Cabbage Juice Titration Lab Introduction: Red cabbage juice is an example of an acid-base indicator. In chemistry, an indicator is used to detect the presence of a specific chemical or a specific type of chemical. In this lab, red cabbage juice is used to indicate whether a solution is acidic or basic. Red cabbage contains the pigments flavonol and anthocyanin. The anthocyanin pigment causes very strong acids to appear red. It causes neutral or weak basic solutions to appear blue, and strong basic solutions to appear colorless. Flavonol, on the other hand, causes strong acidic solutions to appear colorless and strong basic solutions to appear yellow. The following chart shows the correlation between the color of a solution that contains red cabbage indicator and pH. In this lab, you will use cabbage juice as an indicator during titrations. COLOR pH RED CABBAGE INDICATOR COLORS WITH pH VALUES RED VIOLET PURPLE BLUE GREEN 1 2 Strong acid 3 4 Medium acid 5 6 Weak acid 7 neutral 8 YELLOW 9 10 11 12 Weak Medium base base 14 Strong base Materials: several leaves of red cabbage, strainer, pot filled with enough water to cover cabbage leaves, vinegar, baking soda, measuring cup and spoons, eye dropper, and one clean clear jar Procedure: Red Cabbage indicator: 1. Cut several leaves of cabbage into small pieces and place them in the pot with enough water to cover the leaves. 2. Boil the mixture for 20-30 minutes, until the liquid turns a dark purplish color. 3. Add more water if you think the mixture will boil dry before it turns dark purple. © 2010 Connections Education LLC. All rights reserved. 13 4. Transfer the fluid into a glass or jar, pouring it through a strainer to remove the cabbage pieces. Using cabbage juice as an indicator during titration: 1. 2. First you need to calibrate your eyedropper. Figure out how many drops of water are in 1/8 of a teaspoon. Multiply that number by 8 to obtain the number of drops per teaspoon. # of drops/tsp = 96 3. 1 teaspoon is equal to 4.93 mL. Divide the number of drops per teaspoon by 4.93 to obtain the number of drops per ml. You will use this ratio to convert number of drops to mL when you perform your calculations. # of drops/mL = 19.5 4. Next, combine 1 teaspoon of vinegar with ½ tablespoon of red cabbage indicator in a small container and set it aside. This solution is to be used for comparison when you perform your titration. 5. Combine 1 teaspoon of water with ½ tablespoon of red cabbage indicator in a separate container and set it aside. This solution will also to be used for comparison when you perform your titration. This should be the same color as the indicator. 6. Next, mix 4¾ level teaspoons (28.35 g or 1 oz) of baking soda with 1¼ cup (295.74 ml) of water in a small container and set it aside. This will give you a solution with a concentration of 1.14 M. 7. Combine 1 teaspoon of the baking soda solution with ½ tablespoon of red cabbage indicator in a small container and set it aside. This solution can be used for comparison. Should be a blue/turquoise color. 8. Transfer 2 teaspoons (9.86 ml) of vinegar into a clean clear jar. 9. Add 1 tablespoon of cabbage juice to the clear jar that contains the vinegar. (Should be a red/pink color) 10. Use the eye dropper to add the sodium bicarbonate to the vinegar one drop at a time. Keep track of the number of drops you add. © 2010 Connections Education LLC. All rights reserved. 11. Don’t forget to swirl the mixture after every couple of drops. 12. When a permanent light purple color change is apparent the end point has been reached. If it starts turning blue you have gone too far. 13. If it looks like the water solution created in procedure 5, you have added too much NaHCO3. 14. Record the total number of drops of the sodium bicarbonate solution you added to the vinegar in the Data Table. 15. Repeat step 7–13 two more times so that you will have completed 3 titrations. 16. Use the average number of drops used to cause the reaction to reach an endpoint for your final calculations. 17. Complete a formal lab report. Your report should include a heading, an introduction explaining the purpose of the lab, all data collected during the lab, and answers to the questions below. Be sure to first type the question then the answer it. Data Table: # Trial # of drops of NaHCO 3 Volume of NaHCO (mL) 3 1 142 7.28 Volume of CH COOH (mL) 3 9.86 ml 2 145 7.44 9.86 ml 3 139 7.12 9.86 ml average 142 7.28 9.86 ml © 2010 Connections Education LLC. All rights reserved. Questions: 1. Write the balanced equation for the reaction of acetic acid ( CH COOH ) and sodium bicarbonate ( NaHCO ). What type of 3 3 reaction(s) took place? 2. Calculate the number of moles of NaHCO that were required to 3 neutralize the CH COOH in the vinegar. 3 3. Calculate the molarity of the vinegar sample. (Don’t forget to convert mL to L.) 4. Calculate the number of grams of CH COOH in the vinegar. 3 5. Calculate the percent of acetic acid in the vinegar. (The density of vinegar is 1.002 g/ml.) 6. Is it possible for the equivalence point of a titration to not be at pH 7? Explain your answer. 7. What is the molarity of a CsOH solution if 30.0 mL of the solution is neutralized by 26.4 mL 0.25 M HBr solution? © 2010 Connections Education LLC. All rights reserved.