analysis of Group I Cations 7 5. June 1 6. June 3 June 26th - last day to drop with a “W” 12. June 24 The Ten Test Tube Mystery 10 13. June 29 The Ten Test Tube Mystery (cont.) 10 14. July 1 Determination of Iron by Reaction with Permanganate--A Redox Titration 11 15. July 6 Final Quiz/Lab Notebook Check-Out 16. July 8 Electrolysis _Online Assignment (no lab meeting) Due on July 13th This schedule is both approximate and tentative; it may be changed as needed during the semester. The instructor reserves the right to make adjustments as needed to this syllabus at any time during the semester.