Experiment No. and Title:#24, 4-Methylcyclohexene Tentative Due

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Experiment No. and Title:#24, 4-Methylcyclohexene
Tentative Due Date for Report:Wed. Jan. 26 (beginning of period)
Points Possible:12
Required for this report:
Balanced reaction
Table of reagents
Separation scheme
Mechanism(s)
IR spectra with analysis
Melting Point (purified)
Labeled sample (purified)
% yield calculation (crude)
% yield calculation (purified)
1
H NMR analysis
13
C NMR analysis
GC analysis
Melting point (crude)
Labeled sample (crude)
Other:
Answer Questions # 1, 2, 5 (p. 197 ) in Pavia
Additional Questions:
1. Explain how you would be able to determine whether or not this reaction has gone
to completion using
a. an IR spectrum
b. chemical tests
2. Indicate the number of signals you would expect to see in both the 1H NMR
spectra and 13C spectra of
a. 4-methylcyclohexanol
b. 4-methylcyclohexene
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