Rev 082007 SYLLABUS Tulsa Community College, SE Campus Spring 2011 Course: CHEM 2145: Organic Chemistry I Day(s) and Time(s): MW 5:30pm-6:50pm W 7:00pm-7:50pm W 8:00pm-9:50pm Course Delivery Method: Classroom Section #: 305 CRN: 22131 Start and end dates: 1/10/2011 - 5/2/2011 Course format: Lecture, discussion, laboratory Instructor: Steve Minor Office Hours: by appointment Office Email: stephen_minor@mail.tulsacc.edu Office Phone: 918-595-7673 for messages TO CONTACT THE DIVISION OFFICE: Division: Science and Mathematics Associate Dean: Lyn Kent Office: SEC 8125 Phone Number:918-595-8660 TO CONTACT ACADEMIC & CAMPUS SERVICES: Director: Leanne Brewer Office: SEC 2202 Phone: 918-595-7673 COURSE PREREQUISITES: Course Pre-requisite: CHEM 1415 - General Chemistry II COURSE DESCRIPTION: Organic chemistry I is a study of the fundamental concepts of organic structures and bonding, reactions of the principal organic functional groups, organic reaction mechanisms, and the nomenclature of hydrocarbons and their associated derivatives. The laboratory emphasis is on purification techniques, separation methods, organic synthesis, and various instrumental methods of studying and characterizing organic compounds and systems. NEXT COURSE IN SEQUENCE: CHEM 2245: Organic Chemistry II TEXTBOOKS, SUPPLIES, & OTHER RESOURCES: Title: Organic Chemistry Edition: 10th Authors: Graham Solomons and Craig B. Fryhle Publisher: John Wiley and Sons, 2009 Title: Organic Chemistry Laboratory Experiments for TCC-SEC Authors: Bill Briscoe & Toney Miller Publisher: Tulsa Community College Approved safety goggles, a lab coat or lab apron, and a bound notebook for the lab. COURSE OBJECTIVES: Learn the basic chemical principles that interrelate the structure with chemical and physical properties of organic compounds. Page 1 Rev 082007 Learn syntheses and reactions and their mechanisms for classes of organic compounds. Learn to synthesize, purify, and identify organic compounds in the laboratory. Learn how to communicate via report work performed in laboratory experiments. Learn the use of and interpretation of results obtained from organic laboratory instrumentation. Learn how the stereochemical properties of organic molecules affect their chemical and biochemical activity. TEACHING METHODS: The lecture portion of this class will be conducted in the classical lecture and discussion mode, including working of examples and problems. The student must read the lecture chapters and lab procedures before class to get the maximum benefit. The student must invest, at a minimum, an equal amount of time outside of class compared to in-class time to properly prepare and benefit from the course. Participation in class is strongly encouraged and will be a portion of the grading points. EVALUATION TECHNIQUES: Students will earn their grade in this course by accumulating points from the following sources: Four in-class examinations during the semester with 80 points possible on each total 320 points. Question types may be multiple choice, short answer, or problem solving. The examinations will cover the lecture material and suggested homework problems. Four take-home exams with same type of questions as in-class exams. Thirty points possible per exam. The exams can be completed only by students who pick up it up in class on the distribution date. In case of absence by unavoidable circumstances a copy of the exam may be obtained from the Academic and Campus Services office in Room 2202 if I am notified before midnight on the date the exam is distributed. The exam must be turned in by the student in person in class on the due date or no points will be awarded. Total points possible: 120. Suggested review homework problems are listed in Blackboard. Homework problems will be helpful in understanding textbook material but are not a part of the class point system. One comprehensive final exam worth 30 points. The final is mandatory and cannot be made up. The exam is written by a full-time instructor and is given to all CHEM 2145 students. Twelve lab reports with 25 points possible for eleven with one worth 35. The lowest grade will be dropped so points possible are 285. Laboratory Notebook : Possible 30 points, graded after last experiment. The notebook is for recording of lab data and will be signed off on by instructor each week after completion of the experiment. The notebook must be a bound composition –type notebook, not loose leaf or spiral. Only work recorded during the experiment in an approved notebook and signed off on by the instructor at the end of lab will receive credit. At the top of the first page of each experiment must be written the date and name of the experiment. Attendance and class participation – possible 25 points. One point deducted for each lecture not attended. Total possible points for the semester: 810 Extra Credit: 12 points Seven points will be awarded to each person who brings safety goggles to laboratory every week of the semester beginning the week of Experiment 1. Five points will be awarded for Page 2 Rev 082007 successfully sending in on Submit Here prior to Jan. 22 the sample laboratory report form. This submission demonstrates the capability to submit reports and negates any future claims of inability to get the system to work. If this submission is made late, no extra credit will be rewarded and the sample report must still be sent in before regular lab reports will be accepted for grading. GRADING SCALE: A = 90.0% - 100% D = 60.0% - 70.0% B = 80.0% - 89.9% F = below 60.0% C = 70.0% - 79.9% LABORATORY REPORTS: Reports will be due at midnight nine days after the date on which the experiment was performed. Reports, except for Lab #3: Infrared Spectrum, must be submitted on Blackboard through Submit Here using the report form furnished by the instructor or they will not be accepted. Reports submitted on paper will not be graded. If a submission problem is encountered on a personal computer the student cannot use it as an excuse to send in a report late or submit it in class on paper. The problem can often be corrected by switching to a different web browser or downloading the latest version of Java. Reports can be submitted successfully on Apple computers if .xls or .xlsx is added to the Excel file name. In the unlikely event that none of these measures solves the problem, the report can be submitted on one of the many computers available on all TCC campuses. Starting with Experiment 4 the infrared spectrums generated each week will be turned in at the end of the lab period. Points may be deducted for unsafe behavior observed in the laboratory or lack of participation in the experiment. There is no time budgeted to make up laboratory experiments so if you miss one you will not be able to earn any points for it. Late lab reports will be accepted up to one week after the scheduled turn-in date at a ten point reduction in grade. No report will be accepted past one week late. MAKE-UP EXAMS: Lecture exams can be made up only in the case of an emergency such as illness, death in the family, or work conflict. Illness or injury will require a doctor’s excuse. If an exam is to be made up it must be done within one week of the original test date in the Math Lab Testing Center during normal operating hours. If you miss a scheduled exam, it is your responsibility to email the instructor before midnight on the date of the exam to explain the absence. If a makeup is justified, the instructor will communicate with the student by email the next day to arrange for a makeup exam. LABORATORY PARTNERS: Some experiments, due to equipment and time limitations, will be done with students working in teams of two and reporting the same data. Prior to each week’s experiment, the instructor will designate whether work will be done individually or in pairs. Each partner must participate fully in the experiment or points will be deducted for nonparticipation. LABORATORY SAFETY: It is TCC school policy for students to wear a lab coat or lab apron, approved safety goggles (not safety glasses), and closed toe shoes at all times in the laboratory. No sandals may be worn. Low Page 3 Rev 082007 heels are preferred over high heels or platforms. Leather or vinyl shoes are preferred over cloth. The first time a student comes to lab without goggles, he/she will be allowed to borrow a pair and do the experiment without penalty. Failure to bring goggles to any future experiment will result in the student not being allowed to perform the experiment and receiving a zero for a grade. ATTENDANCE: Students are expected to attend every lecture and lab session. Attendance records will be maintained. Attendance and class participation will be taken into account in borderline grading situations. Material is necessarily covered at a rapid pace and it will be difficult to keep up if classes are missed. Concepts presented early in the course must be understood in order to understand material presented later on. COURSE WITHDRAWAL: Contact the Counseling Office at any TCC campus to initiate withdrawal from a course (W grade) or to change from Credit to Audit. Check the TCC Academic Calendar for the drop deadline. Students who stop participating in the course and fail to withdraw before the deadline may receive a course grade of F. Withdrawal, however, may have financial aid consequences for the student. COMMUNICATIONS: Email: All TCC students receive a designated “MyTCC” email address (ex: jane_doe@mail.tulsacc.edu). All communications to you about TCC and course assignments will be sent to your MyTCC email address; and you must use MyTCC email to send email to and receive email from the instructor regarding this course. INCLEMENT WEATHER: TCC rarely closes. If extreme weather conditions or emergency situations arise, TCC always gives cancellation notices to radio and television stations. This information is also posted on the TCC website (www.tulsacc.edu). GENERAL EDUCATION GOALS: General Education courses at TCC ensure that our graduates gain skills, knowledge, and abilities that comprise a common foundation for their higher education and a backdrop for their work and personal lives. TCC’s General Education goals are: Critical Thinking, Effective Communication, Engaged Learning, and Technological Proficiency. CLASSROOM ETIQUETTE: Lectures will be relatively informal with student comments and questions welcome; however, the student should keep in mind the effect of his/her behavior on others in the class and be considerate. Side conversations are distracting; if you have something to say or to ask it should be shared with the whole class. Cell phones must be turned off during class and placed out of sight off the desk in a place where no texting is possible. Texting is absolutely not allowed during lecture or homework problem sessions in the laboratory. The instructor cannot watch every student all the time during experiments so some texting will doubtless occur bit it should be kept to a minimum. Points will be deducted for the experiment if texting becomes excessive. If there is a family or work situation which requires the student to maintain contact, the ringer should be turned down and the student should step out of the room to take any calls. Laptop computers must remain closed during lectures. Page 4 Rev 082007 SYLLABUS CHANGES: Occasionally, changes to the syllabus may be necessary to meet the needs and available time of the class. Altered sections will be handed out in class. STUDENTS WITH DISABILITIES: TCC provides accommodations for qualifying students in compliance with the Americans with Disabilities Act. For information, students may contact the disabled Student Resource Center, 918595-7115, or the Resource Center for the Deaf and Hard of Hearing, 918-595-7428V, 918-5957434TTY. ACADEMIC DISHONESTY: Academic dishonesty (cheating) is defined as the deception of others about one’s own work or about the work of another. Academic dishonesty or misconduct is not condoned or tolerated at campuses within the Tulsa Community College system. The student should review the relevant sections of the TCC Student Code of Conduct Policy Handbook. Tulsa Community College adopts a policy delegating certain forms of authority for disciplinary action to the faculty. Such disciplinary actions delegated to the faculty include, but are not limited to, the dismissal of disrespectful or disorderly students from classes. In the case of academic dishonesty a faculty member may: Require the student to redo an assignment or test, or require the student to complete a substitute assignment or test; Record a "zero" for the assignment or test in question; Recommend to the student that the student withdraw from the class, or administratively withdraw the student from the class; Record a grade of F for the student at the end of the semester. Faculty may request that disciplinary action be taken against a student at the administrative level by submitting such a request to the Dean of Student Services. INSTITUTIONAL STATEMENT: Each student is responsible for being aware of the information contained in the TCC Catalog, the TCC Student Policies & Resources Handbook, and semester information listed in the class schedule. All information may be viewed on the TCC website: www.tulsacc.edu. COMPUTER SERVICES ACCEPTABLE USE: Access to computing resources is a privilege granted to all TCC faculty, staff, and students. Use of TCC computing resources is limited to purposes related to the College’s mission of education, research, and community service. Student use of technology is governed by the Computer Services Acceptable Use Statements/Standards found in the TCC Student Code of Conduct Policy Handbook. These handbooks may be obtained by contacting any Student Activities or Dean of Student Services Office. Page 5 Rev 082007 TENTATIVE COURSE CALENDAR: WEDNESDAY LAB Week EXAMS LABORATORY Homework Prob. Chapt. 1/10/11 Safety Film & Check In 1/17/11 (1) Physical Property Measurements (#1 in Briscoe & Miller) 1 1/24/11 (2) Partition Coefficients by Extraction (#3) 2 1/31/11 (3) Infrared Spectroscopy (#5) 3 2/7/11 (4) Open Column Chromatography (#7) 2/14/11 Exam I: Ch. 1-3 (5a) Isolation of Caffeine (#4) 2/21/11 (5b) Purification of Caffeine (#4) 4 2/28/11 (6) Synthesis of 1-Bromopentane (#9) 5 3/7/11 (7) Synthesis of t-pentyl Chloride (#10) 6 3/14/11 Spring Vacation: No classes 3/21/11 Exam II: Ch. 4-6 (8) Dehydration of an Alcohol (#11) 3/28/11 4/4/11 4/11/11 4/18/11 (9) Hydration of an Alkene (#14) 7 (10) Syn. and Purification of Aspirin (#15) 8 Exam III: Ch. 7 & 8 (11) Williamson Reaction of Ethers (#6) (12) HBr Cleavage of Ethers (#17) 4/25/11 Exam IV: Ch. 10 &11 5/2/11 Comprehensive Final Exam on Monday, 5/2 10 No Laboratory 11 Page 6