Angelina College Science and Mathematics Chemistry 1411L/1412L | General Chemistry Laboratory General Syllabus I. BASIC COURSE INFORMATION: A. Course Description: One-hour credit. Basic laboratory experiments supporting theoretical principles presented in CHEM 1311; introduction of the scientific method, experimental design, data collection and analysis, and preparation of laboratory reports. Co-requisite: CHEM 1411 lecture. Lab fee. B. Intended Audience: 1. This course designated for science majors, or for students with a major, which requires a four credit hour chemistry course beyond introductory chemistry. 2. Note: Do not confuse this course with CHEM 1305, Introduction to Chemistry. Both are “freshman” chemistry courses. Verify with your advisor that this is the appropriate course for your degree plan. II. INTENDED STUDENT OUTCOMES: A. Course Learning Outcomes for all Sections 1. Use basic apparatus and apply experimental methodologies used in the chemistry laboratory. 2. Demonstrate safe and proper handling of laboratory equipment and chemicals. 3. Conduct basic laboratory experiments with proper laboratory techniques. 4. Make careful and accurate experimental observations. 5. Relate physical observations and measurements to theoretical principles. 6. Interpret laboratory results and experimental data, and reach logical conclusions. 7. Record experimental work completely and accurately in laboratory notebooks and communicate experimental results clearly in written reports. 8. Design fundamental experiments involving principles of chemistry and chemical instrumentation. 9. Identify appropriate sources of information for conducting laboratory experiments involving principles of chemistry. III. ASSESSMENT MEASURES A. Assessments for Course Learning Outcomes 1. Students will demonstrate their ability to use basic apparatus and apply experimental methodologies used in the chemistry laboratory by physically performing assigned activities; answering directed questions during lab; answering questions assigned prior to, and following, the lab. 2. Students will demonstrate their ability to demonstrate safe and proper handling of laboratory equipment and chemicals, by physically performing assigned activities; answering directed questions during lab; and completing a quiz on the subject. 3. Students will demonstrate their ability to conduct basic laboratory experiments with proper laboratory techniques by physically performing assigned activities; answering directed questions during lab; answering questions assigned prior to, and following, the lab. 4. Students will demonstrate their ability to make careful and accurate experimental observations by submitting data sheets for critique; physically performing assigned activities; answering directed questions during lab; answering questions assigned prior to, and following, the lab. 5. Students will demonstrate their ability to relate physical observations and measurements to theoretical principles by providing a report for the relevant experiments; answering directed questions during lab; answering questions assigned prior to, and following, the lab. Updated 1/13/2015 1 6. Students will demonstrate their ability to interpret laboratory results and experimental data, and reach logical conclusions by providing a report for the relevant experiments; answering directed questions during lab; answering questions assigned prior to, and following, the lab. 7. Students will demonstrate their ability to record experimental work completely and accurately in laboratory notebooks and communicate experimental results clearly in written reports by providing a report for the relevant experiments; and by responding to directed questions. 8. Students will demonstrate their ability to design fundamental experiments involving principles of chemistry and chemical instrumentation by physically performing assigned activities; answering directed questions. 9. Students will demonstrate their ability to identify appropriate sources of information for conducting laboratory experiments involving principles of chemistry by providing a report for the relevant experiments which require information other than that immediately provided in the written procedure. IV. INSTRUCTIONAL PROCEDURES: A combination of in-class chemistry demonstrations, molecular models, laboratory demonstrations and supplemental information (both printed and digital) augment lecture presentations. Audio-visuals materials and Internet resources are also employed. V. COURSE REQUIREMENTS AND POLICIES: A. Required Textbooks and Recommended Readings, Materials and Equipment 1. Textbook: “Chemistry: The central science”, 13th Edition, by Brown, et al. (Pearson). 2. Mastering Chemistry access code. Supplied with text. (Pearson) 3. Lab Manual: CHEM 1411/1412 laboratory manual (provided at AC bookstore) 4. Access to BlackBoard (provided by AC) 5. Calculator capable of scientific notation 6. For exams: (a) “Scantron” forms and (b) #2 pencil B. Course Policies – This course conforms to the policies of Angelina College as stated in the Angelina College Handbook. 1. Academic Assistance – If you have a disability (as cited in Section 504 of the Rehabilitation Act of 1973 or Title II of the Americans with Disabilities Act of 1990) that may affect your participation in this class, you should see Karen Bowser, Room 208 of the Student Center. At a post-secondary institution, you must self-identify as a person with a disability; Ms. Bowser will assist you with the necessary information to do so. To report any complaints of discrimination related to disability, you should contact Dr. Patricia McKenzie, Administration Building, Room 105 or 936-633-5201. 2. Attendance – Attendance is required as per Angelina College Policy and will be recorded every day. Any student with three (3) consecutive absences of four (4) cumulative absences may be dropped from the class. Records will be turned in to the academic dean at the end of the semester. Do not assume that non-attendance in class will always result in an instructor drop. You must officially drop a class or risk receiving an F. This is official Angelina College Policy. Updated 1/13/2015 2 VI. COURSE OUTLINE: Description of the Course Activities including due dates, schedules, and deadlines. EXP # CHEMISTRY 1411 EXPERIMENTS/ACTIVITIES ASSOCIATED QUIZ Experiment 1 Check-in; safety & lab rules, dimensional analysis; Lecture Text CH 1.9 - 1.11 Experiment 2 Safety Quiz; Equipment Quiz; Density A Vernier Exp. 2 Freezing and Melting Points B Handout Worksheet over Chapters 1-3 Experiment 3 Gravimetric Detn of a Hydrate in a Mixture C Vernier Exp. 1 Calorimetry D Experiment 13 Preparations of Common Alum E Experiment 15 Chemical Periodicity of the Halide Ions F Experiment 23 Acid-Base Titrations G Experiment 10 I.D. Ten Inorganic Compds by Chemical Reactions H Experiment 14 Molecular Models I Experiment 20 Std. Molar Vol of Gas; Review for the Final Exam J Final Exam Checkout and Final exam Updated 1/13/2015 3 EXP # CHEMISTRY 1412-Lab EXPERIMENTS/ACTIVITIES ASSOCIATED QUIZ Check in; safety rules; nomenclature VII. Experiment 9 Some reactions of metal ions A Vernier Exp. 15 Freezing point depression Handout Thermodynamic problem solving (BRING TEXTBOOK) B Vernier Exp. 18 Hess's Law C Experiment 29 Factors which influence rates of reactions D Vernier Exp. 30 Rate law determinations E Experiment 31 Chemical equilibrium -- Introduction F Vernier Exp. 20 Chemical equilibrium -- Kc G Experiment 22 Acid-base titration curves, Part I H Text Ch. 11.5-11.8 Balancing Redox Rxns (BRING TESTBOOK) Experiment 25 Voltaic and electrolytic cells, Part I; , Part I; Final Exam Review Final Exam Checkout; Lab final I EVALUATION AND GRADING: A. Grading Criteria Course grades are assigned in light of a numerically-determined course score (see subsection "B" for details), according to the following table: COURSE SCORE COURSE GRADE 90–100 A 80–89 B 70–79 C 60–69 D Below 60 F Updated 1/13/2015 4 B. Overall Course (CHEM 1411/CHEM 1412) Score will be determined according to the following percentages: 1. 25% from the Final Exam; 45% from the average of Exams 1,2, and 3; 25% from the Laboratory score (see subsection "C" for details); and 5% from the assigned on-line homework ("OWL") 2. The four components are weighted according to the equation: Course Score = 0.25 (Final Exam Score) × 0.45 (average of all midterm exams) × 0.25 (Laboratory Score) × 0.05 (OWL on-line homework score) C. Overall Laboratory Score (a component of the overall Course Score) 1. 80% from the average score of the assigned laboratory experiments (see section "D" for details); 20% from the written laboratory final exam. 2. The two components are weighted according to the equation: Laboratory Score = 0.80 (average of individual experiments score) × 0.20 (laboratory Final Exam Score) D. Scoring of Individual Experiments 1. A student must be physically present during the laboratory period, and actively participate in the experiment, to receive credit for any of the scored components, which follow. 2. 30% from the on-line pre-lab quiz; 70% from the experiment Report, demonstrated in-lab performance/participation, and post-lab questions. 3. The two components (pre-lab quiz and "Report') are weighted according to the equation: Individual Experiment Score = 0.30 (on-line quiz score) × 0.70 (report & participation score) 4. NOTE: if a particular lab experiment is not physically attended, then the total score for that experiment is set to zero. The net result is that the on-line quiz score, the report and participation score, and the post-lab questions score are scored at zero: any scores or materials provided are disregarded. 5. NOTE: if you are asked to leave the lab, that lab will be scored a zero, and it will NOT be available as a candidate for a "dropped" lab. The zero will be averaged into your final laboratory score. 6. NOTE: on occasion, and with permission of each of the professors involved, you may be allowed to attended a different lab section, rather than miss an experiment altogether. This will be allowed a maximum of two times per semester. Note that both professors must agree AND be notified via email, which serves as written documentation of the change. E. Make-up Labs 1. For labs without experiments, a Worksheet will count as the lab grade. 2. There will be NO make-up labs; however, one individual experiment grade will be dropped. 3. Missed lab counts as a “zero.” 4. If you are asked to leave a lab, that lab will necessarily be scored as a zero, and that score will not be eligible to serve as the "dropped" experiment grade. 5. No student will receive credit for a lab, which he/she did not both attend and participate. The instructor may modify the provisions of the syllabus to meet individual class needs by informing the class in advance as to the changes being made. Updated 1/13/2015 5