chemistry and process industries laboratory

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DEPARTMENT OF CHEMICAL ENGINEERING
UNIVERSITY OF ENGINEERING AND
TECHNOLOGY PESHAWAR PAKISTAN
CHEMISTRY AND PROCESS
INDUSTRIES LABORATORY
LAB ENGINEER:
Engr Unsia Habib
LAB INTSTRUCTER:
Mr
LAB TECHNOLOGIST:
LAB ASSISTANT:
Jahanzeb
Mr Irfan
Mr
Safeer Chemistry and Process Industries Laboratory Chemistry and Process Industries Laboratory In the chemistry laboratory students learn how to make up chemical solutions, perform
lab techniques, play it safe in the lab, and perform chemistry lab experiments. There are
many important apparatus in chemistry laboratory. These apparatus are of great
importance since it allows experimentation of elements possible. It allows the students
to have hands-on learning thus it is made fun and easy. Common Equipments for
laboratory includes test tubes, Bunsen burner, beaker, burret, and so on.
2 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory EQUPMENTS DESCRIPTION
General Equipments in Laboratory
Below are photos and names of common lab equipment in Chemistry lab.
3 Balance (electronic)
Beakers
Bunsen Burner
Buret
Clay Triangle
Crucible
Flasks
Crucible Tongs
Dropper Pipets
Dropper in action
Goggles
Evaporating Dish
Department of Chemical Engineering U. E. T Peshawar 4 Chemistry and Process Industries Laboratory Forceps
Funnels
Plastic and
Rubber Policemen
Graduated Cylinders
Pinch Clamp
Pipets and Bulbs
Thermometers
Ring Clamp & Stand
Scoopula
Stirring Rods
Utility Clamp
Test Tubes in Rack
Test Tube Holder
Tube & Holder in Action
Wire Gauze
Clamp in action
Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory Additional Equipments in Laboratory
1. Conductivity meter
A conductivity meter is an electrical device used to measure the amount of electrical
power that is conveyed through a liquid. It is used to determine the amount and types of
salts available in water. An electric current is passed through the water, and the output
used to gauge its conductivity
Figure 1: Conductivity meter
5 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 2. PH meter
A pH meter is an electronic device used for measuring the pH (acidity or alkalinity) of a
liquid .This measure the PH (1-14) of any given sample is measured with the help of this
unit.
Figure 2: PH meter
6 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 3. Rotary Evaporator
Rotary evaporator is used to study the evaporation process for variety of extracts by
changing various parameters like temperature e.g Separation of organic liquid by simple
distillation, to purify a given sample of water by simple distillation and to measure the
distillation rate, Purification of organic compound by steam distillation.
Figure 3: Rotary Evaporator
7 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 4. Viscometer
To equipment is used find the density and viscosity of unknown mixture.Viscometers
only measure in one flow condition. In general, either the fluid remains stationary and an
object moves through it, or the object is stationary and the fluid moves past it. The drag
caused by relative motion of the fluid and a surface is a measure of the viscosity. The
flow conditions must have a sufficiently small value of Reynolds number for there to
be laminar flow.
Figure 4:Viscometer
8 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 5. Stalagnometer
The unit is used to determine the surface tension of desired solvent and to find the
percentage composition of unknown mixture by surface tension method
Figure 5:Stalagnometer
6. Potentiometer Automatic Titration
Potentiometer Automatic Titration performs various types of titrations like Alkanity,
Acidity, Chlorides, Sulphideetc
Figure 6:Potentiometer Automatic Titration 9 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 7. Water Bath
This unit helps to maintain a temperature for various analytical experiments like
evaporation of solution for the measurement of total solid in it
Figure 7: Water Bath 10 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 8. Electric Oven
The unit is used to heat any sample from ambient to 550˚ C. The sterilization of various
glaze wares can be done in this electric oven
Figure 8: Electric Oven
11 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 9. Multi-Purpose Processing Vessel
Thefacilities to mix, emulsify, heat, pasteurize, incubate, cool, chill and cure are all built
in to this purpose-designed unit. As well as preparation of food products for further
processing, the facilities allow production of finished products in batch sizes from 5- 20
litres.
Figure 9: Multi‐Purpose Processing Vessel
12 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 10. Muffle Furnace
Many experiments and procedures taken in the lab requires extreme heat
environment. For this purpose, the high temperature muffle furnace steps in as the
necessary part of laboratory equipment. The unit is used to the Moisture contents,
Volatile matter and Ash contents for various samples in the temperature range of
ambient to 1100˚C.
Figure 10:Muffle Furnace
13 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 11. Flask shaker
The unit is used to shake the flask for mixing the sample.
Figure 11: Flask shaker
14 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 12. Polarimeter
The unit is used to measure the Specific gravity, Purityand concentrationfor various
active samples like sugar solutions, turpentine oil and camphor
Figure 12: Polarimeter
15 Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory List of Experiments
S.No
Name of Experiment
1.
To separate the mixture of various inks by paper chromatography
2.
Separation of organic liquid by simple distillation
3.
To purify a given sample of water by simple distillation method and also
calculate the distillation rate
4.
Purification of organic compound by steam distillation
5.
To find the PH of different mixtures using PH meter
6.
To prepare the nitro benzene from benzene
7.
To prepare di-nitro benzene from nitro benzene
8.
To prepare the di-sulphuric acis and check its presence
9.
To determine the presence of unknown mixtures by viscosity method
10.
To determine the mass of KOH required to neutralize acid in 1gm of used oil
11.
To find the percentage composition of mixture by refractive index
12.
To find the concentration of sugar solution by using polarimeter
13.
To measure the surface tension of given liquid sample
14.
To find out the parchor value of the given organic liquid of unknown
molecular weight
15.
To find out the rheochor value of the given organic liquid of unknown
molecular weight
16.
17.
To determine the percentage composition of unknown mixture by surface
tension method
18.
19.
To determine the moisture content and volatile matter in a given sample of
coal
16 20.
To determine the alkalinity of a given water sample
21.
To determine the ash content in a given coal sample
22.
Estimation of waste solids in water
Department of Chemical Engineering U. E. T Peshawar Chemistry and Process Industries Laboratory 23.
Determination of total suspended solids in a given sample of water
24.
Estimation of volatile component present in coal by ASTM method
25.
Estimation of loss on ignition of sample of limestone , iron and marble by
ASTM
26.
To determine the percentage ash content in a given sample of leather
according to ASTM
17 27.
Determination of PH of water and other solutions
28.
Determination of moisture level in a given sample of leather by ASTM
29.
Determination of moisture level in a given sample of clay
30.
Determination of moisture level in a given sample of cement
Department of Chemical Engineering U. E. T Peshawar 
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