Effect Of Temperature & Strain Rate On Flow Properties 1 • The stress-strain curve and the flow and fracture properties of a material are strongly dependent on: - strain rate - temperature at which the test was conducted. • In general strength decreases and ductility increases as: - strain rate is decreased, or - the test temperature is increased. 2 Figure 2-1. Yield strength changes as a function of (a) temperature and (b) strain 3 Figure 2-2. Effect of strain rate and temperature on stressstrain curves. 4 Figure 2-3. Changes in engineering stress-strain curve of mild steel with temperature. 5 • This general behavior may not take place in certain temperature ranges if structural changes such as precipitation, strain aging, or recrystallization occur. • The above thermally activated processes can assist deformation and reduce or increase strength at elevated temperatures. • When materials are deformed at high temperatures and/or long exposure, structural changes can occur resulting in time-dependent deformation or creep. 6 Figure 2-4. Effect of temperature on the yield strength of bodycentered cubic Ta, W, Mo, Fe, and face-centered cubic Ni 7 Note • For the bcc metals (see Fig. 2.4), the yield stress increases rapidly with decreasing temperature. • For Ni and most fcc metals, the yield stress is only slightly temperature dependent. • Fig. 2.4 can also be used to understand why most bcc metals exhibit brittle fracture at low temperatures. • A comparison of the flow stress of two materials at elevated temperature requires a correction for the effect of temperature on Elastic Modulus. 8 • The temperature dependence of flow stress at constant strain and strain rate can be given by: Q C2 exp RT , 2-1 where Q is the activation energy for plastic flow, C2 is a constant, T is the testing temperature and R is the universal gas constant • A plot of ln versus 1/T will give a straight line with a slope Q/R • The activation energy Q can be determined by performing two tensile tests at two temperatures, T1 and T2 and at a constant strain rate. 1 T1T2 Q R ln 2 T2 T1 2-2 9 • Equation 2.1 can also be written as: f Z f exp( H RT ) 2-3 where H is an activation energy (calorie per mole). It is related to the activation energy of Eq. 2.1 by Q = m H, where m is the strain rate sensitivity. • Z is the Zener-Hollomon parameter or temperature-modified strain rate. Z exp H RT 2-4 10 • The above equation can be written in a different form for hotworking conditions: A(sinh ) n ' exp Q RT 2-5 where A, , and n’ are experimentally determined constants • At low stresses ( < 1.0), Eq. 2.5 reduces to: A1 n ' exp Q RT 2-6 The power law equation (Eq. 2.6) can be used to describe creep, and superplasticity to some extent. 11 • At high stresses ( > 1.2), Eq. 2.5 reduces to: A2 exp(n' ) exp Q RT 2-7 The constants and n’ can be determined from tests at high and low stresses. 12 Strain Rate Effects • Lowest range of strain rates Creep and Stress Relaxation • Intermediate range 10-4 < < 10-2 Hot working/Tensile test • Highest range shock wave or explosive test • Stress-strain curves can be sensitive to strain rate – flow stress increases with strain rate – work hardening rate may also increase with strain rate 13 • Two parameters used to describe the above effects are: - Strain rate sensitivity (m), and this is given as: and ln m ln (2.8) ,T ln w s ln ,T where d w d ,T (2.9) 14 • Equations 2.8 and 2.9 can be expressed as m K (2.10) d ' s K d (2.11) • It is possible to determine m from tensile tests by changing the strain rate suddenly and by measuring the instantaneous change in stress. This technique is illustrated in Fig. 2.5. 15 Figure 2-5. Strain-rate changes during tensile test. Four strain rates are shown: 10-1, 10-2, 10-3, and 10-4s-1. 16 • Applying Equation 2.10 and 2.11 to two strain rates and eliminating K, we have: ln 2 / 1 m ln 2 / 1 (2.12) • One can easily obtain m from the strain rate changes in Figure 2-5 • The parameter m is important in accessing the superplasticity of materials 17 Constitutive Equations • Describe the relations between stress and strain in terms of the variables of strain rate and temperature • Early concept: f(,,,T) = 0 – Analogous to equilibrium in thermodynamics system which states that: f(P, V, T) = 0 • There are several forms of constitutive relations, including the simple power law relation (Hollomon equation) and it’s variants. 18 Other Examples of Constitutive Relations • = f(Z) = f(eH/RT) (2.3) where Z is called the Zener-Hollomon parameter, H is an activation energy (calorie per mole), of which Q = m H • = A(sinh)n` e-Q/RT (2.5) where A, , and n` are experimentally determined constants 19 Constitutive Relations (cont) • At low stresses ( < 1.0) : n ' Q / RT A1 e (2.6) where A, , and n` are experimentally determined constants. • At high stresses ( > 1.2), and the equation reduces to: A2 exp( )e Q / RT (2.7) The constants and n` are related by = n` 20 Figure 2-6. Stress-strain curves for AISI 1040 steel subjected to different heat treatments; curves obtained from tensile test. 21