Set No. 1 Code No: RR310805 III B.Tech I Semester Supplimentary Examinations, February 2008 PROCESS INSTRUMENTATION (Chemical Engineering) Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ⋆⋆⋆⋆⋆ 1. What are the different elements of a measuring instrument? Describe in detail.[16] 2. (a) How is the radiant energy measured? Explain with a neat sketch. (b) Write short notes on Black body Radiation. [8+8] 3. (a) Describe the construction and working of an infrared absorption spectrometer with a figure. (b) Explain the method of finding concentration of a component from a spectrogram. [8+8] 4. (a) Describe the dew point method of measurement of absolute humidity. (b) Write the principle of gas analysis by thermal conductivity. [8+8] 5. (a) Explain with the help of neat sketches, the working principles of electric pressure gages. (b) Mension the useful ranges of absolute for pressure measuring gauges. [10+6] 6. (a) How the level measurement in pressure vessels is carried out. (b) Explain diaphragm box system for liquid level measurement. [8+8] 7. (a) Name the two types of pitot tubes. Explain their construction and operation with figures. (b) State the advantages of a pitot tube in measurement of flow of fluids. [8+8] 8. (a) Show how an orifice is connected in a pipe line through diagrams for the measurement of flow rate of i. Steam ii. Corrosive gas. (b) Explain how viscosity compensation is provided in rotameters with appropriate sketches. [8+8] ⋆⋆⋆⋆⋆ 1 of 1 Set No. 2 Code No: RR310805 III B.Tech I Semester Supplimentary Examinations, February 2008 PROCESS INSTRUMENTATION (Chemical Engineering) Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ⋆⋆⋆⋆⋆ 1. What are the different elements of a measuring instrument? Describe in detail.[16] 2. Discuss the factors which influence the speed of response of a thermocouple. [16] 3. What are the basic differences between atomic emission and atomic fluorescence spectroscopy? Why is source modulation often emplyed in atomic absorption spectroscopy? [16] 4. (a) Describe the dew point method of measurement of absolute humidity. (b) Write the principle of gas analysis by thermal conductivity. [8+8] 5. With a neat diagram explain the constructional features and the working with the circuitry of a thermocouple (thermal type) vacuum gauge [16] 6. (a) Describe a method for continuously measuring specific gravity of liquids. (b) Explain with a neat diagram the pneumatic balance displacement float liquid level meter. [6+10] 7. An orifice meter equipped with flange taps is to be installed to measure the flow rate of crude oil to a cracking unit . The oil is flowing at 380 c through a 10 cm pipe. The maximum flow rate of oil is 80 m3 /h . Mercury is used as manometer liquid and glycol is used as sealing liquid in the leads. Calculate (a) the diameter of orifice and (b) power loss. The power loss Data: Density of mercury =13600 kg/m3 Density of glycol = 1100 kg/m3 Reading of the manometer = 0.76 m Discharge coefficient = 0.61. The power loss and β are correlated by equation power loss = mβ + C. It is given that at β=0.4, power loss is 0.81 and at β=0.6, power loss = 0.62 [8+8] 8. It is desired to draw the instrumentation diagram for a jacketed CSTR with temperature control of exothermic reaction. Present a detailed analysis of the procedure step wise for the construction of the diagram and then draw the diagram. [16] ⋆⋆⋆⋆⋆ 1 of 1 Set No. 3 Code No: RR310805 III B.Tech I Semester Supplimentary Examinations, February 2008 PROCESS INSTRUMENTATION (Chemical Engineering) Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ⋆⋆⋆⋆⋆ 1. What are the different elements of a measuring instrument? Describe in detail.[16] 2. (a) Draw the temps in a thermocouple circuit. Discuss the methods of selecting the Thermo Couple lead wires. (b) What are the properties which must be considered in the selection of a thermal well. [10+6] 3. Why is composition analysis required in a process industry? Write briefly on the qualitative and quantitative measurements with suitable examples. Highlight about positive methods of composition analysis. [16] 4. Describe the method of estimation of SO2 in industrial effluent gas. [16] 5. With a neat diagram explain the constructional features and the working of a Bulk Modulus pressure gauge to measure high pressures [16] 6. (a) Describe air trap system for liquid level measurement. (b) Explain bubbler system for liquid level measurement with a neat diagram. [8+8] 7. A solution having specific gravity 1.15 is flowing through a 75mm diameter pipe at a flow rate of 800litres/min. A sharp edged orifice connected to a simple mercury manometer is installed to measure the flowrate. If the manameter shows a reading of 40cm, what would be the orifice diameter?Assume orifice coefficient as 0.61.[16] 8. Discuss briefly the classification of methods of chemical analysis adopted in a process industry. Highlight their unique features. [16] ⋆⋆⋆⋆⋆ 1 of 1 Set No. 4 Code No: RR310805 III B.Tech I Semester Supplimentary Examinations, February 2008 PROCESS INSTRUMENTATION (Chemical Engineering) Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ⋆⋆⋆⋆⋆ 1. (a) Discuss the principle, working and applications of a bimetallic thermometer. (b) What is meant by order of instrument? [10+6] 2. (a) Explain with a neat sketch the operation of a self balancing potentiometer used for measuring thermocouple signals. (b) Discuss its advantages over the direct reading millivoltmeter. [10+6] 3. Explain the principles of operation of a non-destructive analyser (NMR) for product indentification in petrochemical industries. [16] 4. What is humidity? Explain its importance. Describe how moisture in fibre materials is measured by infra-red transmission technique. [16] 5. (a) On what factors the selection of a material depends for the fabrication of a pressure measuring gauge (b) With a neat diagram explain the working of a Differential pressure Pneumatic Transmitter working on a null-balance vector principle [6+10] 6. (a) Describe in detail the level measurement in pressure vessels. (b) Write about displacement meter for measuring specific gravity with a neat diagram. [8+8] 7. Describe the working principle of a V-notch and its applications. Obtain the equation used to find the flowrates using weirs. [16] 8. Discuss briefly the classification of methods of chemical analysis adopted in a process industry. Highlight their unique features. [16] ⋆⋆⋆⋆⋆ 1 of 1