TEACHER GUIDE Mixtures & Separation Techniques MIXTURES AND SEPARATION TECHNIQUES Overview Now that students have been presented with their challenge from SILA YOUTH and have learned how to identify between physical and chemical changes, they need to expand their knowledge to include mixtures and separation techniques. This is the last step before they will have to create their own protocol, run their experiment and report their results and recommendations. In this activity, students will be looking at the differences between pure substances and mixtures. They will then gain a better understanding of some separation techniques such as filtration and distillation. Once they have been exposed to these concepts, they will use their knowledge to purify a mock contaminated water sample. Subject: Science and Technology World(s) Material World Disciplinary Competencies Competencies Components C1. Seeks answers or solutions to scientific or technological problems. Cr.3. Appropriate implementation of the procedure. C2. Makes the most of his/her knowledge of science and technology Cr.3. Relevant explanations or solutions. Page 2 Level: Secondary 1.1 MIXTURES AND SEPARATION TECHNIQUES Prior Knowledge: Science Prior Knowledge: Math Using a graduated cylinder Links to Math None Vocabulary Decantation Dilute Distillation Distillate Filtrate Filtration Pure substances Purification Heterogeneous mixture Homogeneous mixture Immiscible Insoluble Materials needed Sedimentation Soluble Solution Solvent Suspension Turbidity Duration 5 X 45 minute periods Breakdown None RECAP (5-10 minutes) THE SITUATION (5-10 minutes) EXPERIMENT (10-15 minutes) TEACHER DIRECTED NOTES (20-30 minutes) EXPERIMENT (45-90 minutes) ANALYSIS (30 minutes) REFLECTION ACTIVITY (10-15 minutes) REVIEW QUESTIONS (20-25 minutes) EVALUATION Page 3 Filter funnel Filter paper Retort stand Clamp Beakers Hot plate Contaminated water sample Flask Rubber stopper with a hole Anti-bump granules Glass tubing MIXTURES AND SEPARATION TECHNIQUES DEFINITION OF TERMS Decantation Dilute Distillation Distillate Filtrate Filtration Heterogeneous mixture Homogeneous mixture Immiscible Insoluble Pure substances Purification Sedimentation Soluble Solution Solvent Suspension Turbidity Decantation: To pour a liquid from one container into another Dilute: To make thinner or less concentrated by adding a liquid such as water Distillation: The evaporation and subsequent collection of a liquid by condensation as a means of purification Distillate: A liquid condensed from vapor in distillation Filtrate: Material, especially liquid, that has passed through a filter Filtration: The act or process of filtering, especially the process of passing a liquid or gas, such as air, through a filter in order to remove solid particles Heterogeneous mixture: Is a type of mixture in which the components can easily be identified, as there are two or more phases present Homogeneous mixture: A type of mixture in which the composition is uniform Immiscible: Two or more liquids incapable of being mixed to form a homogeneous substance Insoluble: Incapable of being dissolved; incapable of forming a solution, especially in water Pure substances: A sample of matter, either an element or a compound, that consists of only one type of particle Purification: The act of cleaning by getting rid of impurities Sedimentation: The formation of a deposit in a liquid by the setting out of suspended materials. Soluble: Capable of being dissolved, especially easily dissolved in some solvent, usually water Solution: a homogeneous mixture of two or more substances Solvent: A substance in which another substance is dissolved, forming a solution Suspension: A mixture in which small particles of a substance are dispersed through a gas or liquid. If a suspension is left undisturbed, the particles are likely to settle to the bottom Turbidity: Having sediment or foreign particles stirred up or suspended; muddy Page 4 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 5-10 minutes. The goal of this part of the activity is for students to work autonomously and find the answers to the questions. If students are having difficulty with this, they can use their notes from previous years, their textbook or any other available resources. Permanent colour change After they have recorded their answers, you can ask individual students to share their answers. A gas is produced Formation of a precipitate These are review questions from the previous activity on physical and chemical changes. Heat or light produced QUESTION 2. Answers Answers are on the right side of the page. A. B. C. D. E. F. G. H. I. J. Page 5 P C P P P C P P C P MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 5-10 minutes. This will be the introduction to the “Teacher Directed Notes” section. Before starting this activity take the time to review the following with the students: - The Mine Clean-Up undertaken by the Quebec government and Makivik, - The creation of SILA YOUTH to address this problem, - The contaminated mine sample to be evaluated and processed - The report the student will have to put together. - What the students have discovered in their last activity on physical and chemical changes. Once that has been completed, you can present “The Situation” to the students using the following or other ESL strategies: - Read the stories and questions orally to the students one at a time. - Have each student read the stories silently. - Have the students read silently, pair up and explain the stories to their partner. - Choral reading. The best practice is to use more than one of the suggested strategies. Page 6 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 10-15 minutes. Setting the scene for the experiments to come. Read the “I Observe” section to the students. To make it more theatrical, you can to bring in different types of mixtures to show the difference between homogeneous and heterogeneous mixtures (mixed cake batter, oil & vinegar, soup, salad, etc). This visualization will help the students remember the concept. This might be an ideal time to review the terms from the word wall and the supplementary notes on separation techniques. If possible, demonstrate each of the separation techniques while reinforcing the proper names for the lab equipment and the proper methods to set-up apparatus. Page 7 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: Continued from previous section. Read the “I Develop a Research Question” and the “I Define the Variables” section to the students. To help the students with recording their results, read and clarify the items on the data table (page 13 of the Student Booklet) so that they are clear as to how to respond and record results. The experiments will take 1-2 classes to complete. They can be divided into two sets of experiments to make them more achievable in a 45 minute period. Students can work individually or in groups on the labs. If you choose individual lab groups, a lot more consumable materials will be required. For each lab, you should encourage the students to read the lab directions prior to conducting the experiments. To avoid confusion, only one lab should be conducted at a time. The foundation has now been laid for the “Teacher Directed Notes”. Page 8 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 20-30 minutes. MATTER Pure Substance Mixtures Heterogeneous You should start with having the students complete the pure substance and mixtures graphic organizer. If you want to make this activity more interactive, provide the class with a list of words to be used and allow the students time to fill in the blanks. Their answers can then be shared with the class. Homogeneous Before labeling the two diagrams of particles, go over the definitions for “Homo” and “Hetero”. Once this has been completed, allow the students to try to figure out which container is which. Homogeneous Heterogeneous If you are using examples of different types of solutions, this would be a good opportunity to visually show the differences between homo and hetero solutions. It is Greek in origin and means "same". It is Greek in origin and means "the opposite". The document “Pure Substances, Mixtures & Separation Techniques” covers all of the topics in the TEACHER DIRECTED NOTES section in greater detail. Page 9 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Pure substance Duration: Continued from previous section. Mixture A sample of matter, either an element or a compound, that consists of only one type of particle. Pure Substances: When reviewing pure substances, refer to the periodic table of elements. An example of a pure substance with two or more particles would be distilled water. o A possible demonstration comparing properties of tap water versus distilled water. Homogeneous Distilled Water pH of 7 density of 1 g/ml does not conduct electricity Heterogeneous A type of mixture in which the composition is uniform, There are different particles in the mixture but the particles cannot be differentiated A type of mixture in which the components can easily be identified, as there are two or more phases present Tap Water pH range of 6 - 8.5 density of 0.99999 g/ml poor conductor of electricity Homogeneous Mixtures: Demonstrate how salt (or sugar) can easily dissolve in water – creating a homogeneous mixture. Use this salt-water solution to also demonstrate the terms solute, solvent and solution. (showing solubility) Keep the solution you use when demonstrating distillation ( the salt and water separate and become two different types of particles) Heterogeneous Mixtures: Demonstrate how sand and water cannot be easily dissolved in water – creating a heterogeneous mixture. Use this sand and water mixture to demonstrate insoluble. Use oil and water or oil and vinegar to demonstrate immiscible Page 10 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: Continued from previous section. When solid substances that are heavier then water particles deposit or collect at the bottom of the container they form sediment. To pour a liquid from one container into another Sedimentation: Slow but Sure • When solid substances that are heavier than water particles deposit or collect at the bottom of the container they form sediment. • E.g. Orange juice, Salad Dressing, sand and ocean water. Sedimentation: Using a sand and water mixture demonstrates sedimentation. Place this mixture in a container, shake it and then watch the sand (sediment) collect at the bottom of the container. Demonstrate the above situation with the oil and water or oil and vinegar mixture. Decantation: from one container to another • It is often used after sedimentation. • A heterogeneous mixture that has layers can be separated into distinct substances. Decantation: When decanting from one container to another, it is important to be careful to not agitate the sediment. A glass rod may be used to help decant. Page 11 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: Continued from previous section. The act or process of filtering, especially the process of passing a liquid or gas, such as air through a filter in order to remove solid particles The evaporation and subsequent collection of a liquid by condensation as a means of purification Filtration: Fast and Effective • Separates different substances of a heterogeneous mixture using a barrier device (e.g. Filter paper). • E.g.: Vacuum Filtration: Demonstrate the proper way of folding filter paper to fit in funnel. Can use orange juice (with pulp) or coffee grains and a percolator Distillation: Separating the invisible • Uses the substance’s boiling point. • When the water boils it is condensed and collected in a separate holding device. • Once this pure water is obtained it is called the distillate. • The solid particles that are left behind in the original container are called the residue Any other notes you deem necessary. Distillation: (use salt-water solution) When demonstrating distillation, it is very important to stress proper safety with equipment. Turn off the heat when the water level is low – if you wait too long then the salt will burn at the bottom of the flask Review the states of matter o When the water in the solution reaches the boiling point, it turns into vapour (gas) then cools while travelling along the rubber tube and becomes water again in the collecting beaker. During demonstration review terms such as distillate, residue, etc Page 12 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 45-90 minutes. Experiment 1: Filtration Before beginning the lab, discuss the properties of the “contaminated water” mixture and fill-in the chart with the results. - Review the terms discussed in the results chart (e.g. turbidity) Put possible answers on the board for students to use when filling in the results table Make sure students keep the filtrate and enter their observations in the result table before moving on to Experiment 2. The contaminated water sample can be made in a variety of ways. The most basic one would be to dissolve 10-15 grams of table salt in 100 ml of tap water and then add approximately 25 ml of sand. Many other solutions are possible. You have full autonomy here to make your own as long as the resulting mixture can be separated by filtering and distillation. Oatmeal can also be used in addition to or instead of sand. For more advanced students, oil could be added to the contaminated water sample so that an additional step of decantation could be added. Page 13 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: Continued from previous section. Experiment 2: Distillation The students will use the filtrate collected from experiment 1. If the lab is to be completed on different days, the samples can be refrigerated. Anti-bump granules - Anti-bumping granules are small, irregularly shaped stones added to liquids to make them boil more smoothly. Without granules, a liquid heated in a smooth container can become superheated and release vapour suddenly, sometimes violently. This sudden bubble of gas can cause the solution and reagents to be thrown out of the container, possibly causing severe burns, ruining an experiment, or simply making a mess. Anti bump granules are typically made of porous material such as alumina, calcium carbonate, porcelain or carbon, and often have a nonreactive coating of PTFE (Teflon) Remind students to complete the result chart before and after distillation. Page 14 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: Continued from previous section. Experiment 1: Filtration Results may vary slightly depending on how early the “contaminated water” mixture was prepared. The more times the oatmeal has to soak the better the results Properties Before Filtration After Filtration Colour of solution Cloudy/White Less Cloudy High Low Many Particles Little to no Particles Turbidity (high or low) Presence of suspended particles Experiment 2: Distillation For further enrichment students may test the properties of the distillate to compare it with the properties of water. Properties Colour of solution Turbidity (high or low) Presence of suspended particles Page 15 Before Distillation Slightly Cloudy After Distillation Colourless/Clear Low Low/None Little to no Particles No Particles MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 30 minutes These questions can be completed individually or in groups. The water is not pure. Only the sediment (solid) was removed. Some small particles can still be seen in the Sample. As enrichment or with the class, test the proposed explanations given in the analysis questions. As an enrichment activity, write the question below for students to answer by researching or providing a thorough opinion The water is pure. The last of the solute remained in the flask. Only the water was evaporated and collected in the beaker. “Can distillation be done on a large scale (i.e. a lake or river)?” Filtration Distillation Page 16 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 10-15 minutes. This section can be completed as homework if time does not permit the work to be completed during class time. These questions should be completed individually by the students. ANSWERS: a. I think that the best method to remove large floating particles is ___FILTRATION_____ (sedimentation, filtration, decantation, distillation). These particles are said to be __INSOLUBLE____ (insoluble, soluble, immiscible, in suspension). b. ___DISTILLATION____ (sedimentation, filtration, decantation, distillation) may remove invisible particles. These particles are said to be ___IN__ _SUSPENSION_ (insoluble, soluble, immiscible, in suspension) in water. c. For example: The pulp in orange juice and the spices in Italian salad dressing could be separated using ___FILTRATION____ (sedimentation, filtration, decantation, distillation). d. The sugar in maple syrup and the minerals in sea water could be separated using ___DISTILLATION____ (sedimentation, filtration, decantation, distillation). Page 17 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: 20-25 minutes. This section can be completed as homework if time does not permit the work to be completed during class time. These questions should be completed individually by the students. ANSWERS: 1. D 2. A 3. B 4. C Page 18 MIXTURES AND SEPARATION TECHNIQUES Teaching Strategy: Duration: Continued from previous section. ANSWERS: 1. G 2. D 3. E 4. B 5. A 6. F 7. C 8. H 9. K 10. J Page 19 MIXTURES AND SEPARATION TECHNIQUES Resources Documents Videos “Pure Substances, Mixtures & Separation Techniques Notes” Word or PDF None Explorations Textbook A B 197-205 195-201 Facile Learning For Further Reading / Additional Resources Links Evaluation Previous activity: Other None Observatory Textbook OTHER 9-21 Not applicable Lesson 3 – Topic 1 Various science textbooks Wikipedia: http://en.wikipedia.org/wiki/Main_Page http://fr.wikipedia.org/wiki/Wikip%C3%A9dia:Accueil_principal An evaluation section is included at the end of this booklet. An additional evaluation sheet is also available which includes a student evaluation portion. Mixtures and Separation Techniques Page 20 Next activity: Mine Clean-Up MIXTURES AND SEPARATION TECHNIQUES Flow chart of activities for the Mine Clean-Up LES BLOCK B: Physical & Chemical Changes Mixtures & Separation Techniques Page 21 Mine Clean-Up MIXTURES AND SEPARATION TECHNIQUES 4 2 1 Respects the safety rules without prompting most of the time. Only needs to be reminded of minor issues such as hair being tied back. Respects the safety rules most of the time. Only needs to be reminded once. Respects the safety rules only when prompted by the teacher, numerous times (2 or more). Does not respect the safety rules at all. Works independently and correctly fills in 4-5 squares. Works independently and correctly fills in 3 squares. OR With help from the teacher, is able to correctly fill in all 6 squares. Works independently and correctly fills in 2 squares. OR With help from the teacher, is able to correctly fill in 35 squares. Works independently and correctly fills in 1square. OR With help from the teacher, is able to correctly fill in 12 squares. Works independently and correctly fills in 4-5 squares. Works independently and correctly fills in 3 squares. OR With help from the teacher, is able to correctly fill in all 6 squares. Works independently and correctly fills in 2 squares. OR With help from the teacher, is able to correctly fill in 35 squares. Works independently and correctly fills in 1square. OR With help from the teacher, is able to correctly fill in 12 squares. The student respects safety rules. The student makes useful observations. Data table, Experiment 1. Student Book, page 13. The student makes useful observations. Data table, Experiment 2. Student Book, page 13. Always respects the safety rules without prompting. Works independently and correctly fills in all 6 squares. Works independently and correctly fills in all 6 squares. Page 22 Teacher notes COMPETENCY 1 Seeks answers or solutions to scientific or technological problems Cr.3. Appropriate implementation of the procedure. Criteria Score Competency Average 3 Traces 5 Traces Competencies and Evaluation Criteria Observable Evaluation: MIXTURES AND SEPARATION TECHNIQUES 4 3 2 1 Works independently and comes up with 1 out of 3 points OR With help from the teacher, is able to come up with 2 out of 3 points. Works independently and comes up with an answer that links to the situation OR With help from the teacher, is able to come up with 1 out of three points. The student formulates explanations or solutions that are accurate, useful and complete: Do you think that the distillate is now pure water? Explain why or why not. Student Book, page 14. Works independently and comes up with all three of the following: - water (sample) is pure - only the solute remains in the flask - only water was removed from the filtrate by evaporation There is no level 4 here. Works independently and comes up with 2 out of 3 points OR With help from the teacher, is able to come up with all three points. Works independently and comes up with 1 out of 3 points OR With help from the teacher, is able to come up with 2 out of 3 points. Works independently and comes up with an answer that links to the situation OR With help from the teacher, is able to come up with 1 out of three points. The student formulates explanations or solutions that are accurate, useful and complete: Which two separation techniques were used to purify the contaminated water sample? Student Book, page 14. The student formulates explanations or solutions that are accurate, useful and complete: Questions a-d on page 15 of the Student Book. Works independently and comes up with both filtration and distillation. There is no level 4 here. Works independently and answers all 6 questions correctly. Works independently and answers 5 out of the 6 questions correctly. Traces Works independently and comes up with 2 out of 3 points OR With help from the teacher, is able to come up with all three points. Traces Works independently and comes up with all three of the following: - water (or sample) is not pure - only the solid (sediment) removed - some small particles still remain There is no level 4 here. Works independently and comes up with only one of the following: filtration and distillation. There is no level 2 here. OR With help from the teacher is able to come up with both filtration and distillation. Works independently and comes up with an answer that is not relevant but links to the situation. OR With help from the teacher is able to come up with only one of the following: filtration or distillation. Traces The student formulates explanations or solutions that are accurate, useful and complete: Do you think that the filtrate is now pure water? Explain why or why not. Student Book, page 14. Works independently and answers 3 or 4 out of 6 questions correctly OR With help from the teacher is able to correctly answer all 6 questions. Works independently and answers 1 question correctly. OR With help from the teacher is able to correctly answer 1-2 questions. Traces COMPETENCY 2 Makes the most of his/her knowledge of science and technology Cr.3. Relevant explanations or solutions. Page 23 Works independently and answers 2 of the questions correctly. OR With help from the teacher is able to correctly answer 3-5 questions. Competency Average 5 Criteria Score Competencies and Evaluation Criteria Observable Evaluation: MIXTURES AND SEPARATION TECHNIQUES 2 1 Carefully chooses vocabulary that may surpass expectations. All vocabulary used is appropriate. Most vocabulary used is appropriate. Some vocabulary used is appropriate. Nothing written and the vocabulary used is inappropriate Working in a group Participation is essential to the functioning of the group. Student ensures that all members contribute. Contributes positively to the working of the group. Participation is considered functional and adequate. Participation in the group is limited and forced. Refuses to communicate or work in a group. OTHER The student uses appropriate vocabulary. Page 24 Competency Average 3 Criteria Score 4 Teacher notes Traces 5 Teacher notes Competencies and Evaluation Criteria Observable Evaluation: