QUALITY ASSURANCE MANUAL
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for
Oilfield Environmental & Compliance, Inc.
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307 Roemer Way
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2010 Preisker Lane
Santa Maria, CA 93454
Santa Maria, CA 93454
(805) 922-4772
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Revision 17 – June 2013
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Laboratory Director
& Vice President:
Laboratory Manager:
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Prepared By –
Quality Assurance Manager:
Laboratory Quality System Authority
Julius Carstens
06/01/2013
Date
Lisa Race
06/01/2013
Date
Carrie McCrillis
06/01/2013
Date
This Quality Manual governs the quality program for all operating units of the laboratory, as shown on
the organization chart presented in the manual.
Quality Assurance Manual
Rev 17 – June 2013
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Laboratory Signature Authority
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Laboratory Director
& Vice President:
Julius Carstens
Laboratory Manager:
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Carrie McCrillis
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Quality Assurance Manager:
Lisa Race
Project Manager:
Marissa Censullo
Meredith Sprister
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Project Manager:
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
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TABLE OF CONTENTS
SECTION 1 – QUALITY ASSURANCE OVERVIEW
1.1
QUALITY ASSURANCE MANUAL
1.2
Scope of Testing
1.3
Glossary & Acronyms
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SECTION 3 – QUALITY ASSURANCE FUNCTIONS
3.1
QUALITY POLICY & OBJECTIVES
3.2
CHANGE MANAGEMENT
3.3
DOCUMENT AND RECORD MANAGEMENT
3.4
CORRECTIVE & PREVENTIVE ACTION (CAPA)
3.5
CONTROL OF NON-CONFORMING WORK
3.6
TEST METHODS AND METHOD VALIDATION
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3.7
MEASUREMENT TRACEABILITY
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3.8
3.9
AUDITS
MANAGEMENT REVIEW
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SECTION 2 – PERSONNEL, ORGANIZATION AND RESPONSIBILITIES
2.1
Responsibility and Lines of Authority
FIGURE 2A – ORGANIZATION CHART
2.2
Job Descriptions
2.3
Data Integrity, Ethics & General Training
2.4
PURCHASING SERVICES AND SUPPLIES
Demonstration of Competency (DoC)
Initial Test Method Evaluation
Precision and Accuracy
3.7.1
3.7.2
3.7.3
Reference Materials
Handling and Storage of Reference Standards and Materials
Labeling of Reference Standards, Reagents, and Materials
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3.6.1
3.6.2
3.6.3
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SECTION 4 – CLIENT SERVICE FUNCTIONS
4.1
CLIENT CONFIDENTIALITY
4.2
REVIEW OF REQUESTS, TENDERS AND CONTRACTS
4.3
COMPLAINTS
4.4
SUBCONTRACTING OF TESTS
4.5
REPORTING OF RESULTS
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4.5.1
4.5.2
4.5.3
4.5.4
4.5.5
Analytical &
Quality Control Reports
Case Narrative
Electronic Transmission of Results
Amendments to Reports
SECTION 5 – LABORATORY FUNCTIONS
5.1
ACCOMMODATIONS & ENVIRONMENTAL CONDITIONS
5.2
SAMPLE MANAGEMENT
5.3
EQUIPMENT
5.4
REFERENCES FOR ANALYTICAL METHODS
5.5
QUALITY OF TEST RESULTS
Table 5A – ESSENTIAL QUALITY CONTROL ELEMENTS FOR CHEMISTRY
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TABLE OF CONTENTS (Continued)
APPENDIX A – CONTACT & QUALIFICATIONS OF KEY PERSONNEL
Qualifications:
Julius Carstens
Laboratory Director
Lisa Race
Laboratory Manager
Carrie McCrillis
Quality Assurance Manager
Marissa Censullo
Project Manager
Meredith Sprister
Project Manager
Jesse A. De La Cruz
Technical Supervisor
Gracie Venegas
Operations Coordinator
Maryann Long
Volatile Organic Department Manager
Dwain Zsadanyi
Semi-Volatile Organic Department Manager
Drew Miller
Wet Chemistry Department Manager
Parwinder Parmar
Metals Department Manager
(Vacant)
Oil & Gas Department Manager
Pete Alcocer
Oil & Gas Client Services & Operations Consultant
Roger Dickinson
Field Operations Supervisor
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APPENDIX B – LIST OF STANDARD OPERATING PROCEDURES (SOP)
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APPENDIX C – EQUIPMENT LIST
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APPENDIX E – Data Capability Tables
INORGANICS
METALS
TPH ORGANICS
VOLATILE ORGANICS
SEMIVOLATILE ORGANICS
PNA-SIM
PESTICIDES/PCBs
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APPENDIX F – QC Data Evaluation Flowcharts
Evaluation of Initial Calibration
Evaluation of Continuing Calibration
Evaluation of Method Blank and Instrument Blank Results
Evaluation of Sample Results for Inorganic Analyses
Evaluation of Sample Results for Organic Analyses
Evaluation of Surrogate Compound Recoveries
Evaluation of Laboratory Quality Control Sample & Duplicate
Evaluation of Matrix Spike Recoveries
Evaluation of Duplicate Sample and/or Matrix Spike Duplicate Results
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APPENDIX D – SAMPLE TREATMENT: HOLDING TIMES & CONTAINERS
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SECTION 1 – QUALITY ASSURANCE OVERVIEW
QUALITY ASSURANCE MANUAL - The objective of the OEC Quality Assurance Manual is
to outline the quality organization for the laboratory. The Quality Assurance Manual sets the
standard under which all laboratory operations are performed including the laboratory's
organization, objectives, and operating philosophy. The Quality Assurance Manual defines the
policies, procedures, and documentation that meet the objectives and requirements of the
sampling and analytical services that OEC provides to its’ clients.
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1.1
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OILFIELD ENVIRONMENTAL & COMPLIANCE INC. (OEC) is an analytical laboratory and field
support company located in Santa Maria, California. It is operated as a commercial environmental
laboratory, specializing in the analytical testing of solids, liquids, air, and product matrices. It is the goal
of OEC to provide its’ clients with data that is valid, defensible and reproducible while meeting their
specific needs.
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The Quality Assurance Manager ensures that OEC policies and objectives for quality are
documented by reference or by inclusion in the Quality Assurance Manual. The Quality
Assurance Manual is communicated to, understood by, and implemented by all personnel
concerned. Where the Quality Assurance Manual does not document laboratory requirements, a
separate SOP will do so.
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In the following sections, detailed information will be given on OEC procedures for personnel
qualifications, sample collection, CoC documentation, sample handling, storage and disposition,
equipment calibrations and maintenance, reagents, SOPs, quality control procedures and data
reduction, validation and verification.
Scope of Testing – The laboratory scope of analytical testing services includes those listed in
Appendices D & E.
1.3
Glossary & Acronyms – Refer to GEN-DEFIN, Acronyms & Definitions for a complete listing of
laboratory terms and acronyms.
Acceptance criteria – Criteria often applied to data drawn from existing sources
(“secondary “ data) addressing the adequacy of existing information.
Accuracy – The average of results of same sample compared to amount of known analyte in
sample.
Audit – A systematic and independent examination to determine whether quality activities and
related results comply with planned arrangements and whether these arrangements are
implemented effectively and are suitable to achieve objectives.
Bias – The systematic or persistent distortion of a measurement process that causes errors in one
direction.
Blank – A sample containing none of the analytes of interest subjected to the usual analytical
process to establish a zero baseline. It is used to detect contamination during sample handling
preparation and/or analysis.
Chain-of-custody (CoC) – An unbroken trail of accountability that ensures the physical security
of samples, data and records.
Comparability – A measure of the confidence with which a method or set of data can be
compared to another.
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1.2
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Conformance – an affirmative indication or judgment that a product or service comply with the
relevant specification, contract or regulation.
Continuing Calibration Verification (CCV) – The protocol to check the calibration curve on a
batch basis to verify that it is still valid. The normal check is to test one of the original mid-level
calibration standards and verify that the RPD is within the acceptance range of the method.
Corrective action – Any measures taken to rectify conditions adverse to quality and where
possible, to prevent recurrence.
Data quality – A measure of the degree of acceptability or use of data for a particular purpose.
Data reduction – The process of transforming the number of data items by arithmetic
or
statistical calculations, standard curves and concentration factors and assemble them into a more
useful form.
Data validation – An analyte-/sample-specific process that extends the evaluation of data beyond
method, procedural or contractual compliance to determine the analytical quality of a specific
data set.
Data verification – The process of evaluating the completeness, correctness and
conformance/compliance of a specific data set against the method, procedural, or contractual
specifications.
Detection limit – The lowest concentration or amount of the target analyte that can be
determined to be different from zero by a single measurement at a stated level of probability.
Used to distinguish samples that do not contain a specific analyte from samples that contain low
concentration of the analyte.
Duplicates – For each batch analyzed, a sample duplicate, laboratory control duplicate and a
matrix duplicate will be added for quality control purposes to demonstrate precision in
performing the analysis.
Field blank – A clean analyte-free sample which is carried to the sampling site and then exposed
to sampling conditions, returned to laboratory and treated as an environmental sample. It is used
to provide information about contaminants that may be introduced during sample collection,
storage and transport.
Holding time (HT) – The period of time a sample may be stored before analysis.
Initial Calibration Verification (ICV) – Immediate analysis of standards from a different
manufacturer than that of the calibration standards to check suitability of a calibration curve.
Internal Standard (IS) – Compounds added to the sample after sample preparation for
qualitative and quantitative analysis. The compounds serve to give a standard of retention time
and instrument response.
Laboratory Control Sample (LCS) – A sample made with reagent water and known amounts of
target analytes. It is analyzed with a batch to serve as quality control on the sample preparation
process.
Matrix spike sample (MS) – A sample prepared by adding a known amount of the target analyte
to a specified amount of a matrix. It is used to determine the effect of the matrix on a method’s
recovery efficiency.
Method – A body of procedures and techniques for performing an activity, systematically
presented in the order in which they are to be executed.
Method blank (MB) – A blank prepared and analyzed exactly like the sample to indicate if a
bias has been introduced into the analytical procedure.
Method Limit (ML) or Method Detection Limits (MDL) – Minimum level of a target analyte
that can be determined with 99% confidence.
Reporting Limit (RL) or Practical Quantitation Levels (PQL) – The lowest level that can be
reliably achieved during routine laboratory operating conditions within specified limits of
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precision and accuracy. The number given is selected by multiplying the standard deviation
results from the MDL procedure.
Precision – A measure of agreement among repeated measurements of the same property under
identical conditions. It is generally expressed in terms of the standard deviation.
Quality assurance – The sum of all quality control performed, the reporting of the data and
improvement made to ensure that processes are of the quality needed.
Quality control – Procedure to evaluate a single aspect of an analyte or test.
Spike – A substance that is added to an environmental sample to increase the concentration of the
target analyte by a known amount. It is used to measure accuracy. Spike duplicates are used to
assess measurement precision.
Standard Operating Procedure (SOP) – A document that details the method for an operation,
analysis or action with thoroughly prescribed techniques and steps to be followed. It is officially
approved as the method for performing certain tasks.
Abbreviation
Mega
Kilo
Deci
Centi
Milli
Micro
Nano
M
k
d
c
m
μ
n
Pico
p
Value
6
10
3
10
-1
10
-2
10
-3
10
-6
10
-9
10
SI Parameter
Base Unit
Abbreviation
Mass
Length
Time
Temperature
Amount of Substance
Electric Current
Luminous Intensity
Gram
Meter
Second
Kelvin
Mole
Ampere
Candela
g
m
s
K
mol
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SI Prefix
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Units – All units used to qualify any incoming samples must be properly identifiable. The
laboratory utilizes SI and additional units in our measuring systems. Listed below are common
industry units of measure.
SI Units (NIST)
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Additional common industry units
L – Liter (volume parameter accepted for use with SI) Hence:
mL – milliliter (0.001 L)
μL – microliter (0.000001 L)
Ω = Ohm: V=IR (used for DI water purity measurement)
ºC = Centigrade:
ºC = K – 273.15
ºF = Fahrenheit:
ºF = 9/5(ºC) + 32
ppb – parts per billion (normally μg/L for aqueous samples or μg/kg for solid samples)
ppm – parts per million (normally mg/L for aqueous samples or mg/kg for solid samples)
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ACRONYMS not otherwise defined
Blk
–
Blank
°C
–
degrees Celsius
CAPA
–
Corrective Action & Preventive Action
cal
–
calibration
COC
–
Chain of custody
DO
–
Dissolved oxygen
DOC
–
Demonstration of Competency
EPA
–
Environmental Protection Agency
g/L
–
grams per liter
GC/MS
–
gas chromatography/mass spectrometry
ICP-MS
–
inductively coupled plasma-mass spectrometry
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Initial calibration verification
Initial Demonstration of Capability
Pound per Square Inch
Laboratory Control Sample
Laboratory Fortified Blank
Milligrams per Kilogram
Milligrams per Liter
Matrix Spike
Matrix Spike Duplicate
Oilfield Environmental and Compliance, Inc.
Practical Quantitation Limit
Quality Assurance
Quality Control
Quality Assurance Manual
Reporting Limit
Relative Percent Difference
Relative Standard Deviation
Standard Operating Procedures
Spike
Standard
Micrograms per Liter
Ultraviolet
Volatile Organic Compound
Whole Effluent Toxicity
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–
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–
–
–
–
–
–
–
–
–
–
–
–
–
–
–
–
–
–
–
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ICV
IDoC
lb/in2
LCS
LFB
mg/Kg
mg/L
MS
MSD
OEC
PQL
QA
QC
QAM
RL
RPD
RSD
SOPs
spk
std
µg/L
UV
VOC
WET
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SECTION 2 – PERSONNEL, ORGANIZATION AND RESPONSIBILITIES
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Oilfield Environmental And Compliance, Inc. (OEC) is a legally identifiable organization, located in
Santa Maria, California. Through application of the policies and procedures outlined in this chapter, the
laboratory assures that it is impartial and that personnel are free from undue commercial, financial, or
other pressures that might influence their technical judgment. The laboratory is responsible for carrying
out testing activities that meet the requirements of the EPA Standards and that meet the needs of the
client.
2.1
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OEC management is committed to quality and to the Quality Organization as stated in the Quality Policy,
which is upheld through the application of related policies and procedures. A complete training program
is administered to new employees prior to their handling client samples. Through proper training new
employees are made aware of causes of unethical or illegal actions during analysis. The use of operating
procedures specifying appropriate and inappropriate instrument and system manipulation practices,
comprehensive systems audit, a corrective action program, electronic and hard copy post-analysis data
audits and external performance evaluations contribute to quality workmanship from OEC employees.
RESPONSIBILITY AND LINES OF AUTHORITY
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OEC “SENIOR MANAGEMENT” includes the titles Laboratory Director, Laboratory Manager,
and Quality Assurance Manager. The term “MANAGEMENT” additionally includes the titles
Technical Supervisor, Operations Manager, and Department Managers. Approved signatories for
the laboratory include the Laboratory Director, Laboratory Manager, Project Managers and
Quality Assurance Manager.
The Laboratory Director has overall responsibility for the technical operations and establishment
of total laboratory policies, including the required quality of laboratory operations.
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OEC senior management is responsible for the policies, procedures, changes and delegation of
responsibilities related to the Quality System. OEC management assumes specific responsibility
for maintenance of the Quality System. This includes defining roles and responsibilities to
personnel, approving documents, providing required training, providing a procedure for
confidential reporting of data integrity issues, and periodically reviewing data, procedures, and
documentation. The management also ensures that audit findings and corrective actions are
completed within required schedules.
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The Laboratory Director appoints designated alternates during the absence of the Laboratory
Director, Laboratory Manager, Quality Assurance Manager, Technical Supervisor or Department
Managers.
The Laboratory Director is responsible for defining the minimal level of education, qualifications,
experience, and skills necessary for all positions in the laboratory and that technical staff have
demonstrated capabilities in their tasks. Training is kept up to date as described in this manual by
periodic review of training records and through employee performance review.
The Department Manager ensures technical competence of personnel operating equipment,
performing tests, or evaluating results, and limits authority to perform laboratory functions to
those appropriately trained and/or supervised.
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FIGURE 2A –ORGANIZATION CHART
Refer to Appendix A for contact information and resumes of key personnel
2.2
JOB DESCRIPTIONS
Job descriptions are available for all positions that manage, perform, or verify work affecting data quality.
Job descriptions include the specific tasks for each position.
2.2.1
Laboratory Director
a)
Is in charge of all laboratory activities, and is the highest-level manager. The laboratory
director signs, and is responsible for overall laboratory and management compliance with
the Quality Assurance Manual.
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b)
Supervises all laboratory activities including staffing, training, procurement, safety,
productivity and quality assurance.
Responsible for acquisition and maintenance of laboratory certification.
Acts as technical consultant for clients as necessary.
Acts as technical consultant for laboratory operations as necessary.
Determines the minimum qualification level for all positions in the laboratory.
Responsible for appointing alternates for critical laboratory positions when necessary.
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c)
d)
e)
f)
g)
Laboratory Manager
a)
Assumes Laboratory Director responsibilities when absent.
b)
Responsible for content maintenance of the LIMS system.
c)
Ensures that all quality parameters related to projects are within method and client
specified requirements.
d)
Responsible for laboratory adherence to the Quality System and legal defensibility of
data.
e)
Acts as technical consultant for clients as necessary.
f)
Acts as technical consultant for laboratory operations as necessary.
2.2.3
Quality Assurance Manager
a)
Assumes Laboratory Manager responsibilities when absent.
b)
Designs and oversees the Quality Assurance Program, and maintains any certifications
thereto.
c)
Maintains and updates the Quality Assurance Manual and Statement of Qualifications.
d)
Designs, maintains and monitors all other components of the Quality System, including,
but not limited to: Corrective & Preventive Action System (CAPA), Document Control
System, Demonstrations of Capability for equipment and employees, Control Charting
and Limit Updates, Orientation & Training Program, Management Review, Change
Management System, Proficiency Testing, Internal Auditing & Continual Improvement.
e)
Has knowledge and experience in QA/QC procedures.
f)
Has knowledge of analytical procedures to evaluate data objectively and perform
assessments.
g)
Notifies laboratory management of deficiencies.
h)
Trains staff personnel in quality control procedures.
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2.2.2
Technical Supervisor
a)
Assumes Quality Assurance Manager responsibilities when absent.
b)
Responsible for all technical aspects of laboratory function, including instrument
operation, improvements, maintenance, and parts & consumables inventory.
c)
Documents and performs (as necessary) preventive and corrective maintenance on
analytical and support equipment. Instructs personnel in proper procedures for
maintenance and related documentation.
d)
Investigation of equipment technology and regular reports/recommendations to upper
management relating to laboratory apparatus status and needed improvements or updates.
e)
Development and installation of new laboratory methods and equipment.
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2.2.4
2.2.5
Project Manager
a)
Responsible for the final review of sample results and related quality control.
b)
Ensures that all quality parameters related to projects are within method and client
specified requirements.
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c)
d)
Compiles result packages and approves analytical reports issued by the laboratory.
Acts as primary contact for clients.
Operations Coordinator
a)
Manages ordering and logistics for client sampling and laboratory operations.
b)
Schedules couriers and contact point for field operations.
2.2.7
Department Manager
a)
Responsible for the daily laboratory operation and adherence to quality standards.
b)
Supervises and trains chemists and other personnel within the analytical group.
d)
Verifies chain-of-custody and assures that appropriate analyses are performed within
required ‘holding’ and ‘turn-around’ times.
e)
Responsible for secondary review and approval of analytical raw data.
f)
Reports any QC problems and performs necessary corrective actions to restore quality
control. Submits corrective action reports to the Quality Assurance Manager.
g)
Prepares and maintains logbooks and documentation of department activities.
h)
Schedules and performs instrument validation, calibration and preventive maintenance.
2.3
DATA INTEGRITY, ETHICS & GENERAL TRAINING
2.3.1
ORIENTATION TRAINING – New employees are given an orientation upon arrival. Standard
Operating Procedures (SOPs) for the laboratory Health and Safety Plan, Client Confidentiality,
and Corrective Action Reports (CAR) are included in this orientation. All SOPs have training
verification forms as part of the document, and these forms are filled out and maintained in the
employee’s training file.
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2.2.6
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DATA INTEGRITY is the result of the processes that together assure valid data of known and
documented quality. OEC management emphasizes integrity procedures by providing ethical and
complete training for a position before allowing any employee to handle client samples.
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It is necessary that employees understand that any infractions of the laboratory data integrity
procedures will result in an investigation that could lead to very serious consequences such as
immediate termination, or civil/criminal prosecution. New employees are required to read the
Data Integrity and Ethics procedures and complete the associated Training Verification Form(s).
Signatures on these forms are used to document the employee’s understanding and obligation to
data integrity. Training records regarding data integrity and ethics are signed and dated by senior
management. Data integrity procedures and evidence of inappropriate actions are reviewed
annually through regularly scheduled internal audits or periodically through in-depth data or
records review and are updated by management.
2.3.2
REPORTING INFRACTIONS – Employees can confidentially report ethic and data integrity
issues by having (1) unrestricted access to senior management, (2) the assurance not to be treated
unfairly for reporting ethics and data integrity breaches, and (3) anonymous reporting.
Any potential data integrity issue is handled confidentially until a follow-up evaluation, full
investigation, or other appropriate actions have been completed and the issues clarified.
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Inappropriate activities are documented, including disciplinary actions, corrective actions, and
notifications of clients, if applicable. These documents are maintained for a minimum of 5 years.
ANALYTICAL TRAINING – Oilfield Environmental & Compliance allows only trained
personnel to perform specific tasks in the laboratory. All employees are properly trained and
complete an Initial Demonstration of Capability (IDoC) before they are assigned tasks that can
affect data quality. IDoC must be performed whenever there is a new analyst or a significant
change in the analytical instrumentations. Proficiency is demonstrated by preparing and
analyzing four replicates of Quality Control Check with recovery results within 70-130% or
current laboratory defined control limits and RPD ≤ 20%. Management assumes the
responsibility to assure personnel are trained and necessary records of training are kept on-file.
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2.3.3
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The Laboratory Director will determine the need for an investigation of data integrity issues.
Allegations will remain confidential to the extent necessary. All documentation for investigations
of an inappropriate data integrity activity shall include notifications of clients, corrective actions
taken, and any disciplinary actions involved.
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Upon completion of orientation, the supervisor of the new employee will oversee the training of
specific tasks in the laboratory.
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The initial training for a new task will contain the following steps:
a)
All documentation involved with a new and unfamiliar task will be read and understood
by the trainee.
b)
Instruction in the proper use of all equipment utilized in the task the trainee is learning.
c)
Instruction in the location of all necessary reagents required and proper techniques for
measuring and preparing these reagents.
d)
Instruction in the proper procedure for tasks assigned including any prep work, if
needed.
e)
Instruction for all quality control procedures for the task assigned.
f)
Instruction in all safety procedures for the task assigned.
g)
Training will be under the direct supervision of the supervisor or senior analyst. During
the training period, the trainee may sign laboratory notebooks or logbooks, but the senior
analyst or supervisor that is responsible for the data generated must cosigned these books.
h)
The trainee will demonstrate proficiency in the new task before they can operate
independently. The proficiency for a test method is accomplished by a demonstration of
competency. The supervisor or senior analyst must sign the training form to show
approval of competency.
i)
Each step of the training process is documented.
j)
Management will determine on-going training by assessment of the company’s need for
training for new equipment or new positions or for cross training for existing positions.
2.4
PURCHASING SERVICES AND SUPPLIES
Oilfield Environmental & Compliance’s (OEC) suppliers for all their reagents and supplies are worldrenowned companies that include companies that are ISO certified. The laboratory has procedures in
place for purchasing, receiving, and storage of supplies that affect the quality of environmental tests.
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Management reviews and approves the supplier of services and supplies and approves technical
content of purchasing documents prior to ordering.
2.4.2
OEC purchases reagents and chemical standards for all its tests that conform to the specifications
of the Committee on Analytical Reagents of the American Chemical Society. Other grades may
be used, provided it is first ascertained that the reagent is of sufficient purity to permit its use
without lessening the accuracy of the determination. Upon receipt, bottles are checked for
breakage, leakage and expiration date. The certificate of analysis that accompanies the chemical
is maintained on file and the chemical stored according to manufacturer’s specifications or for the
test method SOP that the reagent will be used.
2.4.3
The purchase of services is primarily limited to annual calibration and maintenance of support
equipment and is performed by representatives of the companies where the equipment was
purchased.
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2.4.1
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SECTION 3 – QUALITY ASSURANCE FUNCTIONS
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Oilfield Environmental & Compliance’s Quality System is documented in this Quality Assurance Manual
and associated quality system documents. Together they describe the policies, objectives, principles,
responsibilities, accountability, and implementation plan of the organization for ensuring quality in its
work processes and services.
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3.1
QUALITY POLICY & OBJECTIVES
The quality policy is signed and dated as a component of this manual, and is issued under the authority of
the highest level of laboratory management, which demonstrates management’s commitment to integrity,
ethics, the quality system and associated standards. All of Oilfield Environmental & Compliance’s
objectives and policies are documented and the laboratory personnel are required to know and implement
them in their work.
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Quality Policy Statement – At Oilfield Environmental & Compliance, Inc. (OEC) the purpose of the
quality control program is to produce data of known quality that meets the requirements of standard
analytical methods or the client needs. The objectives of the quality assurance activities for the laboratory
are to provide a system for ongoing evaluation of analytical data throughout the course of operations and
to have quality control data that will ultimately be used to define the QC parameters in terms of accuracy,
precision, completeness and defensibility. Our policy is a dedication to provide quality environmental
testing by upholding the highest quality standards in a professional and ethical manner. This dedication
requires ongoing commitment and continually improves the quality of our work.
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Quality Objectives – Objectives are achieved by performing quality assurance with every group of
samples analyzed. The quality assurance is verified by checking sample duplicates, spikes, spike
duplicates, laboratory control samples and blanks. In addition, surrogate recoveries are measured if
applicable to the method. The quality control data generated with the samples may be supplied to the
client upon request. The quality of data generated is confirmed by its assessment against the following
objective parameters:
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Accurate – The degree of accuracy is determined by the agreement between an observed value and an
accepted reference or true value. Accuracy is ensured by the adherence to quality handling protocols and
use of dual source certified reference materials for all possible methodologies. Accuracy is monitored
through the performance of quality control check samples, matrix spikes, laboratory quality control
spikes, and surrogate/internal standard spikes.
Precise – The degree of precision is determined by the difference in resultant value of two identically
prepared items. Precision is ensured by adherence to protocols for replicate analyses. Precision is
monitored by the performance of sample and/or field duplicates, matrix spike and control spike
duplicates, and the subsequent calculation of relative standard deviation (RSD) or relative percent
difference (RPD).
Complete – The degree of completion is determined by the amount of valid data returned from any
sampling set compared to the expected amount under normal conditions. Completeness is ensured by
adherence to all quality protocols for every sample received. OEC makes a concerted effort to provide the
most complete resultant data possible for every sampling set.
Defensible – The degree of defensibility of a specific data set is measured by the completeness of
documentation and traceability to certified standards for comparison. OEC strives to provide the best
quality for our clients and as such, all samples are documented and treated as if their results will be
scrutinized for legal purposes.
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3.2
CHANGE MANAGEMENT
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Oilfield Environmental & Compliance (OEC) maintains a change control system that encompasses all
critical processes to the laboratory. This includes new entries or changes to LIMS, equipment, staff,
documents (forms & records), methods (external documents), or Standard Operating Procedures (SOPs).
The SOP for Change Management defines the change procedures for each type of laboratory critical
function.
3.3
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All changes made within the laboratory are done in such a manner as to fully document all components of
the change, fully train all affected personnel before a change is put into effect, and verify all necessary
approvals prior to making changes. Obsolete documents or references are removed as soon as a change
goes into effect to minimize the possibility for error or confusion.
DOCUMENT AND RECORD MANAGEMENT
Controlled Documents are uniquely identified, issued, tracked and kept current as part of quality
management. Many of the controlled documents are also approved documents which means they
need to be signed and dated. All controlled documents are identified by such methods as issued
date, revision number, page number, total number of pages or a mark indicating the end of
document and signature of approving authority. Approved copies of documents are available in
the appropriate areas of the laboratory. These are distributed by the Laboratory Director, Quality
Assurance Manager or Department Manager.
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3.3.1
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To demonstrate that quality has been achieved, Oilfield Environmental & Compliance (OEC) maintains a
document management system that includes distributing, reviewing, modifying and controlling all text.
This management system includes both current and obsolete documents.
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3.3.1.1 OEC retains documents that are both internal and external. A master list of controlled
internal and external documents is maintained by the Quality Assurance Manager. The list is
updated periodically.
a)
Internal documents include SOPs, QC files, Client folders, logbooks and the Quality
Assurance Manual.
b)
External documents include reference methods and standards, instrument user manuals,
certificates of analysis and certificates of traceability.
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3.3.1.2 Changes may be performed by handwritten modification to a hard copy document, on a
temporary basis, with a date and identifier (initials) accompanying the change. When changes are
necessary, the obsolete documents are removed. Changes made to electronic documents must be
accompanied by a change tracking function. Amendments to documents are incorporated into a
new revision and reissued as soon as practicable.
3.3.2
Obsolete Documents – All invalid or obsolete documents are removed, and except for the
archived copy, destroyed. This will prevent unintended use. Obsolete documents retained for
legal use or historical knowledge preservation are appropriately marked and stored in the OEC
storage area and kept for a period of ten years.
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Standard Operating Procedures (SOPs) are documents that give a detailed description of how
laboratory processes may be accurately reproduced. They are used to ensure consistency of
application of common procedures. There are two types: 1) test method SOPs, which have
specifically required details, and 2) general use SOPs that document the more general
organizational procedures. Copies of all SOPs are accessible to all personnel. Each SOP indicates
the effective date, the revision number, and the signature(s) of the Laboratory Director, the
Quality Assurance Manager and when applicable the Department Manager and method reference.
A list of representative OEC SOPs can be found in Appendix B.
3.3.4
Records are a subset of documents. Records may be on any form of media, including electronic
and hard copy. Records allow for the historical reconstruction of laboratory activities related to
sample handling and analysis. Oilfield Environmental & Compliance (OEC) maintains a record
system appropriate to its needs, records all laboratory activities, and complies with applicable
standards or regulations as required.
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3.3.3
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3.2.4.1 Records of all procedures to which a sample is subjected while in the possession of the
laboratory are kept for a period of ten years. OEC retains all original observations, calculations
and derived data, calibration records, and a copy of the test report for a minimum of ten years.
The laboratory maintains a record management system for control of laboratory notebooks,
instrument logbooks, standards logbooks, and records for data reduction, validation, storage and
reporting.
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3.2.4.2 Records, including electronic records, are easy to retrieve, legible, and protected from
deterioration or damage; held secure and in confidence; and are available to accrediting
authorities for a minimum of ten years. All electronic records are backed-up and placed off site.
Access to protected records is limited to laboratory management or their designees to prevent
unauthorized access or amendment.
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3.2.4.3 In the event that the OEC transfers ownership or goes out of business, records are
maintained or transferred according to the clients’ instructions.
3.4
CORRECTIVE & PREVENTIVE ACTION (CAPA)
3.4.1
PREVENTIVE ACTION – At OEC, preventive action eliminates or minimizes nonconformances and incorrect data through scheduled preventive maintenance on equipment and
through the review process.
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Preventive action includes, but is not limited to, review of QC data to identify quality trends,
regularly scheduled staff quality meetings, annual budget reviews, managerial reviews, and other
actions taken to prevent problems.
All employees have the authority to recommend preventive action procedures, however
management is responsible for implementing preventive action.
3.4.2
CORRECTIVE ACTION is the action taken to eliminate the causes of an existing nonconformity,
defect, or other undesirable situation in order to prevent recurrence (NELAC, 2003).
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3.4.2.1 POLICY – All deficiencies that occur in the Oilfield Environmental & Compliance
laboratory are considered serious and remedial action is taken immediately. This includes data
quality, systematic problems, instrument failures or safety practices. Corrective action taken is
appropriate for the magnitude of the problem and the degree of risk.
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3.4.2.2 PROCEDURE – The individual that is initially aware of a problem is responsible for
initiating corrective action. All deficiencies are investigated and a corrective action plan
developed and implemented if determined necessary.
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a)
Selection and Implementation of Corrective Actions – Once a non-conformance
is noted, the first action is an investigation to determine the origin of the problem. A
Corrective Action Report (CAR) is initiated (See SOP-Corrective Action Reports) listing
cause of problem and possible solution. It is then submitted to the Quality Assurance
Manager to receive a unique number and recorded in the CAPA system. The Department
Manager will determine the corrective action to be taken.
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b)
Monitoring of Corrective Action – The Department Managers will monitor
implementation and results of the corrective action. The Quality Assurance Manager will
track, catalog and review the corrective action to assess effectiveness.
3.4.2.3 TECHNICAL CORRECTIVE ACTION – Sample data associated with a failed quality
control is evaluated for the need to be reanalyzed or qualified. When quality control results are
unacceptable, all pertinent information is documented on a CAR.
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a)
The analyst is responsible for initiating and recommending corrective actions.
Analysts routinely implement corrective actions for data with unacceptable QC measures.
First level correction may include re-analysis for obvious cause without further
assessment. If the test method SOPs addresses the specific actions to take, they are
followed. Otherwise, corrective actions start with assessment of the cause of the problem.
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b)
The Department Manager will review corrective action reports and suggest
improvements, alternative approaches, and procedures where needed.
c)
If the data reported are affected adversely by the nonconformance, the client is
notified in writing. The discovery of a non-conformance for results that have already
been reported to the client must be immediately evaluated for significance of the nonconformance, its acceptability to the client, and determination of the appropriate
corrective action.
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3.4.2.4 POLICY FOR EXCEPTIONALLY PERMITTING DEPARTURES FROM
DOCUMENTED POLICIES AND PROCEDURES – Oilfield Environmental & Compliance
allows the release of non-conforming data only with approval on a case-by-case basis by the
appropriate Department Manager, Laboratory Director or Laboratory Manager. Planned
departures from procedures or policies do not require audits or investigations. Examples of
exceptions would be insufficient sample volume, expired holding time, or sample data not
affected by the results. Permitted departures for non-conformances are fully documented and the
reason for the departure along with qualification for acceptance is included with test data given to
the client.
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CONTROL OF NON-CONFORMING WORK
NON-CONFORMING WORK is work that does not meet acceptance criteria or requirements.
Non-conformances can include unacceptable quality control results departures from standard
operating procedures or test methods. Requests for departures from laboratory procedures are
approved by the Laboratory Director and documented.
3.5.1
Oilfield Environmental & Compliance’s policy for control of non-conforming work is to identify
the non-conformance, determine if it will be permitted, and take appropriate action. All
employees have the authority to stop work on samples when any aspect of the process does not
conform to laboratory requirements.
3.5.2
The procedure for investigating and taking corrective action of non-conforming work is described
in Section 3.4.2 Corrective Action. Employees should immediately notify their Department
Manager of any non-conformance. The Department Manager evaluates the significance of the
nonconforming work and takes corrective action immediately. The client is notified if their data
has been impacted. The Department Manager authorizes the resumption of analysis on all nonconformance work.
3.6
TEST METHODS AND METHOD VALIDATION
Oilfield Environmental and Compliance (OEC) ensures the quality of its analysis by using test
methods approved by EPA and other industry-recognized analytical methods. OEC also
guarantees quality analysis by having all analyst demonstrate capability of performing the test
methods that they are assigned and that all methods are validated before being put to use. A list
of Test Methods that OEC uses can be found in Appendix C through E.
3.6.1
Demonstration of Competency (DoC), Initial & Continuing – OEC confirms that it is capable of
generating data of acceptable accuracy and precision on all methods before employing them by
having all analyst complete a Demonstration of Competency to establish the analyst‘s ability to
perform the methods.
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A DoC is performed for each analyte whenever the method, analysts, analytes, or instrument type
is changed. The DoC is documented for each SOP (test method) and matrix performed. These
records are maintained in the training files for each analyst. The Department Manager certifies
that staff members in their area of expertise are trained and authorized to perform all tests for
which we are accredited by signing the SOP training form.
Initial Test Method Evaluation – For chemical analyses, the Initial Test method evaluation
involves the determination of the Method Detection Limits (MDL), confirmation of the Reporting
Limit (RL, also known as PQL: Practical Quantitation Limits), an evaluation of precision and
bias, and an evaluation of the selectivity of the method.
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3.6.2
3.6.2.1 MDL – The method detection limit (MDL) is the minimum concentration of a target
analyte that can be measured and reported with 99% confidence that the value is above zero.
MDLs must be updated on an annual basis and the studies are kept on file in the laboratory.
Analytical reports requiring ‘J’ flag reporting will display the MDL value for a particular as the
‘Method Limit’ (ML).
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3.6.2.2 RL & PQL – After the MDL is determined, a reporting limit (RL), or practical
quantitation limit (PQL), must be established. The RL calculation may vary depending on the
type and sensitivity of a particular method. An example of a standard RL calculation is as
follows:
RL = standard deviation of 7 replicates * 10.
The lowest calibration standard is equal to the RL. The RL will always be greater than the MDL.
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Precision and Accuracy – OEC objective for precision and for accuracy is to equal or exceed the
precision and accuracy for these analytical methods on similar samples. Data quality objectives
for accuracy and precision are method specific, and are defined in the SOP for each method.
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3.6.3
PRECISION is the degree to which a set of observations or measurements of the same property,
obtained under similar conditions, conform to themselves. Precision is usually expressed as
standard deviation, variance, or range, in either absolute or relative terms. Laboratory control
limits are established for measurements of laboratory duplicates, duplicate laboratory control
samples and matrix spike duplicates for quantitative tests when applicable.
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For ACCURACY, the laboratory control limits are established for measurements of external
standards, laboratory control samples and matrix spike samples and internal performance
evaluation check samples for quantitative tests.
MEASUREMENT TRACEABILITY
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Measurement quality assurance comes in part from traceability of standards to certified materials. In
general, calibration is performed with at least five levels of concentration to cover the working range. All
equipment used that affects the quality of test results are calibrated (1) prior to equipment being put into
service (2) annually or sooner if specified by the method, (3) the analytical response has changed beyond
method tolerance, (4) whenever there is a significant modification of the instrument or the method. The
calibration standards are traceable to national standards of measurement or manufacturers’ certification.
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Measurements from laboratory equipment provide the uncertainty required by test method or client. If
traceability of measurements to SI units is not possible or not relevant, evidence for correlation of results
through inter-laboratory comparisons, proficiency testing, or independent analysis is provided. All
equipment that affects the quality of test results are calibrated according to the minimum frequency
suggested by the manufacturer, by regulation, by method, or as needed. Clients can verify that required
uncertainty is achieved by reviewing the internal quality control data, if requested.
3.7.1
Reference Materials, where commercially available, are traceable to national standards of
measurement, or to Certified Reference Materials, usually by a Certificate of Analysis. Internal
reference materials, such as working standards or intermediate stock solutions, are checked as far
as technically and economically possible.
a)
Stock standard solutions are prepared from neat substances or purchased from vendors
with certified analyte concentrations. New stock standard solutions are verified against existing
standards prior to use.
b)
Standard preparation is documented in analyst logbooks. Results are stored with
calibration data for the method.
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c)
Working standards are verified against certified standards from a second vendor, a
different lot or a different preparation from neat substances. Working standards are prepared
from stock standard solutions by volumetric dilution with method-specific solvents.
d)
Specific working standard concentrations and diluents are documented in laboratory
SOPs for each method.
Handling and Storage of Reference Standards and Materials – The laboratory manages and
transports reference standards and materials in a way that protects their integrity. Reference
standard and material integrity is protected from incompatible materials by being kept in separate
areas. The integrity is also protected by minimizing exposure to degrading environments or
materials.
Reference standards and materials are stored according to manufacturer’s
recommendations and separately from working standards or samples.
3.7.3
Labeling of Reference Standards, Reagents, and Materials – Reference standards and materials
are tracked from purchase, receipt, and storage through disposal. Expiration dates are the date on
the bottle or six months from date bottle is opened whichever comes first.
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3.7.2
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3.7.3.1 Records for all standards, reagents, reference materials, and media include:
a)
the manufacturer/vendor name (or trace ability to purchased stocks or neat compounds)
b)
the manufacturer’s Certificate of Analysis or purity (if supplied)
c)
the date of receipt
d)
reference to the method of preparation
e)
date of preparation
f)
recommended storage conditions
g)
an expiration date after which the laboratory shall not use.
h)
preparer’s initials (if prepared)
3.7.3.2 In methods where the purity of reagents is not specified, analytical reagent grade is used.
If the purity is specified, that is the minimum acceptable grade.
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3.7.3.3 All containers of standards, reagents, or materials, whether original or prepared, are
labeled with an expiration date.
3.7.3.4 All containers of prepared standards and reference materials have a unique identifier,
preparation name, expiration date, preparer’s name and preparation date.
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3.7.3.5 Standard preparation records are kept in the LIMS system and laboratory notebooks and
indicate trace ability to purchased stocks or neat compounds, reference to the method of
preparation, date of preparation, expiration date, and preparer's initials.
3.8
AUDITS
AUDITS measure laboratory performance and verify compliance with accreditation/ certification and
project requirements. Audits specifically provide management with an on-going assessment of the quality
system. They are also instrumental in identifying areas where improvement in the quality system will
increase the reliability of data. There are both internal and external audits.
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3.8.1
Internal Audits – At Oilfield Environmental Compliance the review of the appropriateness and
adequacy of the Quality Assurance Program is ongoing. To contain problems with the Quality
program, reviews may be done monthly, quarterly and at the least, annually. Personnel may not
audit their own activities except when it can be demonstrated that an effective audit will be
carried out.
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3.8.1.1 Annually, the laboratory prepares a schedule of internal audits to be performed during the
year. These audits verify compliance with the requirements of the quality system, including
analytical methods, SOPs, ethics policies, and other laboratory policies. The Quality Assurance
Manager (or other members of Laboratory Management) will plan and execute the scheduled
audits and reviews. All audits, audit findings and any corrective action taken as a result of an
audit will be documented.
3.8.1.2 Notification of clients for events that cast doubt on the validity of the results is completed
within 24 hours.
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3.8.1.3 Review of the auditing process is done to ensure that corrective actions that were needed
were implemented and effective.
External Audits – It is Oilfield Environmental & Compliance’s policy to cooperate and assist with
all external audits, whether performed by clients or an accrediting authority. All external audits
are fully documented and tracked to closure.
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3.8.2.1 Management ensures that all areas of the laboratory are accessible to auditors as
applicable and that appropriate personnel are available to assist in conducting the audit.
3.8.2.2 Any findings related to an external audit follow corrective action procedures.
3.8.2.3 Management ensures that corrective actions are carried out within the timeframe
specified by the auditor(s).
MANAGEMENT REVIEW
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3.9
In accordance with a predetermined schedule and procedure described herein, the laboratory management
periodically and at least annually conducts a review of the laboratory's quality system and environmental
testing activities to ensure their continuing suitability and effectiveness, and to introduce necessary
changes or improvements. The review shall take account of the following:
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a) the suitability of policies and procedures;
b) reports from managerial and supervisory personnel;
c) the outcome of recent internal audits;
d) corrective and preventive actions;
e) assessments by external bodies;
f) the results of inter-laboratory comparisons or proficiency tests;
g) changes in the volume and type of the work;
h) client feedback;
i) complaints; and,
j) other relevant factors, such as quality control activities, resources and staff training.
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Findings from management reviews and the actions or findings that arise from them are recorded
in the minutes and CAPA system as necessary. The management ensures that those actions are
carried out within an appropriate and agreed timeframe. Laboratory management evaluates
actions from previous reviews in each meeting and maintains records of any further findings or
actions as necessary.
3.9.2
MANAGEMENT REVIEW REQUIREMENTS
3.9.2.1 Review Input – The input to management review shall include information on
a)
results of audits,
b)
customer feedback,
c)
process performance and product conformity
d)
status of preventive and corrective actions,
e)
follow-up actions from previous management reviews,
f)
changes that could affect the quality management system, and
g)
recommendations for improvement.
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3.9.1
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3.9.2.2 Review Output – The output from the management review shall include any decisions
and actions related to
a)
improvement of the effectiveness of the quality management system and its
processes,
b)
improvement of product related to customer requirements, and
c)
resource needs.
d)
new findings and actions, as necessary
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SECTION 4 – CLIENT SERVICE FUNCTIONS
4.1
CLIENT CONFIDENTIALITY
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Oilfield Environmental & Compliance (OEC) works in partnership with clients to monitor the
laboratory’s performance in executing the client’s requests. Each request is reviewed to determine the
nature of the request and the laboratory's ability to comply with the request within the confines of
prevailing statutes and/or regulations without risk to the confidentiality of other clients.
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The laboratory confidentiality policy is to not divulge or release any information to a third party without
proper authorization.
All electronic data (storage or transmissions) are kept confidential, based on technology and laboratory
limits, as required by client or regulation.
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For further details, refer to the SOP for Client Interaction, Confidentiality & Complaint Handling.
REVIEW OF REQUESTS, TENDERS AND CONTRACTS
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The President and/or the Laboratory Director do the review of all new work for Oilfield Environmental &
Compliance, Inc. (OEC). The Laboratory Director determines if it has the necessary accreditations and
resources, including schedules, equipment, deliverables, and personnel to meet the work request. By
using the review process, the management is able to determine if it has adequate resources to meet the
requirements of the client. The contract will specify clearly defined requirements and test methods.
The client is informed of the results of the review.
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The Laboratory Director, Laboratory Manager or Quality Assurance Manager will inform the client of
any deviation from the contract including the test method or sample handling processes. All differences
between the request and the final contract are resolved and recorded before any work begins. It is
necessary that the contract be acceptable to both the laboratory and the client.
When the client needs amendments to the original contract, the review process is repeated. The
participating personnel are given copies of the amendments.
COMPLAINTS
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4.3
Oilfield Environmental & Compliance values its customers and provides them with high-quality
analytical testing with the shortest possible turn-around time. OEC reviews all complaints and determines
appropriate action as quickly as possible to assure the customer that complaints are addressed and
corrected. This includes requests to verify results or analytical data.
All customer complaints are documented by the person receiving the complaint and referred to the
Laboratory Director or Laboratory Manager to be addressed. If it is determined that a complaint is
without merit, it is documented, and the client is contacted. If it is determined that the complaint has
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merit, a corrective action is initiated. See Section 3.4.2 of this manual or the SOP for corrective actions
for procedure details.
4.4
SUBCONTRACTING OF TESTS
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A SUBCONTRACT LABORATORY is defined as a laboratory external to Oilfield Environmental &
Compliance, Inc. (OEC) that performs analyses for this laboratory. When subcontracting analytical
services, OEC assures work requiring accreditation is placed with a state of California accredited
laboratory or one that meets applicable statutory and regulatory requirements for performing the tests. A
list of subcontractors and their test methods with certifications is maintained.
OEC notifies the client of the intent to subcontract the work when presenting the contract by stating what
methods the laboratory does not perform and need to be subcontracted. When possible, the laboratory
gains the approval of the client to subcontract their work prior to implementation of a specific work order,
customarily through electronic mail.
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The laboratory performing the subcontracted work is identified in the final report. OEC assumes
responsibility to the client for the subcontractor’s work, except in the case where a client or a regulating
authority specified which subcontractor is to be used.
REPORTING OF RESULTS
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The result of each test carried out at Oilfield Environmental & Compliance is reported accurately, clearly,
unambiguously, objectively and complies with all specific instructions contained in the test method.
The laboratory report should contain all necessary information that is pertinent, including but not limited
to:
a)
all results from analyses performed.
b)
any discrepancies that may have occurred.
Analytical Reports – Each test report generated contains the following information (unless not
required by the client):
a)
a title
b)
the name and address of the laboratory
c)
the name and address of the client if applicable
d)
the identification of the test method used
e)
an unambiguous identification of the sample(s), including the client identification code
f)
the date of sample receipt
g)
the test results with failures identified and units of measurement
h)
the name, function, and signature of the person authorizing the test report, and the date of
issue
i)
at the laboratory’s discretion, a statement that the report shall not be reproduced except in
full without written approval of the laboratory
j)
qualification of results with values outside the working range
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4.5.1
4.5.2
Quality Control Report – A QC report is generated with each sample delivery group, when
applicable or desired by client and contains the following:
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a)
Method Blank Report which includes results of analyte found in the MB and detection
limit for the analyte
Laboratory Control Sample Report that includes percent recovery of analyte in the LCS,
relative percent difference of LCS/LCSD and control limits for percent recovery and
RPD.
Matrix Spike Report that includes percent recovery of analyte in the MS, relative percent
difference of MS/MSD, and control limits for percent recovery and RPD.
Duplicate Report that includes results of analyte found in the sample duplicate, the
dilution factor and detection limit for analyte.
b)
c)
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d)
Case Narrative – A case narrative with a full explanation and all the necessary documentation
should be written if the following occurs:
a)
the chain-of-custody has not been properly administered
b)
the sample cannot be analyzed because of interference
c)
quality control results are in nonconformance
4.5.4
Electronic Transmission of Results – All test results transmitted by telephone, fax, telex, e-mail,
or other electronic means comply with the requirements of this Quality Assurance Manual and
associated procedures to protect the confidentiality and proprietary rights of the client.
4.5.5
Amendments to Test Reports – Amended test reports may be handled in two ways:
a)
if the correction is for anything except actual test results, the report will look the same as
the original; a note will be included explaining the correction.
b)
if a new report is issued because of new test results than the new report will be titled
“Revised”.
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4.5.3
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SECTION 5 – LABORATORY FUNCTIONS
5.1
ACCOMMODATIONS & ENVIRONMENTAL CONDITIONS
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Oilfield Environmental & Compliance (OEC) operates a commercial environmental analytical laboratory
that provides high-quality analytical testing services with a minimum turn-around time. Access to
environmental test areas is limited to OEC personnel. Laboratory workspace is arranged to prevent
contamination of samples and is kept organized and clean to support environmental testing. Interference
from environmental conditions will result in testing being stopped or reanalyzed to assure quality data
results.
5.2
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OEC’s laboratory occupies six thousand five hundred square feet of industrial space. It is currently setup
with separate rooms for sample receiving and storage, volatile analysis, semi-volatile analysis, inorganic
preparation, inorganic analysis, oil and gas preparation, oil and gas analysis and WET chemistry
preparation to ensure non-contamination of samples. In addition, sensitive laboratory areas are arranged
so the flow of a positive-pressure secured air supply helps minimize contamination.
SAMPLE MANAGEMENT
Laboratory analyses are performed to produce data representative of conditions when the sample was
obtained. To ensure integrity, each sample processed at OEC is checked upon receipt, uniquely
identified, stored and disposed of properly, and all relevant information is recorded correctly.
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The laboratory has a sample acceptance policy that specifies the conditions of a sample upon receipt. The
client is immediately notified if these conditions are not met.
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When samples are received at the laboratory, their condition is documented, they are given unique
identifiers, and they are logged into the sample tracking system. The laboratory controls and monitors
sample movement and usage between laboratory departments utilizing an Internal Chain-of-Custody
(ICOC) system. The procedures for preservation checks, sample identification, sample logging, sample
dispersal, and sample storage and disposal is found in the SOPs for SAMPLE LOGIN & SAMPLE
DISPOSAL.
EQUIPMENT
5.3.1
General Equipment Requirements – Oilfield Environmental and Compliance employees operate
and maintain a wide variety of analytical equipment for the performance of a variety of chemical
analysis. All instruments are subject to preventive maintenance procedures per manufacturer
instruction to minimize the occurrence of instrument failure or malfunction. All maintenance is
documented in the appropriate laboratory record.
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5.3
5.3.1.1 Only OEC personnel who are trained and completed an IDoC are allowed to operate
equipment.
5.3.1.2 All equipment is calibrated or checked before being placed into use to ensure that it
meets laboratory specifications and the relevant standard specifications.
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5.3.1.3 Instructions and manufacturers manuals are available to laboratory staff to indicate the
proper use and maintenance of equipment.
5.3.1.4 Equipment that is defective or outside specifications is clearly labeled as being out of
service. Small support equipment such as thermometers would be immediately discarded.
Support Equipment – Support equipment includes devices for weighing, measuring, heating or
cooling standards or samples. These are also purchased from reputable companies and calibration
and functionality are verified at the time of receipt. All support equipment is maintained in
proper working order and records are kept of all repair and maintenance activities, including
service calls. For further details refer to the OEC SOP: Small Instrument-Support Equipment
Calibration & Monitoring
5.3.3
Analytical Equipment – All equipment at OEC is properly maintained, inspected, and cleaned.
Maintenance of analytical instruments and other equipment may include regularly scheduled
preventive maintenance or maintenance on an as-needed basis due to instrument malfunction and
is documented in Instrument Maintenance Logs, which become part of the laboratory’s
permanent records. Initial and Continuing Calibration of each instrument is performed according
to the test method SOP being carried out.
5.3.4
Equipment List – Refer to Appendix B
5.4
REFERENCES FOR ANALYTICAL METHODS
5.4.1
Test Methods for Evaluating Solid Waste: Physical/Chemical Methods, U.S. Environmental
Protection Agency, SW-846, Third Edition (September 1986), Final Update I (July 1992), Final
Updates II and IIA (September 1994), Final Update IIB (January 1995), and Final Update III
(December 1996).
5.4.2
Standard Methods for the Examination of Water and Wastewater, American Public Health
Association, American Water Works Association, Water Pollution Control Federation, 18th
Edition, 1992; 19th Edition 1995; 20th Edition 1999.
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5.3.2
Draft Method for Total Petroleum Hydrocarbons and Total Organic Lead, Hazardous Materials
Laboratory, California Department of Health Services, Berkeley, CA, February, 1988.
5.4.4
Leaking Underground Fuel Tank & Site Mitigation Unit Manual, Santa Barbara County Fire
Department, Fire Prevention Division, January 2007.
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5.4.3
5.4.5
Criteria for Identification of Hazardous and Extremely Hazardous Wastes, California Code of
Regulations (CCR), Title 22, Division 4.5
5.4.6
HAZCAT: A System of Field Identification and Classification of Commonly Spill Materials,
State of California, Division of Occupational Safety and Health, Department of Industrial
Relations, September, 1986.
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Oilfield Environmental & Compliance, Inc.
Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air,
Center for Environmental Research and Development Office of Research Development US EPA,
January 1997, TO-14.
5.4.8
Clean Water Act (CWA) Analytical Test Methods, Code of Federal Regulations (CFR), Title 40
Part 136.
5.4.9
ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 194282959, United States.
5.5
QUALITY OF TEST RESULTS
5.5.1
Essential Quality Control Procedures – All essential quality control elements are collected and
assessed on a continuing basis. The qualities of test results are recorded in such a way that trends
are detectable, and where practicable, are statistically evaluated. There is a Standard Operational
Procedure (SOP) for each test method that Oilfield Environmental & Compliance uses. Section 9
of each SOP lists the Quality Control criteria. This is sometimes supplemented with quickreference criteria in a table format in the Appendices area of the SOP.
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5.4.7
All laboratory personnel follow the quality control procedures specified in test methods. The most
stringent of control procedures is used in cases where multiple controls are offered. If it is not
clear which is the most stringent, that mandated by test method or regulation is followed.
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5.5.1.1 To monitor the validity of environmental tests performed, review includes any one or
combination of the techniques below:
a)
Utilizing certified reference materials and/or internal quality control using
secondary reference materials;
b)
participation in proficiency testing programs;
c)
replicate testing using the same or different methods;
d)
retesting of retained samples;
e)
correlation of results for different characteristics of a sample.
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5.5.1.2 Written procedures to monitor quality controls, including acceptance criteria, are located
in the test method SOPs, except where noted, and include such procedures as:
a)
use of laboratory control samples and blanks to serve as positive and negative
controls for chemistry methods;
b)
use of laboratory control samples to monitor test variability of laboratory results;
c)
use of calibrations, continuing calibrations, certified reference materials and/or
PT samples to monitor accuracy of the test method;
d)
measures to monitor test method capability, such as limit of detection, limit of
quantitation, and/or range of test applicability, such as linearity;
e)
use of regression analysis, internal/external standards, or statistical analysis to
reduce raw data to final results;
f)
use of reagents and standards of appropriate quality;
g)
procedures to ensure the selectivity of the test method;
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Internal Quality Control Practices – Analytical data generated with QC samples that fall within
prescribed acceptance limits indicate the test method is IN CONTROL. QC samples that fall
outside QC limits indicate the test method is OUT OF CONTROL (non-conforming) and that
corrective action is required or that the data are qualified. Oilfield Environmental &
Compliance’s QC procedures and QC limits are included in test method standard operating
procedures (SOPs), or where unspecified in the SOPs, are detailed elsewhere. All QC measures
are assessed and evaluated on an on-going basis, so that trends are detected. Please refer to
Appendix F, QC Data Evaluation Flowcharts for a more detailed description of general standard
corrective actions followed by the laboratory.
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5.5.2.1 The following general controls are used:
1. Positive and Negative Controls such as:
a)
Blanks (negative)
b)
Laboratory control sample (positive)
c)
Reference Toxicants (positive)
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2. Selectivity is assured through:
a)
absolute and relative retention times in chromatographic analyses
b)
two-column confirmation when using non-specific detectors
c)
two different GC detectors
d)
use of acceptance criteria for mass-spectral tuning (found in test method SOPs);
e)
use of the correct method according to its scope assessed during method
validation;
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3. Consistency, Variability, Repeatability, and Accuracy are assured through:
a)
proper installation and operation of instruments according to manufacturer’s
recommendations or according to the processes used during method validation
b)
monitoring and controlling environmental conditions (temperature, access,
proximity to potential contaminants)
c)
selection and use of reagents and standards of appropriate quality
d)
cleaning glassware appropriate to the level required by the analysis. Cleaning
procedures are provided in test method SOPs
e)
following SOPs and documenting any deviation, assessing for impact, and
treating data appropriately
f)
testing to define the variability and/or repeatability of the laboratory results, such
as replicates
g)
use of measures to assure the accuracy of the test method, including calibration
and/or continuing calibrations, use of certified reference materials, proficiency
test samples, or other measures
5.5.2.2 Acceptance or rejection criteria are created according to laboratory policy where no
method or regulatory criteria exist. Acceptance criteria define the boundary for the appropriate
response from laboratory personnel, such as corrective action, reporting with qualifiers,
reanalysis, review, and others.
1. Test Method Capability is assured through:
a)
establishment of the method detection limits where appropriate
b)
establishment of the practical quantitation limits or reporting level
c)
establishment of the range of applicability such as linearity
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2. Data reduction is assured to be accurate by:
a)
selection of appropriate formulae to reduce raw data to final results such as
regression
b)
periodic review of data reduction processes to assure applicability
Negative
Control
(Method Blank)
Positive
Control
(Laboratory
Control
Sample)
Matrix Spike;
Matrix Spike
Duplicates
Surrogate
spikes
Initial
calibration
Verification
Reprocess, reanalyze,
or qualify data.
Method specific
or determined by
laboratory
Corrective action and
qualify data.
Per method
requirement
Method specific
or determined by
laboratory
Corrective action and
qualify data
Per method
requirement
Method specific
or determined by
the laboratory
Reanalyze standard
immediately;
Corrective action
Start of each
analytical run
Method specific
or determined by
laboratory
Reanalyze standard
immediately;
Corrective action
Per method
requirement
Method Blanks – A reagent or method blank (MB) is prepared and analyzed with each day’s
samples (24 hour period) at a minimum of one sample per 20 or less samples of the same matrix.
The volume of the blank should be approximately equal to the sample. Analysis of the blank
verifies that method interferences caused by contaminants in solvents, reagents and equipment are
known and minimized. Target analyte should be non-detected in a method blank.
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5.5.3
Qualify data and take
corrective action
Method specific
or determined by
laboratory
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Continuing
Calibration
Verification
1/batch
Corrective action
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Item
Essential Quality Control Elements for Chemistry
Acceptance
Frequency
Criteria
1/batch
Method specific
or reporting limit
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Table 5A
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The following table summarizes the key elements of a quality control system for a laboratory performing
chemical analyses.
Laboratory Control Samples – Standard reference materials or laboratory control samples (LCS)
from an independent source are introduced periodically (at least once per day during testing
activity) into the testing scheme to evaluate testing procedure. Duplicate LCS (LCSD) may be
analyzed in lieu of MS/MSD if necessary.
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5.5.4
5.5.5
Matrix Spikes and Matrix Spike Duplicates – One sample in every batch (20 or less samples) is
spiked in duplicate at a level, which provides a final concentration greater than or similar to the
original concentration before dilution. This provides a matrix spike (MS) and matrix spike
duplicate (MSD) from which to evaluate laboratory accuracy (spike recovery) and precision
(relative percent difference between duplicates).
5.5.6
Surrogate Spikes – SURROGATES are substances with chemical properties and behaviors
similar to the analytes of interest used to assess method performance in individual samples.
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Surrogates are added to all samples (in test methods where surrogate use is appropriate) prior to
sample preparation or extraction. Surrogate recovery results are compared to the acceptance
criteria as published in the mandated test method.
5.5.7
Data Review – Oilfield Environmental & Compliance reviews all data generated in the laboratory
for compliance with method, laboratory and, where appropriate, client requirements.
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The analyst should compile the results of the above validation samples onto the laboratory
logbooks and LIMS system. The analyst electronically signs his work in LIMS and should sign
and date his own logbooks. Any correction must be crossed out with a single line and be dated
and initialed. All QC method parameters are verified within the LIMS system by the analyst. If
the batch contains any QC issues, a corrective action report should be completed and submitted to
the Department Manager with the raw data and the Quality Assurance Manager.
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The Department Manager or a qualified peer should review the raw data and approve the
preliminary results in the raw data file and LIMS. The reviewer should counter-sign and date the
logbooks and the raw data. Any QC problems should be noted in the batch case narrative or as a
corrective action report.
The Department Manager should review the QC parameters for each set of data and approve the
QC results in the file. Any corrective action or narrative must be reviewed and related samples
validated as necessary by the Department Manager or Quality Assurance Manager prior to draft
report generation. Draft reports are then submitted to the Laboratory Director for final approval.
Control of Data – All pertinent data that are subject to transcription, calculation, or other manual
manipulation is checked in a systematic manner. All commercial software used at OEC is in an
application range that is considered sufficiently validated for use in the laboratory.
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5.5.8
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OEC’s procedure to insure that reported data is free from transcription and calculation errors, and
all quality data has been calculated correctly, is to have all quality control data reviewed by
Department Manager and Laboratory Manager before being released to client. Computers and
software are protected, maintained, and secure through measures such as document controls,
locked access, and control of the laboratory environment.
ACKNOWLEDGMENT:
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This manual was created with help from the INELA Template ver.1
OEC Quality Systems
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Oilfield Environmental & Compliance, Inc.
APPENDIX A –
CONTACT & QUALIFICATIONS OF KEY PERSONNEL
To contact your desired party, dial the OEC main number at (805) 922-4772 and either ask for
them by name or if prompted for an extension, use as listed:
Laboratory Director
jcarstens@oecusa.com
x1100
Direct: (805) 354-7301
Lisa Race
Laboratory Manager
lrace@oecusa.com
x1310
Direct: (805) 354-7302
Carrie McCrillis
Quality Assurance Manager
cmccrillis@oecusa.com
x1101
Marissa Censullo
Project Manager
mcensullo@oecusa.com
x1111
Direct: (805) 354-7303
Roy Diaz
Project Manager
rdiaz@oecusa.com
x1113
Meredith Sprister
Project Manager
msprister@oecusa.com
x1112
Direct: (805) 354-7304
Jesse DeLaCruz
Technical Supervisor
jdelacruz@oecusa.com
X1601
Gracie Venegas
Operations Coordinator
gvenegas@oecusa.com
X1301
Direct: (805) 354-7305
Maryann Long
Volatile Organic
Department Manager
mlong@oecusa.com
x1201
Dwain Zsadanyi
Semi-Volatile Organic
Department Manager
dzsadanyi@oecusa.com
x1501
Drew Miller
Wet Chemistry
Department Manager
dmiller@oecusa.com
x1701
Parwinder Parmar
Metals Department Manager
pparmar@oecusa.com
x1300
Pete Alcocer
Oil Production
Client Services &
Operations Consultant
palcocer@oecusa.com
x1401
Roger Dickinson
Field Operations Supervisor
rdickinson@oecusa.com
x1401
Cynthia Crawford*
Accounting Coordinator
ccrawford@oecusa.com
x1102
Kevin Calcagno*
Sales & Contracts Rep.
kcalcagno@oecusa.com
(805) 354-7306
John Hatzman*
Sales & Contracts Rep.
jhatzman@oecusa.com
(805) 354-7307
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Julius Carstens
* Included for contact reference information only, qualifications not included
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Oilfield Environmental & Compliance, Inc.
Julius Carstens, Laboratory Director
(Page 1of 2)
QUALIFICATIONS
EDUCATION & CERTIFICATIONS
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Mr. Carstens has been the owner and primary operator of OEC since 1997. Prior to that, he acquired
extensive experience in the environmental and oil production analytical fields through education and
hands-on experience in both a laboratory and field environment.
B. S. Biochemistry, 1995, California Polytechnic State University, San Luis Obispo, CA

B. S. Soil Science, 1995, California Polytechnic State University, San Luis Obispo, CA

Registered Environmental Assessor (California Environmental Protection Agency. REA # 06476)

OSHA HAZWOPER 8-hour Supervisor & 40-hour Trained (OSHA 29 CFR 1910.120)

SECORP Industries Safety Class for H2S

California Water Environment Association (Laboratory Analyst # 311)
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EXPERIENCE
1997-Present
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Laboratory Director- Mr. Carstens manages operations for the analytical laboratory and field service
firm. He has over 20 years laboratory experience in the analysis of environmental samples and has
worked on numerous field sampling projects during this time. Mr. Carstens has extensive experience in
the areas of air, gas, soil/water, and petroleum analysis, EPA protocols, and field sampling. He is
responsible for overall management of technical operations, technical consulting functions, personnel
development and business operations including the direction of the financial and marketing departments.
Mr. Carstens consulting responsibilities include advising clients of the appropriate sampling and
analytical protocols primarily related to, air and oil testing. He is integrally involved in data interpretation
with the clients on such projects. He has also participated in the development of new sampling and
analysis protocols for the measurement of gas and petroleum characteristics. OEC has developed a
working relationship with the oil companies in the Santa Maria Valley and also government agencies
responsible for environmental monitoring, such as the APCD.
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Oilfield Environmental & Compliance, Inc.
Julius Carstens, Laboratory Director
(Page 2of 2)
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1993-1997
Cirrus Environmental, Santa Maria, CA
Soil & Chemist/Project Coordinator - Responsible as project coordinator for laboratory based projects.
Performed chemical analysis for laboratory and coordinated specific organic and inorganic analyses.
Provided client consultation to assist in the determination of analytical methods most appropriate for their
project.
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1990-1993
Cal Poly State University, San Luis Obispo, CA
Worked as a laboratory technician to determine the change in soil cation exchange of soils amended with
synthetic organic polymers. Also worked on the bio-degradation rate of diesel fuel, gasoline, and motor
oil, using in situ bacteria CO2 respiration rates.
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MONITORING PROJECTS - Limited scope of monitoring projects that Mr. Carstens has performed:
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Venoco Inc., South Ellwood Oil & Gas Facility, Santa Barbara, CA
He performed sample design, equipment selection, and analytical methods, for the determination of
petroleum and H2S odor being emitted by the loading of a petroleum barge. Determination of sampling
points and interval of sampling was determined, while on the barge for a 48-hour period. This remote site
was tested on two separate occasions, during the loading of 75,000 barrels of crude oil. Over 60 samples
were taken during each loading event. Results of C1-C6 hydrocarbons, fixed gasses, and hydrogen
sulfide, were available to the client within a 3-day period.
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Torch Operating Co. HS&P Facility, Lompoc, CA
Worked with Torch staff and Santa Barbara APCD to determine the accuracy of Del Mar Testing Unit
located at HS&P. OEC provided a staff of technicians to gather 45 minute interval sampling from a
produced gas stream. This sampling event ran continuously for 72 hours. All samples were analyzed for
hydrogen sulfide. The data from these tests assisted Torch in proper equipment replacement of the Del
Mar unit. With the instillation of a new gas processing system, OEC has been asked to conduct weekly
sampling and analysis of HS&P waste gas for hydrogen sulfide and mercaptans. OEC is also on call for
the analysis of butane & propane mix, being produced by the HS&P facility. Analysis consists of field
sampling, field-testing, and laboratory testing.
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Dole Dried Fruit Co. Raisin Facility, Fresno, CA
While working for Cirrus Environmental, Inc., Mr. Carstens designed and implemented a two-week study
of PM 10 emissions. The objective of the test program was to determine the PM 10 emissions from raisin
dust, and determine if this facility was operating within their APCD permit. Four high volume samples
were located around the perimeter of the testing facility. The method used during this test program was
40CFR Part 50 App. B PM10 High Volume Method.
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Oilfield Environmental & Compliance, Inc.
Lisa Race, Laboratory Manager & Safety Officer
(Page 1of 3)
QUALIFICATIONS
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Ms. Race has over 25 years of experience using organic, inorganic and air toxic methodologies. She
brings to OEC a strong working knowledge of applicable regulations regarding air, water, wastewater and
hazardous waste testing and disposal. Included are several years experience performing all aspects of
Environmental Health and Safety function.
EDUCATION
B.S. Biochemistry, 1984, University of Wyoming
Certificate in Hazardous Materials Management (partial)
Certificate in D.O.T. shipping and handling
Certificate in Fundamental Ergonomics
Certificate in Leadership and Management Training (multiple certificates)
EXPERIENCE
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2008-Present
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



Ms. Race is responsible for daily laboratory function and management. Her extensive laboratory
experience is utilized to maximize laboratory function and efficiency, and serves as a client resource for
projects and data consultation.
TEST AMERICA Inc., Morgan Hill, CA
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2001-2008
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Senior Project Manager- Coordinated with clients, laboratory personnel and subcontract laboratories to
track and report results for projects. Responsible for all aspects of managing 3 of the top 10 clients
including creating quotes, adding or updating bid in the LIMs system, reviewing SOWs and ensuring all
project requirements were met. Responsible for creating invoices, EDDs, geotracker EDFs and PDF
reports. Responsible for reviewing CLP data packages and training personnel on how to create the final
CLP packages using the raw data and the final reports.
Volatiles Department Manager- Responsible for interviewing, hiring and training new personnel for the
department. Set up the 8260 full list, 524 and 624 methods and streamlining the 8015/8021 analyses.
Increased productivity by 500%. Set up all new instrumentation and instructed analysts in how to use
them. Responsible for scheduling sample analyses and personnel to ensure samples were analyzed within
holding time and met TAT.
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Oilfield Environmental & Compliance, Inc.
Lisa Race, Laboratory Manager & Safety Officer
2000-2001
(Page 2of 3)
Cirrus Environmental Inc., Santa Maria, CA
1994-2001
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Laboratory Director- Oversaw all aspects of the laboratory including certification, training, quality
control, sample analysis, field sampling, project management and client contact. Coordinate all
subcontract work. Assist the marketing director in preparing quotes and evaluating and bidding on
specific projects.
Environmental Analytical Service Inc., San Luis Obispo, CA
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Laboratory Supervisor- Managed the laboratory by creating a smooth flow of information, sample
distribution, sample analysis, data reduction and data review and ensuring that project specifications were
met. Coordinate the flow of information between the laboratory and administration by establishing
standard procedures for the dissemination of information and establishing routine meetings between
laboratory and administrative staff to discuss current or potential problems. Modified laboratory
procedures to reduce the standard sample turnaround time from 20 working days to less than 14 working
days. Instituted method modifications which decreased gas usage and resulted in reducing the laboratory
gas budget by forty percent. Set up a “rewards” program to improve employee morale.
1991-1994
Coast to Coast Analytical Services, San Luis Obispo, CA;Tempe, AZ
U
nc
Mobile Laboratory Manager- Managed mobile laboratory projects including on and off site client contact,
analyzing samples, reviewing data and generating reports. Set up the Los Angeles site long term mobile
lab project which resulted in generating a profit rather than a loss for Mobile Lab #2. Responsible for
setting up the Arizona mobile laboratory including obtaining all necessary permits and certifications in
order to meet Arizona state regulatory requirements. Implemented and audited quality assurance/quality
control guidelines. Created and/or updated mobile laboratory Standard Operating Procedures documents.
Trained and supervised employees in mobile laboratory procedures.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 38 of 89
Oilfield Environmental & Compliance, Inc.
Lisa Race, Laboratory Manager & Safety Officer
1987-1991
(Page 3of 3)
Enseco-CRL, Santa Maria, CA
on
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d
Environmental Chemist: Organics- Headed and performed all organic operations within 1 year of initial
training. Trained and supervised back-up analysts on all organic analyses.
Environmental Chemist: Inorganics- Planned and implemented the set-up of the inorganic laboratory by
modifying and customizing methodologies, allowing efficient use of available resources while offering a
greater variety of services to the customer. Trained and supervised all aspects of the inorganics
laboratory. Acted as a back-up analyst for inorganics after moving to organics.
Quality Assurance/Quality Control Coordinator- Assumed the major responsibility for responding to
quality control questions from clients. Reviewed all data to ensure that it met with all quality assurance
guidelines prior to release to customers.
Environmental Health and Safety Coordinator- Conducted hazardous communications training for new
and current employees. Managed facility hazardous and non-hazardous waste disposal and recycling per
all applicable regulations. Completed required reports on facility emissions per applicable regulations.
Trained employees in proper handling and shipping techniques, including dangerous goods shipping.
Tracked and updated current chemical inventory.
Program Administration- Gathered information specific to the size and scope of projects including any
specific quality assurance/quality control and reporting requirements. Tracked project status from
acceptance of samples to release of report, notifying clients of any problems that would affect project
specifics. Reviewed final reports prior to release to ensure they met all project specifics.
1984-1987
Wyoming Department of Agriculture-Division of Laboratories, Laramie
U
nc
Analyzed private and municipal waters and wastewaters for all inorganic parameters required. Extracted
pesticide residues in foliage samples.
Analyzed tissue samples for strychnine using liquid
chromatography.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 39 of 89
Oilfield Environmental & Compliance, Inc.
Carrie McCrillis, Quality Assurance Manager &
Human Resources Representative
(Page 1of 2)
QUALIFICATIONS
lle
d
Ms. McCrillis has over 10 years of experience in the environmental laboratory and quality-system
management field. Environmental laboratory experience includes performing as an analyst, Quality
Assurance Manager, safety officer, project manager and laboratory director. Proficient in environmental
contract review and data package compilation, EPA methodology and quality control systems, national
and state regulatory agency requirements (NELAP/ELAP), ISO QMS, CLP & GLP protocols for data
verification and validation.
EDUCATION
B.S., Chemistry, California Polytechnic State University, San Luis Obispo, CA, 1999
OSHA 40-Hour Hazmat Training Certificate + Refreshers
ISO Internal Auditor Training, 2006 (ASQ certified)
AFFILIATIONS
American Chemical Society (ACS)
American Society for Quality (ASQ)
on
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EXPERIENCE
nc
2008-Present
U
Quality Assurance Manager – Responsibilities include maintenance of OEC Quality Systems, including
maintenance of state certification and all documentation related thereto. Including, but not limited to,
maintaining and updating all standard operating procedures, quality assurance manual, and the statement
of qualifications. Maintenance of quality documentation and organization as necessary related to
instrument controls, employee training, corrective & preventive action, performance evaluations, and
laboratory audits.
2006-2008
Celite, World Minerals Inc., Imerys – Lompoc, CA
Quality System Specialist – Responsible for the maintenance of the site ISO certification and monitoring
of quality system protocols, training, documentation, and internal audits. Performed general supervision
and payroll processing for QC laboratory personnel. Participated in implementation and training for
multiple enterprise-level software systems including IFS/THERMO-LIMS (ERP), Kronos (Payroll &
Timekeeping), & Intelex (quality management software).
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 40 of 89
Oilfield Environmental & Compliance, Inc.
Carrie McCrillis, Quality Assurance Manager &
Human Resources Representative
ZymaX envirotechnology, inc. – San Luis Obispo, CA
d
2002 – 2005
(Page 2of 2)
lle
2002-2005 Quality Assurance Officer – Responsibilities include management and revision of the QA
Program including maintenance of state certification and all documentation related thereto. Including, but
not limited to, all administrative and laboratory standard operating procedures, control documentation for
all laboratory instruments, documentation of technical and analytical training for all analysts,
documentation and monitoring of laboratory corrective actions, and organization of all performance
evaluations and audits. Additionally responsible for the compilation of CLP and contract-design data
packages.
1999-2002
tro
2003-2005 Safety Officer – Responsibilities include organization and maintenance of all safety-related
hardware, consumables & documentation for the laboratory. Primary contact for any city, county, fire
department or OSHA inspections. Responsible for overall employee safety awareness including annual
training refreshers.
Cirrus Environmental, Inc. – Santa Maria, CA
on
2001-2002 Laboratory Director – Oversaw laboratory operation and supervised all chemists, laboratory
technicians and field technicians. Administered the Quality Assurance Program and was responsible for
overall laboratory data quality as the primary signatory. Provided guidance for all analytical
methodology and procedures. Responsible for the maintenance of laboratory certification through
California ELAP. Acted as project manager and technical contact for all clients.
nc
1999-2001 Quality Assurance / Quality Control Officer – Reviewed all analytical data to meet quality
control objectives prior to report generation. Responsible for all analytical report generation, including
samples, QC and data packages. Responsible for maintenance and revision of the laboratory Quality
Assurance Program and any internal or external audits. Maintenance of all laboratory quality
documentation and state certification.
U
Former positions held at Cirrus include organic & inorganic analytical chemist and extraction technician.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 41 of 89
Oilfield Environmental & Compliance, Inc.
Marissa Censullo, Project Manager
(Page 1of 1)
QUALIFICATIONS
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d
Ms. Censullo has several years of experience in the environmental laboratory industry. She has a strong
working knowledge of applicable methods and regulations regarding air, water, wastewater and hazardous
waste testing and disposal. She has an analytical background with environmental methods and
instrumentation.
EDUCATION
B.S. Environmental Science and Policy, 2010, Concentration in Environmental Science,
University of South Florida, St. Petersburg FL
on
EXPERIENCE
tro

2011-Present
nc
Ms. Censullo is responsible for final laboratory data review, report generation and dissemination. She
serves as primary client contact for laboratory and project activity. Previous responsibilities include
performance of extractions and analyses in the Wet Chemistry & Inorganics Department.
Jun-Dec 2010
U.S.G.S. Coastal and Marine Science Center, St. Petersburg, FL
U
INTERNSHIP – Retrieved, organized, and analyzed environmental data that had been collected on
physical, chemical and nutrient variables for waters in Florida Bay and Biscayne National Park. Used
ArcGIS software to produce digital products including shapefiles overlain on an interactive map, and a
series of graphs linked to shapefiles.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 42 of 89
Oilfield Environmental & Compliance, Inc.
Meredith Sprister, Project Manager
(Page 1of 1)
QUALIFICATIONS
lle
d
Ms. Sprister has several years of experience in the environmental laboratory industry. She has a strong
working knowledge of applicable methods and regulations regarding air, water, wastewater and hazardous
waste testing and disposal. She has an analytical background with environmental methods and
instrumentation.
EDUCATION
B.A. Environmental Studies, Minor in Music, 2008 University of California, Santa Barbara
EXPERIENCE
2010-Present
tro
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on
Ms. Sprister is responsible for final laboratory data review, report generation and dissemination. She
serves as primary client contact for laboratory and project activity. Previous responsibilities include
performance of extractions and analyses in the Wet Chemistry & Inorganics Department.
2009-2010
Creek Environmental Laboratories, San Luis Obispo, CA
nc
Inorganics & Wet Chemist / Laboratory Technician – Prepared and analyzed soil, drinking water and
aqueous samples on laboratory machinery including ICP-MS, ICP-OES, Mercury by Cold Vapor AA and
Flame AA. Performed STLC and TCLP extractions and analyses. Performed wet chemistry tests
including Ferrous Iron, Orthophosphate, Fluoride by ISE, Hexavalent Chromium in water and soil,
MBAS and Chemical Oxygen Demand. Performed short holding time tests including pH, turbidity, EC,
color, odor and salinity. Proficient at all EPA Metals digestion methods including 3050, 3060, 3005,
200.7/.8 and 3010. Performed instrument maintenance. Some experience with quality assurance and
laboratory management.
U
2006-Present
Drive Customs, San Luis Obispo, CA
Website Manager & Bookkeeper
Development and maintenance of a fully functional website including photos, contact information and
basic HTML (www.drivecustoms.com). Bill paying, invoice preparation, basic accounting and
reconciliation using QuickBooks. Internet promotion, business card and logo design. Preparation of lease
paperwork, dealer agreements and other technical documents.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 43 of 89
Oilfield Environmental & Compliance, Inc.
Jesse A. De La Cruz, Technical Supervisor
(Page 1of 2)
QUALIFICATIONS
lle
d
Mr. De La Cruz has over 15 years of experience in the environmental field ranging in areas from method
development, laboratory management, field sampling, machine troubleshooting, maintenance, repair, and
supervision.
EDUCATION
A. Biology, 1993, Allan Hancock College, Santa Maria, CA

OSHA HAZWOPER 40 hour Trained (OSHA 29 CFR 1910.120)
EXPERIENCE
2002–Present
tro

on
Mr. De La Cruz is responsible for the scheduling, maintenance, and verifying QA/QC parameters are met
for all data for the Semi-Volatile and Inorganic laboratories. He is primarily responsible for any new
method development, the analysis of proficiency testing (PT) samples, analysis of MDL / RL / DoCs for
all supervised personnel, and training of technicians and analysts within these laboratories.
2001–2002
ZymaX Envirotechnology, San Luis Obispo, CA
U
nc
Inorganics/Semi-Volatiles Lab Manager– Mr. De La Cruz oversaw the daily operations of the inorganic
and semi-volatiles department, making sure that holding times, QA/QC controls, and turn-around-times
were met. Inorganics responsibilities included method development on IC for Hexavalent Chromium by
EPA 218.6 and EPA 1799 and for perchlorates by EPA 314.0. He was trained by Agilent on ICP/MS
applications/software and by Metrohm Peak on IC applications/software. Semi-volatile responsibilities
included troubleshooting, analysis, preventative maintenance, scheduling, data approval, and occasional
preparation of samples. He oversaw and assisted in the testing of environmental check samples. He
managed and scheduled 3 analysts, 5 lab technicians in the inorganics lab and 4 analysts, 14 lab
technicians in the semi-volatiles lab. Mr. De La Cruz performed CLP type work and helped in the
approval and writing of standard operating procedures. He was responsible for ordering supplies and he
signed and approved all data generated by the departments.
Instrumentation used in the inorganics department- Hewlett Packard 4500 ICP/MS, ARL 3410 ICP,
Metrohm Peak IC, Leeman Labs Cold Vapor Mercury Analyzer, Accumet ISE meter, Fisher pH meter, 10
position midivap cyanide distillation apparatus, Environmental Express 54 position hot block digestor.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 44 of 89
Oilfield Environmental & Compliance, Inc.
Jesse A. De La Cruz, Technical Supervisor
(Page 2of 2)
Harding/ESE, Santa Maria, CA
lle
1999–2001
d
Instrumentation used in the semi-volatiles department- Hewlett Packard 5890 GC with 5971 Mass
Spectrometer – with 7673 autosamplers, Hewlett Packard 6890 GC with dual ECD, Zymark Turbovap,
Ultrasonic dual horn disruptors. Methods performed in the semi-volatiles department: EPA 8270 BNA,
8270 PNA and PNA SIM, Hydrocarbon, Methanol, Ethanol, 1,4-Dioxanes all using the GC/MS systems;
EPA methods 8081 Pesticides, 8082 PCB’s, and EPA 504 using the GC with dual ECD system.
1993–1999
tro
Health and Safety Officer/Field Technician- Mr. De La Cruz oversaw excavations of petroleum
containing sumps in the Santa Maria Valley. He was responsible for the sampling and testing of
environmental samples and the safety of workers on the job site. He helped write Site Assessment Plans,
Health and Safety Plans, and Site Restoration Plans for Unocal projects.
Cirrus Environmental, Santa Maria, CA
on
1996-1999– Operations Supervisor/Quality Control Officer- Mr. De La Cruz supervised routine
operations and implemented quality control measures. He supervised 22 chemists, analysts, and
technicians in organic and inorganic analyses, including AA, ICP, GC, GC/MS, and general chemistry.
He reviewed all analytical data. He implemented corrective actions and generated corrective action
reports. He was responsible for troubleshooting and preventative maintenance of the AA, ICP, GC,
GC/MS instruments. He oversaw and assisted in the testing of environmental check samples. He assisted
in the approval and writing of most of the Standard Operating Procedures.
nc
1994-1996– Organic Analytical Chemist/Health and Safety Officer– Mr. De La Cruz was responsible for
sample preparation, analysis, reporting, stocking, and maintenance of 8240, 8260, 8270, and 524.2 using
Hewlett Packard 5890 GC with 5972 Mass Spectrometers. His other duties included the training of
chemists in AA, ICP, GC, GC/MS, general wet chemistry, and field sampling techniques. As the health
and safety officer, his responsibilities included industrial hygiene and compliance with OSHA regulations
as well as for stocking personal protective equipment and the updating of MSDS.
U
1993-1994– Inorganic analytical Chemist- Mr. De La Cruz was responsible for the supervision of 7
laboratory technicians in inorganic bench-top chemistry, ICP and AA. Other duties included the analysis
and generation of reports for hazardous wastes in wastewaters, soils, and drinking water samples. He
performed various field sampling for ground water monitoring wells and managed all sampling for the
City of Santa Maria Landfill monitoring wells. Other experience included treatability studies, in situ, and
excavated bioremediation techniques and hazardous waste minimization techniques. He is experienced in
the monitoring of air samples and regulatory compliance using NIOSH protocols. He is able to use PID,
OVA, H2S Meter, Turbidity Meter, Dissolved Oxygen Probe, Field pH/Conductivity/ Temperature
Meter, well depth gauges, Petroflag screening kit, and the Sensidyne HAZ CAT test kit for the
characterization of waste stream materials.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 45 of 89
Oilfield Environmental & Compliance, Inc.
Gracie Venegas, Operations Coordinator
(Page 1of 1)
QUALIFICATIONS
d
Ms. Venegas has been performing administrative functions in the environmental industry since 1987
including management, operations, and purchasing.
lle
EXPERIENCE
2005-Present
2001-2005
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Ms. Venegas is responsible for workflow of laboratory projects from log-in through completion.
Coordination of couriers, client services & communication, and requisition of laboratory purchases.
Management of sample control/office personnel.
ZymaX Envirotechnology, San Luis Obispo, CA
on
Operations Manager- Responsible for workflow of environmental laboratory projects after log-in through
completion. Coordination of couriers, client services, organization of sample and waste disposal, and
requisition of analytical purchases. Includes management of front office personnel and overseer of all
facilities management.
1999-2001
WZI, Santa Maria, CA
Office Manager- Ms. Venegas handled client communication, including the management of proposals.
Responsible for monitoring lab data, project costs, personnel and general clerical duties.
1991-1998
Cirrus Environmental, Santa Maria, CA
nc
Office Manager- Ms. Venegas generated reports and proposals. She supervised office personnel and
handled supply purchasing. Secretary to the company President.
1987 – 1990
Casmalia Resources – Santa Maria, CA
U
Secretary/Receptionist – Secretary to Director of Engineering and Site Operations. Supervision of office
personnel. General clerical duties.
1982 – 1987
Rockwell International – Santa Maria, CA
Secretary/Travel Coordinator/Industrial Security – Responsible for itinerary and workup of travel
packages. Security Officer processing new hires and terminations, security clearances, safety training,
security briefing. Coordination and requisition of office supplies. General clerical duties.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 46 of 89
Oilfield Environmental & Compliance, Inc.
Maryann Long, Volatile Organics Manager
(Page 1 of 2)
QUALIFICATIONS
lle
EDUCATION & CERTIFICATION
d
Ms. Long has over 15 years hands-on experience as a chemist, supervisor and laboratory manager in the
environmental field.
B.S., Biology, California State University, San Bernardino, 1979

Laboratory Analyst Grade 3 by CWEA

Certified Manager by Institute of Certified Professional Managers

First Aid and CPR
AFFILIATIONS
California Water Environment Association (CWEA); Tri-Counties Regional Section of CWEA
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EXPERIENCE
2011–Present
nc
Ms. Long is responsible for the scheduling, maintenance, and verifying QA/QC parameters are met for all
data from the Volatile Organic Laboratory. She is primarily responsible for any new method
development, the analysis of proficiency testing (PT) samples, analysis of MDL / RL / DoCs for all
supervised personnel, and training of technicians and analysts within this department.
U
2011
Colorado State University, Center for Environmental Management of Military
Lands – Camp Roberts, CA
Environmental Technician – Assisted in the preparation of environmental documents according to the
National Environmental Policy Act (NEPA) and California Environmental Quality Act (CEQA)
requirements. Included the tracking of NEPA documents on the Share Point database. Reviewed and
commented on environmental reports, technical documents, sampling data and Environmental Condition
of Property (ECOP) documents. Assisted in site visits to activities and tenants on Camp Roberts to
review environmental requirements and ensure compliance with laws and regulations. Provided
contractor oversight for environmental projects. Oversaw the collection, management, and disposal of
hazardous waste through satellite accumulation sites and the central accumulation points.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 47 of 89
Oilfield Environmental & Compliance, Inc.
Maryann Long, Volatile Organics Manager
Creek Environmental Laboratory/Centauri Labs – San Luis Obispo, CA
d
1996–2010
(Page 2 of 2)
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2000-2010 Laboratory Manager – Managed every aspect of the laboratory operations from setting goals
to organizing, leading, and monitoring for the production of defensible data. Conducted the hiring,
training and review of laboratory staff. Responsible for implementation and reporting of State
Performance Evaluation Program. Involved with meeting criteria to maintain the Laboratories State
Certification. Performed detailed second party review of analytical data. Used the Laboratory
Information System (LIMS-Promium) extensively to monitor work flow in the laboratory. Maintained
adequate supplies for the smooth functioning of the laboratory.
U
nc
on
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1996-2000 Inorganic Chemist – Principal analyst for the determination of metals by Inductively Coupled
Plasma (ICP), Atomic Absorption (AA), and mercury by cold-vapor AA. Performed the chemical and
physical analysis of drinking water, wastewater, and solid samples performed according to EPA methods
and Standard Methods. Used the LIMS system for sample status and reporting. Maintained laboratory
equipment for peak performance.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 48 of 89
Oilfield Environmental & Compliance, Inc.
Dwain Zsadanyi,
Semi-Volatile Organic Department Manager
(Page 1of 2)
QUALIFICATIONS
lle
d
Mr. Zsadanyi has over 25 years hands-on experience as analyst and department manager running GC/MS
for trace analysis of priority pollutants, hazardous substance list compounds, fuels in soil and water.
Interpretation of mass spectra. Maintenance and cleaning of HP GC/MC’s, autosamplers and purge-andtrap units. Training of new analysts. Method development and data interpretation.
EDUCATION
B.S., Chemistry, California Polytechnic State University, San Luis Obispo, 1982

Teaching Credential in Physical Science, California Polytechnic State University, San Luis
Obispo, 1986

OSHA 40 Hour HazMat Certificate + Refreshers

on
AFFILIATIONS
tro

American Chemical Society
nc
EXPERIENCE
2006–Present
U
Mr. Zsadanyi is responsible for the scheduling, maintenance, and verifying QA/QC parameters are met
for all data from the Semi-Volatile Organic Laboratory. He is primarily responsible for any new method
development, the analysis of proficiency testing (PT) samples, analysis of MDL / RL / DoCs for all
supervised personnel, and training of technicians and analysts within this department.
2005–2006
Creek Environmental Laboratory – San Luis Obispo, CA
Project Manager – Provided technical client services & project coordination. Performed data review,
provided result interpretation, and performed analyses as necessary.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 49 of 89
Oilfield Environmental & Compliance, Inc.
Dwain Zsadanyi,
Semi-Volatile Organic Department Manager
ZymaX envirotechnology, inc. – San Luis Obispo, CA
d
1994–2005
(Page 2of 2)
lle
2001–2005, Project Manager – Responsible for data review, interpretation of analytical results and
providing technical advice to clients. In charge of research and method development.
1994–2001, Semi-Volatile Laboratory Manager – Responsible for operation of Semi-Volatile Organics
GC/MS group. Primary duties included critical review of all data, final report generation, method
development, staffing and scheduling. Additional duties included sample preparation, analysis, data
interpretation, and instrument calibration and maintenance.
Coast to Coast Analytical Services – San Jose and San Luis Obispo, CA
tro
1990 – 1994
Organics GC/MS Chemist – Performed volatile and semi-volatile methods. Sample preparation, analysis,
data reduction and processing. Method development for new procedures/analysis (including low DL SIM
analysis). Maintenance and repair of analytical equipment. Review and approval of reports. Organizing
and scheduling workload and personnel. Purchasing/acquisition of supplies.
California Polytechnic State University – San Luis Obispo, CA
on
1984–1986
Laboratory Instructor – Plan, conduct and evaluate lessons. Record keeping and report writing of student
performance.
Teacher – Various California School Districts
nc
1986–1990
1969–1972
Food Inspector – U.S. Army
U
Analysis and inspection of food for army procurement. Site inspection of vendor facilities. Analysis for
wholesomeness and specification requirements. Random sampling and sample preparation for QC
reporting of consignments.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 50 of 89
Oilfield Environmental & Compliance, Inc.
Drew Miller, Wet Chemistry Department Manager
(Page 1of 1)
QUALIFICATIONS
lle
d
Mr. Miller has several years of experience in the environmental laboratory field including working as a
principal chemist for the inorganics department, performing method development, instrument
troubleshooting, maintenance, and repair, and supervision.
EDUCATION
B.S., Biological Sciences, California Polytechnic State University, San Luis Obispo, 2008
EXPERIENCE
on
2008–Present
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
2012-Present, Inorganics Department Manager – Mr. Miller is responsible for the scheduling,
maintenance, and verifying QA/QC parameters are met for all data from the Wet Chemistry and Metals
laboratories. He is primarily responsible for any new method development, the analysis of proficiency
testing (PT) samples, analysis of MDL / RL / DoCs for all supervised personnel, and training of
technicians and analysts within these laboratories.
U
nc
2008-2011, Inorganics Analyst & Principal Chemist – Mr. Miller scheduled, maintained consumable
inventory, performed instrument maintenance, method development, and assisted with training for all wet
chemistry and metals methodologies. Additionally, he performed as the primary contact for external
auditors of the department.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 51 of 89
Oilfield Environmental & Compliance, Inc.
Parwinder Parmar, Metals Department Manager
(Page 1 of 2)
QUALIFICATIONS
EDUCATION & CERTIFICATION
lle
d
Mr. Parmar has over 10 years hands-on experience as a chemist and supervisor in the metals analysis of
solids and liquids using EPA methodologies. His experience also includes analytical work in the wet
chemistry and wine industry methodologies.
B.Sc., Biology and Chemistry, Punjabi University, Patiala (India), 1996

M.Sc., (Microbial and Food Technology) – Dept. of Biotechnology, Punjabi University, Patiala
(India), 1998

PhD., Dept. of Biotechnology, Punjabi University, Patiala (India), 2003
on
EXPERIENCE
tro

2012–Present
nc
Mr. Parmar is responsible for the scheduling, maintenance, and verifying QA/QC parameters are met for
all data from the Metals Department. He is primarily responsible for any new method development, the
analysis of proficiency testing (PT) samples, analysis of MDL / RL / DoCs for all supervised personnel,
and training of technicians and analysts within this department.
2005-2012
BC Laboratories Inc. Bakersfield, CA
U
Metals Department Supervisor - Mr. Parmar was responsible for the scheduling, maintenance, and
verifying QA/QC parameters are met for all data from the Metals Department. He was primarily
responsible for any new method development, the analysis of proficiency testing (PT) samples, analysis
of MDL / RL / DoCs for all supervised personnel, and training of technicians and analysts within this
department.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 52 of 89
Oilfield Environmental & Compliance, Inc.
Parwinder Pal Parmar, Metals Department Manager
2001-2005
(Page 2 of 2)
Curtis & Tompkins Ltd., Berkley, CA
1998-2000
lle
d
Chemist - Mr. Parmar was responsible for the digestion and analysis of soil and water samples for metals
analysis using ICP/ICP-MS, Hydra AA Mercury analyzer and Flame AA. He also performed wet
chemistry analyses for the Wet Chemistry department as requested.
Master Winery, India
U
nc
on
tro
Chemist - Mr. Parmar was responsible for the chemical analysis, monitoring of fermentation and handling
of the microbial work associated with producing wine. He was also responsible for entering the data
associated with the work into a database.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 53 of 89
Oilfield Environmental & Compliance, Inc.
Pete Alcocer,
Oil Production Client Services &
Operations Consultant
(Page 1of 1)
QUALIFICATIONS
lle
d
Mr. Alcocer has been involved in using bioremediation techniques in the field such as microbial bacteria
remediation, vapor extraction, and excavation. In performing soil, water, gas, and oil sampling in
accordance with EPA and ASTM guidelines, Mr. Alcocer has gained experience and expertise in using
such field analyzers as the vapor probe, OVA-128, PID, LEL, Oxygen sensor, and Draeger type reagent
tubes.
EDUCATION
U.S. Marine Corps, 1975-1978, Field Communications Training

SECORP Industries Safety Class for H2S

Environmental Hazardous Materials Technology Certificate, 1993, Allan Hancock College, Santa
Maria, CA

OSHA HAZWOPER 40-hourTrained (OSHA 29 CFR 1910.120)
on
tro

EXPERIENCE
1984-Present
nc
Mr. Alcocer is involved in the majority of OEC’s field sampling program, providing independent
field analyses of crude and refined gas/oil product for central California oil production companies. Field
tests have included on-site tank testing for Reid vapor pressure, LPG/gasoline, specific gravity, moisture
content, corrosivity, and various air monitoring analyses.
Mr. Alcocer’s laboratory responsibilities include GC analysis of hydrocarbons in gases and
liquids by FID and TCD per ASTM methods and hydrogen sulfide by FPD. He provides comprehensive
crude oil profiles, which include API gravity, kinematic viscosity, total sulfur content, salt content,
flashpoint, and quantitative distillation.
U
1983–1984
RMR Contractors, Santa Maria, CA
Welder/Independent Contractor- Mr. Alcocer worked as a pipeline welder, certified under ASME B31-3.
He performed construction and repair of oil, gas, and steam pipelines.
1980-1982
D & R Contractors
Welder- Mr. Alcocer’s duties included oilfield pipeline construction and pipefitting, including major
structural welding.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 54 of 89
Oilfield Environmental & Compliance, Inc.
Roger Dickinson,
Oil Production
Field Operations Supervisor
(Page 1of 1)
QUALIFICATIONS
lle
d
Mr. Dickinson has over 5 years experience in field operation activities and performing soil, water, gas,
and oil sampling in accordance with EPA and ASTM guidelines.
EXPERIENCE
2008-Present
Santa Maria Joint Union High School District, CA
on
2006-2008
tro
Mr. Dickinson is responsible for administrating the majority of OEC’s field sampling program,
providing independent field analyses of crude and refined gas/oil product for central California oil
production companies. Field tests have included on-site tank testing for Reid vapor pressure,
LPG/gasoline, specific gravity, moisture content, corrosivity, and various air monitoring analyses.
nc
Bus Driver, Bus Attendant (Transportation Assistant), Food Service, Custodian - Mr. Dickinson carried a
Class B Commercial License and completed training for School Bus Drivers, DL45 School Bus
Certification, and CA Highway Patrol First Aid. He was responsible for providing safe transportation of
regular education and special education students, supervising Bus Attendant on special needs routes,
maintaining fuel logs, student count logs, time logs, and mileage logs, daily inspections of district
transportation vehicles, and maintaining orderly conduct of students while riding the bus.
2007
Kinyon Construction, Santa Maria, CA
U
Millwright Worker - Mr. Dickinson worked in a team responsible for fabricating iron pipes, replacing
valves, pumps, and motors. These tasks included welding, performing job site safety inspections and
operating heavy equipment including: Man Lift, Fork Truck, Petti Bone truck. Tenure included
completion of various MSHA training coursework.
2002-2006
Costal Imports, Pismo Beach, CA
Owner- Mr. Dickinson’s duties included the development and management of various business systems,
including merchandising, advertising, human resources, accounting, website, and inventory control.
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 55 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX B: STANDARD OPERATING PROCEDURES (SOP)
Document ID
Title
ADM
Administrative Procedures
ADM-BILLING
ADM-CHANGE
ADM-CLIENT
ADM-ETHICS
ADM-HSP
ADM-PP
ADM-Purch
ADM-SOP
ADM-Training
ADM-Vehicle
Project Billing & Accounting Practices
Change Management
Client Confidentiality, Complaint Handling
Ethics Training & Policies
Health & Safety Plan
Personnel Policy
Material Procurement
Standard Operating Procedures
Orientation & Training Program
OEC Vehicle Procedures
GEN
General Laboratory Procedures
GEN-Audit
GEN-CAPA
GEN-Data
GEN-Defin
GEN-DISPOSAL
GEN-DOC
GEN-EDATA
GEN-EVCM
GEN-EXTR-CALWET
GEN-EXTR-TCLP
GEN-INT
GEN-LOGIN
GEN-POWER
GEN-SECM
Internal Audit Program
Corrective & Preventive Action
Data Reduction, Validation & Reporting
Acronyms & Definitions
Sample & Waste Disposal
Document Control
Electronic Data Generation & Record Retention
Equipment Validation, Calibration & Maintenance
California Waste Extraction Test (CALWET)
TCLP Extraction - EPA 1311
Manual Integration
Sample Login & Dispersal
Power Shutdown & Startup Guide
Small Instrument - Support Equipment Calibration & Monitoring
F
Field Operations Procedures
F-AirMonitor
F-AUGER
F-GasVaporProbe
Air Monitoring & Sampling Procedures
Manual Hand Auger Field Sampling
Gas Vapor Probe Installation & Sampling
U
nc
on
tro
lle
d
rev 03/15/2013
F-GEOPROBE
F-GOR GWR
F-GWMonitor
F-HOST
F-NG
F-NGL
F-SAMPLING
F-SRB
Geoprobe System Instructions
GOR & GWR Sampling Protocol
Groundwater Monitoring Field Sampling
HOST Vapor Pressure Sampling Method
Natural Gas Cylinder Sampling
Natural Gas Liquid Cylinder Sampling
General Sampling Guide
Sulfate Reducing Bacteria Field Sampling
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 56 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX B: STANDARD OPERATING PROCEDURES (SOP)
Document ID
Title
F-SurfaceWater
F-Tedlar
FA-Dew Point Dreager
FA-Dew Point
FA-Freeze Valve
FA-H2S Dreager
FA-H2S HACH
FA-pH
FC-Guadalupe
Surface Water Sampling
Tedlar Bag Gas Sampling
Dew Point testing by Dreager Tube (Gas Detector Tube)
Water Vapor Content of Gaseous Fuels by Measurement of Dew Point Temperature
Freeze Valve Method
Hydrogen Sulfide testing by Dreager Tube (Gas Detector Tube)
Field Analysis of H2S in Water using HACH
Field Analysis of pH
Site-Specific Courier Instructions: Guadalupe
IN-ME
Inorganics - Metals Department Procedures
IN-Hardness
IN-Hg
IN-Hg-DIGEST
IN-ME-PREP-200
IN-ME-PREP-3000
IN-ME-ICP
IN-ME-ICPMS
Calcium & Total Hardness by Calculation
Mercury Analysis by CVAA
Mercury Digestion for CVAA Analysis
Metals Preparation by EPA 200.2
Metals Preparation by EPA 3000 Series Methods
Metals Analysis by ICP
Metals Analysis by ICPMS
IN-WC
Inorganics – Wet Chemistry Department Procedures
d
lle
tro
on
Acid and Base Number by Color-Indicator Titration
Total Alkalinity (SM2320B)
Ammonia as Nitrogen by Ion Selective Electrode (EPA 350.3 & SM4500NH3)
Chlorophyll-a by Spectrophtometry
Chemical Oxygen Demand
Specific Conductance (SM2510B)
Hexavalent Chromium by Colorimetry
Total Cyanide
Ferrous Iron
Igniteability / Flashpoint (EPA 1010)
Anions by Ion Chromatography (EPA 300.0)
Anionic Surfactants as MBAS
Hexane Extractable Oil & Grease
pH Measurement
Total Phenolics
Total Phosphorus
Reactive Cyanide & Sulfide
Total Sulfide
Settleable Solids
Total Dissolved Solids
U
nc
IN-AB#
IN-Alkalinity
IN-Ammonia
IN-Chlorophyll
IN-COD
IN-Conductivity
IN-CrVI
IN-Cyanide
IN-Fe
IN-FP
IN-IC(Anions)
IN-MBAS
IN-O&G
IN-pH
IN-Phenol
IN-P
IN-RXCNS
IN-S
IN-SETT
IN-TDS
rev 03/15/2013
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 57 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX B: STANDARD OPERATING PROCEDURES (SOP)
Document ID
Title
IN-TS
IN-TSS
IN-Turbidity
IN-VS
Total Solids
Total Suspended Solids
Nephelometric Turbidity
Volatile Solids
OG
Oil & Gas Production Analysis Department Procedures
OG-ADA
OG-API
OG-BS&W
OG-BTU (NATGAS)
OG-CORR
OG-DMETER
OG-DISSGAS
OG-DIST
OG-GOR-EXTR
OG-GWR-EXTR
OG-HYDROMETER
OG-H2S
OG-H2SMER
OG-oPO4
OG-P
OG-PSIMPLE
OG-RATIO
OG-RVP
OG-RVPTVP
OG-S(XRF)
OG-SCAQMD
OG-SEDIMENT
OG-SHRINK
OG-TCDA
OG-TRS
OG-V
OG-VISC
Determination of ADA in Water
API GRAVITY OF PETROLEUM (HYDROMETER METHOD)
Determination of Water and Sediment in Crude Oil By Centrifuge Method
NATURAL GAS ANALYSIS BY GAS CHROMATOGRAPHY
Corrosion Inhibitor
Specific Gravity (Relative Density) by Density Meter
Dissolved Compounds in Gas Extracts
Distillation of Petroleum Products
Gas-Oil Ratio Extraction
Gas-Water Ratio Extraction
Specific Gravity by Hydrometer
Hydrogen Sulfide in Gaseous Fuels (Lead Acetate Reaction Rate Method)
H2S AND MERCAPTANS IN OIL AND SLUDGE
ORTHOPHOSPHATE BY COLORIMETRY
TOTAL PHOSPHOROUS BY COLORIMETRY
PEAK SIMPLE CHROMATOGRAPHY SOFTWARE
GAS OIL RATIO
Reid Vapor Pressure
REID VAPOR PRESSURE (RVP) TO TRUE VAPOR PRESSURE (TVP)
Sulfur in Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectroscopy
SCAQMD METHOD 307-91 Determination of Sulfur in a Gaseous Matrix
Determination of Water and Sediment in Crude Oil By Centrifuge
SHRINKAGE FACTOR
TCDA Analysis by GC
TRS from Stationary Sources by GC/SCD
Vanadium
Kinematic Viscosity of Liquids
SV
Semi-Volatile Organics Department Procedures
SV-CLEAN-GPC
SV-CLEAN-SAC
SV-CLEAN-SGC
Gel Permeation Chromatography
Sulfuric Acid Cleanup - EPA 3665A
Silica Gel Cleanup - EPA 3630C
rev 03/15/2013
tro
lle
d
Total Kjeldahl Nitrogen
Total & Dissolved Organic Carbon
U
nc
on
IN-TKN
IN-TOC
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 58 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX B: STANDARD OPERATING PROCEDURES (SOP)
Document ID
Title
SV-CLEAN-SC
SV-EXTR-AQ
SV-EXTR-Fractionation
SV-EXTR-PROD
SV-EXTR-SO
SV-DIOXANE
SV-GLYCOL
SV-Methanol
SV-PCB
SV-PEST
SV-PNASIM
SV-SARA
SV-D2887
SV-SVOC
SV-TPH(FID)
SV-TPH(GCMS)
SV-TPH(LGVOL)
Sulfur Cleanup - EPA 3660B
Extraction of Aqueous - EPA3510C
Fractionation of Extracts
Extraction of Products
Ultrasonic Extraction of Solids - EPA 3550B
1,4-Dioxane by GC/MS
Glycol Analysis by GC/FID
Methanol Analysis by GC/FID
Polychlorinated Biphenyls (PCBs) by GC/(ECD)2
Organichlorine Pesticides by GC/(ECD)2
PNA Analysis by GC/MS in SIM Mode
SARA Fractionation & Analysis
Simulated Distillation by ASTM D2887
Semivolatile Organic Compounds by GC/MS
Semivolatile Petroleum Hydrocarbons by GC/FID
Semivolatile Petroleum Hydrocarbons by GC/MS
Semi-Volatile TPH Determination by Large Volume Injection & GC/FID
VO
Volatile Organics Department Procedures
VO-524.2
VO-624
VO-GRO(FID)
VO-PID
VO-TPH&VOC
VO-VOC
VO-AIR
Volatile Organic Analysis of Drinking Water
Volatile Organic Analysis by EPA 624
GRO-TPH Determination by GC/FID (LUFT & EPA 8015B)
Aromatic Volatile Organics by GC/PID
TPH & Related VOC Determination by GC/MS
Volatile Organic Analysis (EPA 624 & 8260B)
Volatile Organic Compounds in Air
U
nc
on
tro
lle
d
rev 03/15/2013
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
Page 59 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX C – OEC EQUIPMENT LIST
Semi-Vols Rm.
Auto Sampler – Carousel
Auto Sampler – Carousel
Auto Sampler – CTC Liquid
Auto Sampler – IC/MS
Auto Sampler - ICAP
Auto Sampler – Injector
Auto Sampler – Injector (GC1)
Auto Sampler – Injector (GC8)
Auto Sampler – Injector (GCMS1)
Auto Sampler – Injector (GCMS6)
Auto Sampler - Teledyne Tekmar
AUTOCAN
Auto Sampler (CobraII)
Auto Sampler (CobraII) (GC3)
Auto Sampler (CobraII) (GC5)
Auto Sampler (CobraII)
Auto Sampler (CobraII) (GCMS2)
Auto Sampler Archon (51 pos)
Auto Sampler Archon (51 Pos)
(GC4)
Auto Sampler Archon (51 Pos)
(GC7)
Auto Sampler Archon (51 Pos)
(MS11)
Auto Sampler Archon (81 Pos)
(MS5)
Auto Sampler Archon (81 Pos)
(MS9)
Auto Sampler Archon (81 Pos)
(MS13)
Semi-Vols Rm.
Semi-Vols Rm.
Roemer Storage
METALS Rm.
METALS Rm.
Preisker Storage
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
SERIAL #
Ingersoll Rand
1203564
Premium Plus
A.O.Smith 'Century'
NuTech
Perkin-Elmer AS90
HP 7673B
HP 7673B
HP 7673B
HP 7673B
HP 7673B
Agilent 6850
(G2880A)
G2614A
G2614A
COMBI/PAL
CETAC ASX-520
CETAC ASX-520
G2913A
HP7673B
HP 7673B
HP 7673B
HP 7673B
B28410964
BY07-16
09004
206
207
84
136
3138A27453
3205A28236
3331A32853
3328A32563
3506A37974
CN30520433
CN44631260
CN84651351
123099
020605A520
050957A520
CN44822036
2950A20230
3240A32527
3429A39421
3009A21046
on
VOLS Room
144ACAN-000
DS06103002
365
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
Cobra II
Cobra II
Cobra II
Cobra II
Cobra II
Varian
1147-0905
COB167102508
1130-0605
COB167102509
COB180070510
13485
347
VOLS Room
Varian
14056
VOLS Room
OI Analytical
14117
VOLS Room
Varian
15123
3
VOLS Room
EST Model 8100
14032
18
VOLS Room
EST Model 8100
14103
350
VOLS Room
EST Model 8100
13985
nc
U
HADY #
d
Auto Sampler – (GCMS10)
Air Compressor
Model #
lle
Air Compressor (Coleman)
Air Compressor (Coleman) motor
Atmospheric pressure regulator
Auto Sampler
Auto Sampler – Controller (GC1)
Auto Sampler – Controller (GC8)
Auto Sampler – Controller (GCMS6)
Auto Sampler – Tray (GC8)
Auto Sampler – Tray (GCMS6)
ROOM
Outside cagePreisker-VOLS
CLOSET'
CLOSET'
GAS Room
Preisker Storage
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
tro
PROPERTY DESCRIPTION
Revised 11/21/12 - LR
Auto Sampler for TOC
Prep Room
Auto Sampler Tray (GC1)
Auto Sampler Tray (GCMS1)
Bomb Ignition Unit, Para
Semi-Vols Rm.
Semi-Vols Rm.
GAS Room
Shimadzu (ASI5000A)
HP 7673B
HP 7673B
346
36902235
3342A33539
2942A20870
2901 EB Lot 0793
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307 Roemer Way | Santa Maria | CA 93454
173
169
276
Quality Assurance Manual
Rev 17 – June 2013
Page 60 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX C – OEC EQUIPMENT LIST
Revised 11/21/12 - LR
PROPERTY DESCRIPTION
ROOM
Model #
Bomb, Cylinder, (Oxy calorimeter)
GAS Room
Para
Bomb, Oxygen, calorimeter
Branson cage, sonicator
Brother Printer
Canister Cleaner Entec Model 3100A
Centrifuge
Centrifuge, Floor model
Centrifuge, Table Model
Chiller, Neslab 208/230V 9.7 AMP
(not in service)
Chiller, Neslab 208/230V 9.7AMP
(not in service)
Chiller, Thermo Fisher 115V, 11.1
AMP (ICP)
Chiller, Thermo Scientific 208/230V,
10.1 AMP (ICPMS)
Chromatography Data System
Chromatography Data System
Chromatography Data System
Condensor/vaporizer (#1) - Hood 13
Condensor/vaporizer (#2) - Hood 11
Condensor/vaporizer (#3) - Hood14
Condensor/vaporizer (#4) - Hood 12
Conductivity meter
Controller
Controller
Controller, Interface SCD
Copier
GAS Room
Roemer-Storage
SAMPLE Rec.
VOLS Room
GAS Room
Prep Room
Prep Room
Para
Branson Max Booster
Roemer-Storage
Neslab CFT-75
199218069
Roemer-Storage
Neslab CFT-75
694279212
Roemer-Storage
Neslab Thermo Flex
900
R100050038
Roemer-Storage
Neslab Merlin 1175
10515 2009
Peak Simple 202, 4ch
Peak Simple 202, 4ch
Peak Simple 202, 4ch
Caliper TurboVap II
Caliper TurboVap II
Caliper TurboVap II
Caliper TurboVap II
Myron L
HP ProCurve
Perk-El AS90/AS91
Sievers 355
N1148W
N1341W
N4397
TV0553N12804
not available-in use
not available-in use
TV0842N14837
172519
J3300A
not available-in use
01220
75
81
Cylinder Dolly
Density meter, AP PAAR
Density meter, keypad
Dessicator, glass (round)
Dessicator, plastic cabinet, (Square)
Dessicator, plastic cabinet, (Square)
Detector, wavelength analyses
Digi Block A
GAS Room
GAS Room
GAS Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Preisker Storage
Preisker Storage
GAS Room
SAMPLE Rec.
Outside CageRoemer
VOLS Room
GAS Room
GAS Room
Prep Room
Prep Room
Prep Room
Metals Prep
Metals Prep
190091
107136559520
none
none
219
220
61
66
3SGE170004
62
Digi Block A Controller
Metals Prep
Digi Block B
Metals Prep
Digi Block B Controller
Metals Prep
Dismembrator, sonic (HOOD #10)
Dismembrator, sonic (HOOD #12)
Dismembrator, sonic (HOOD #13)
Distillation - Ammonia
Prep Room
Prep Room
Prep Room
Prep Room
DMA 48
DMA 48
none
Fisher Scientific
Sanko
Thermo Spectronic
Vendor CPI
George T. Hall Co.
Inc.
Vendor CPI
George T. Hall Co.
Inc.
Fisher Sci 500
Fisher Sci 500
Fisher Sci 500
Easy Distillation
HADY #
279
d
277
165
01325
03240E
7L003
428-22363
229
tro
lle
Beckman 356529
IEC
on
U
nc
Cylinder Dolly
Entec Model 3100A
SERIAL #
101A19940C20092
988
L341EB
not available-in use
184
100
363
287
33
134
85
S1125602.15
S1125602.7
BCK09035896A
BBW04112875
BCK08054855A
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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163
164
Quality Assurance Manual
Rev 17 – June 2013
Page 61 of 89
Oilfield Environmental & Compliance, Inc.
Freezer, Kenmore
Freezer, Kenmore (Stds)
Fridge
Fridge #2
SAMPLE Rec.
VOLS Room
Preisker Storage
Preisker VOL
Storage
VOLS Room
Preisker Storage
GAS Room
SAMPLE Rec.
Semi-Vols Rm.
Semi-Vols Rm.
Semi-Vols Rm.
GAS Room
GAS Room
GAS Room
GAS Room
GAS Room
253.165021
253.267321
VWR Scientific-Revco
none
WB22349282
217
WB24445575
VWR R429GA14
N31S-617753-05
354
Beverage-Air'
SL-1020
none
8045920
102017
none
185
355
222
VWR Scientific-Revco
Danby 'Designer'
Emerson OR300A
HP 5890
HP 5890
HP 5890
HP 5890
Agilent 5890 Series II
Agilent 6850N
(G2630A)
Agilent 6850
(G2630A)
Agilent 6890 Plus+
HP 5890 GC Series II
Agilent 6890N
(G1530N)
HP 5890 Series II
Agilent 6890N
Agilent 6890N
Agilent 6850N
(G2630A)
Agilent 7890A
(G3440A)
not available-in use
1196070021003920
63426502
none
none
2443A04188
2750A19263
2843A19402
167
168
334
232
233
234
237
GAS Room
Agilent 5890 Series II
3336A56889
Semi-Vols Rm.
GAS Room
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
Semi-Vols Rm.
Semi-Vols Rm.
HP 5890
Agilent 5890 Series II
HP 5890 Series II
HP 5890 Series II
HP 5890 Series II
HP 5890 Series II
HP 5890 Series II
3223A43525
Gas Chromatograph (GC) (MS10)
Semi-Vols Rm.
Gas Chromatograph (GC) (MS13)
Gas Chromatograph (GC) (MS2)
VOLS Room
Semi-Vols Rm.
nc
VOLS Room
Gas Chromatograph (GC) (MS5)
VOLS Room
Gas Chromatograph (GC) (MS6)
Gas Chromatograph (GC) (MS7)
Gas Chromatograph (GC) (MS8)
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
Gas Chromatograph (GC) (MS9)
VOLS Room
Gas Chromatograph (GC) (not in use)
GAS Room
U
HADY #
364
353
187
Gas Chromatograph (GC) (MS11)
Gas Chromatograph (GC) (not in
use)?
Gas Chromatograph (GC)(MS1)
Gas Chromatograph (GC)(SCD2)
Gas Chromatograph (GC1)
Gas Chromatograph (GC3)
Gas Chromatograph (GC4)
Gas Chromatograph (GC5)
Gas Chromatograph (GC6)
SERIAL #
WB70426086
WB0326162
not available-in use
on
Fridge #3 (Aqueous samples)
Fridge #4, ( OLD Walk In)
Fridge #7, products (O&G)
Fridge #8 (Large Walk-in)
Fridge, #5 (8081/8062 Stds.)
Fridge, #6 (8015/8270 Stds.)
Fridge, Emerson (small)(Stds)
Gas Chromatograph (GAS1)(TCD1)
Gas Chromatograph (GAS2)(TCD2)
Gas Chromatograph (GAS3)(SCD1)
Gas Chromatograph (GAS4)(FID1)
Gas Chromatograph (GAS5)(SCD2)
VOLS Room
Model #
Easy Distillation
Easy Distillation
Easy Distillation
GCA/Precision Sci
Kenmore 253.280…
Frigidaire Model #
FKFH21F7HWD
lle
Freezer (soil samples) (frost free)
ROOM
Prep Room
Prep Room
Prep Room
GAS Room
VOLS Room
tro
PROPERTY DESCRIPTION
Distillation - Cyanide
Distillation - Phenol
Distillation – TKN
Flash Point machine
Freezer (soil samples)
Revised 11/21/12 - LR
d
APPENDIX C – OEC EQUIPMENT LIST
US10309009
US00002632
US00022331
3118A35482
10
US10145036
348
3235A46821
CN10445037
US10250006
CN10820018
CN10847057
3223A42509
2623A08375
2950A26689
3133A37065
3019A28656
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Oilfield Environmental & Compliance, Inc.
GAS Room
GAS Room
GAS Room
GAS Room
GAS Room
GAS Room
GAS Room
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
Semi-Vols Rm.
Prep Room
Semi-Vols Rm.
Dell Inc. OptiPlex 390
Dell Inc. OptiPlex 390
Dell Inc. OptiPlex 390
Dell Inc. OptiPlex 390
Gel Permeation Cleanup Instr.
VOLS Room
Semi-Vols Rm.
VOLS Room
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
VOLS Room
Prep Rm. Hood
#6
CLOSET'
CLOSET'
Semi-Vols Rm.
GAS Room
GAS Room
Supervisors Room
METALS Rm.
U
Hood air monitor (ALNOR)
(Hood#11)
Hood air monitor (ALNOR) Hood #4
Hood air monitor (ALNOR) Hood #2
Hood air monitor (ALNOR) Hood #5
Hood air monitor (ALNOR) Hood #3
HADY #
US00024443
7H2ZTR1
3VCF7V1
7H2YTR1
7H2XTR1
Dell Inc. OptiPlex 390
Dell Inc. Vostro 230
Dell Inc. Vostro 230
Dell Inc. Vostro 230
Dell Inc. Vostro 230
Dell Inc. OptiPlex 380
Dell Inc. Vostro 230
Dell Inc. Vostro 230
Dell Inc. OptiPlex 330
Compaq Evo D510
SFF
4KXJ7V1
FJK3NN1
FJM2NN1
FJL1NN1
FJK2NN1
HVX4PL1
FJL3NN1
FJM1NN1
6L0PCG1
6X32KN9XA030
Dell Inc. Vostro 230
FJM3NN1
Dell Inc. Vostro 230
Dell Inc. OptiPlex 330
Dell Inc. OptiPlex 330
Dell Inc. OptiPlex 330
J2 Scientific
AccuPrep MPS
Nitrox 'UHP-352A'
PMR1-010972
part of above ??
Thermolyne 45500
Type F4391
Model (969-4650)
Dell Inc. OptiPlex
GX520
FJN1NN1
99D30G1
3YMGCG1
C9D30G1
037A0089
99232-17
not available-in use
4550020104955
77066
205556
1V4RHB1
211
212
166
82
223
Prep Room
AirGard 200
TSS 81360
99
Metals Prep
SAMPLE Rec.
Semi-Vols Rm
Metals Prep
AirGard 200
AirGard 200
AirGard 200
AirGard 200
Fisher Science
'Contempra Fume'
Genie Scientific
Genie Scientific
TSS 81361
TSS 81352
TS 81351
TSS 81362
224
195
102
59
none
324
none
none
194
nc
Generator, zero air (in Samp closet)
Generator, zero air GAUGE (in closet)
Glass case, sonicator (hood #3)
Heater box
Heating Chauffage (Heizung)
Helium Detector Portable
HG2 Computer
SERIAL #
2938A24839
3235A44680
lle
Semi-Vols Rm.
Model #
HP 5890 Series II
HP 5890 Series II
Agilent 6890
(G1530A)
on
GCMS11 Computer
GCMS2 Computer
GCMS5 Computer
GCMS6 Computer
GCMS7 Computer
GCMS8 Computer
GCMS9 Computer
ROOM
VOLS Room
Semi-Vols Rm.
tro
PROPERTY DESCRIPTION
Gas Chromatograph (GC7)
Gas Chromatograph (GC8)
Gas Chromatograph (GC9) – Large
Volume Injection
GAS1 Computer
GAS10 Computer
GAS11 Computer
GAS4 Computer
GAS5 Computer
GAS8 Computer
GAS9 Computer
GC1 Computer
GC3 Computer
GC4 Computer
GC5 Computer
GC6 Computer
GC7 Computer
GC8 Computer
GC9 Computer
GCMS10 Computer
Revised 11/21/12 - LR
d
APPENDIX C – OEC EQUIPMENT LIST
Hood, #17
VOLS Room
Hood, #2
Hood, #5
SAMPLE Rec.
Semi-Vols Rm.
PLH-1097-1.0
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307 Roemer Way | Santa Maria | CA 93454
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Rev 17 – June 2013
Page 63 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX C – OEC EQUIPMENT LIST
SERIAL #
none
None
None
None
None
None
81360
PP22E-3
OP22A-9
PA-3-8
FH-414C-A
FH-414D-A
none
none
1819001003198
1819001006114
1788001006141
1788001007106
1830002003158
1830002006117
1833001002200
1833001008123
1818011003129
1818011005207
1820022003126
1820023005180
HQLS4H1
System Serial
Number
20095011
0939907
960QVK1
89D30G1
4465
Granville 6392
HADY #
HP 59822B
Agilent 59864B
HP 59864A
7520
US60111438
1466
4
VOLS Room
Agilent 59864B
US6018823
Preisker
Computer Room
Promium, Element
ver.6.07:2016
Hewlett-Packard
Compaq dc7800 Small
Form Factor
Dell Inc. OptiPlex 360
Dell Inc. OptiPlex 330
METALS Rm.
METALS Rm.
METALS Rm.
METALS Rm.
Roemer Storage
Preisker Storage
Preisker Storage
Semi-Vols Rm.
VOLS Room
VOLS Room
U
nc
ICAP 6300 DUO
ICP MS (Elan 6100)
ICP2 Computer
ICPMS Computer
Ionization Gauge Controller
Ionization Gauge Controller
Ionization Gauge Controller
Ionization Gauge Controller
Ionization Gauge Controller (MS11)
Ionization Gauge Controller (MS5)
Ionization Gauge Controller (Not
Used)
Lab Info Management System (LIMS)
upgraded to 25 users
LAB02 Computer
LAB03 Computer
lab05 Computer
d
360
361
362
5
lle
Model #
none
Genie 8' Double Sash
Genie 5' Single Sash
Genie 5' Single Sash
Labconco
Genie
Genie
SafeAire
SafeAire
St. Charles
Hamilton/ SafeAire
Hamilton/ SafeAire
Genie
Genie
Metrohm 819
Metrohm 819
Metrohm 788
Metrohm 788
Metrohm 830
Metrohm 830
Metrohm 833
Metrohm 833
Metrohm 818
Metrohm 818
Metrohm 820
Metrohm 820
Dell Inc. OptiPlex 330
System manufacturer/
Product Name
Thermo Scientific
PE Sciex Elan 6100
Dell Inc. OptiPlex 960
Dell Inc. OptiPlex 330
HP 59822B
59822B
tro
ROOM
Prep Room
Prep Room
Prep Room
Prep Room
Semi-Vols Rm.
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
GAS Room
GAS Room
Metals Prep
Metals Prep
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
Prep Room
on
PROPERTY DESCRIPTION
Hood, #7
Hood, #6
Hood, #8
Hood, #10
Hood,#1
Hood,#9
Hood,#11
Hood,#12
Hood,#13
Hood,#14
Hood,#15
Hood,#16
Hood,#3
Hood,#4
IC Detector 1
IC Detector 2
IC Filtration Sample Processor 1
IC Filtration Sample Processor 2
IC Interface unit 1
IC Interface unit 2
IC Liquid Handling Unit 1
IC Liquid Handling Unit 2
IC Pump 1
IC Pump 2
IC Separation Center 1
IC Separation Center 2
IC1 Computer
IC2 Computer
Revised 11/21/12 - LR
2UA8150D55
H5NQXH1
B9D30G1
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318
316
317
313
315
110
48
150
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Page 64 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX C – OEC EQUIPMENT LIST
Mass Selective Detector (MS10)
SERIAL #
8XLF4F1
FF56CP1
FJL2NN1
HVX3PL1
79D30G1
2YMGCG1
91-1152
C131530155
11488-1-952
1225
1145
not available-in use
3022A01202
3435A01885
2919A00438
VOLS Room
VOLS Room
Semi-Vols Rm.
VOLS Room
Semi-Vols Rm.
Semi-Vols Rm.
VOLS Room
METALS Rm.
METALS Rm.
METALS Rm.
Dell Inc. Vostro 230
Dell Inc. OptiPlex 380
Dell Inc. OptiPlex 330
Dell Inc. OptiPlex 330
Model 4430
Model 4430
Model 4430
LTM A58/A68PS
LTM A58/A68PS
GFC 17
HP 5971A
5972
5971
Agilent 5973
(G2577A)
Agilent 5973N
Agilent 5973 Netcore
5971
Agilent 5973N
5971
Agilent 5973N
Agilent 5975C
CETAC (M-6100)
CETAC (ASX-400)
CETAC
Metals Prep
SCP 'DigiPrep MS'
2110040031
Metals Prep
SCP 'DigiPrep MS'
MSX0307400469
Metals Prep
Metals Prep
Roemer Supervisor Office
Roemer Supervisor Office
GAS Room
VOLS Room
GAS Room
Prep Room
Roemer Supervisor Office
Roemer Computer Closet
Roemer - Project
Managers
'DigiPrep MS keypad
'DigiPrep MS keypad
630404160
KP30050506
216
MACH
1017
345
Agilent – LTM
Module
Para
A50MEB
278
Thermo FB1415M
Vulcan A1750
Dell Inc. OptiPlex 360
1257090730460
DCL0613104
16NQXH1
Dell Inc. OptiPlex 380
8BWNZQ1
Semi-Vols Rm.
SAMPLE Rec.
Preisker Storage
VOLS Room
VOLS Room
Semi-Vols Rm.
Semi-Vols Rm.
CLOSET'
Preisker Storage
Roemer Storage
Semi-Vols Rm.
Semi-Vols Rm.
nc
U
OEC10 Computer
OEC11 Computer
45
46
44
lle
Prep Room
VOLS Room
HADY #
d
Model #
Dell Inc. OptiPlex 330
Dell Inc. Vostro 230
on
Mass Selective Detector (MS11)
Mass Selective Detector (MS13)
Mass Selective Detector (MS2)
Mass Selective Detector (MS5)
Mass Selective Detector (MS6)
Mass Selective Detector (MS7)
Mass Selective Detector (MS9)
Mercury Analyzer (Quick Trace)
Mercury Autosampler
Mercury Peristaltic Pump
Metals reduction, acid/heat (in hood
#3)
Metals reduction, acid/heat (in hood
#3)
Metals reductor keypad (in hood #3)
Metals reductor keypad (in hood #3)
Modular Accelaerated Column Heater
(MACH) 6890
Modular Accelaerated Column Heater
(MACH) 6890 – Dual Setup
Motor (attached to Oxy calorimeter)
MS13 Computer
Muffle Furnace
Muffle Furnace
OEC1 Computer
ROOM
tro
PROPERTY DESCRIPTION
LAB06 Computer
LAB10 Computer
LAB11 Computer
LAB12 Computer
LAB14 Computer
LAB2 Computer
LAB7 Computer
Lamp Power Supply
Lamp Power Supply (GC4)
Lamp Power Supply (GC7)
MACH
MACH
Mass flow controller (sample closet)
Mass Selective Detector
Mass Selective Detector
Mass Selective Detector (MS1)
Revised 11/21/12 - LR
214
151
US30945080
US21884505
US03340488
3118A02486
US10441770
3114A02129
US44647056
US81819247
090602QT6
090603ASX-4
100608-DMP
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Oilfield Environmental & Compliance, Inc.
APPENDIX C – OEC EQUIPMENT LIST
OEC23 Computer
OEC26 Computer
OEC28 Computer
OEC29 Computer
OEC30 Computer
Dell Inc. OptiPlex 390
Dell Inc. OptiPlex 380
4KXJ7V1
5525ZQ1
Dell Inc. OptiPlex 380
Dell Inc. OptiPlex 380
OEC-R1 Computer
OECR-DMZ Computer
Roemer - Project
Managers
Semi-Vols Rm.
Presiker - Office
Presiker - Office
Presiker - Office
VOLS Room
Presiker – Server
Computer Room
Roemer – Server
Computer Closet
Roemer – Server
Computer Closet
Presiker – Server
Computer Room
nc
OECSVR3 Computer
Oil Bath, MGW 'Lauda'
Oven
Oven #1 (Fisher Sci)
Oven for Entec 3100A
Oven, drying
Oven, drying
Taft - Server
Computer Room
GAS Room
Prep Room
Prep Room
VOLS Room
Preisker Storage
Preisker Storage
Oven, drying
PREP Room
Oven, Drying
VOLS Room
Oven, heating (in hood #16)
Oven, heating, 'Turkey' (in hood #16)
Oxygen analyzer, portable
GAS Room
GAS Room
GAS Room
U
oec-t1 Computer
HADY #
5524ZQ1
8BWPZQ1
Dell Inc. OptiPlex 390
JGQZKS1
Dell Inc. OptiPlex 780
D09X4P1
Dell Inc. OptiPlex 390
3VCG7V1
Dell Inc. OptiPlex
3010
Dell Inc. OptiPlex 380
2YT8YV1
Dell Inc. OptiPlex 360
Dell Inc. OptiPlex 360
J5NQXH1
9VQRML1
Dell Inc. OptiPlex 780
Dell Inc. Vostro 230
Rackable Systems Inc.
#S5000PSL
Dell Inc. PowerEdge
T300
Dell Inc. PowerEdge
1900
Dell Computer
Corporation
PowerEdge 840
Dell Inc. PowerEdge
T110 II
T-1
Blue M'
'Isotemp' 650G
Thermo Sci 3513ET
VWR1320
Thelco (in hood)
Thermo Scientific
Precision
Quincy Lab Model:
40GC
Neycraft
General Electric
Teledyne 320A-B
F09X4P1
FF53CP1
A0072ABB
on
OEC5 Computer
OEC6 Computer
OEC7 Computer
OEC8 Computer
OEC9 Computer
OEC-P1 Computer
Roemer Supervisor Office
Roemer Supervisor Office
Roemer - Project
Managers
Roemer - Project
Managers
Presiker - Office
SERIAL #
G5NQXH1
9WHQML1
FDY2CP1
d
OEC21 Computer
OEC22 Computer
Roemer –Front
Office
VOLS Room
Presiker - Open
Office
Model #
Dell Inc. OptiPlex 360
Dell Inc. OptiPlex 360
Dell Inc. Vostro 230
lle
OEC19 Computer
OEC20 Computer
ROOM
Presiker - Office
tro
PROPERTY DESCRIPTION
OEC13 Computer
OEC14 Computer
OEC18 Computer
Revised 11/21/12 - LR
HVX3PL1
GV0XJK1
B1MDGD1
GP4MJH1
8C1FLS1
A14045
12A-1631
103N0065
1482080191829
1100690
11AG-3
231
60
335
27
604171
G4-005254
not available-in use
168962
90200
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226
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Oilfield Environmental & Compliance, Inc.
Power Supply
Power Supply, electrothermal
Power supply,UPS
Pressure Filter
Pressure Filter
Pressure Filter
Pressure Filter (in Sample Closet)
Pressure Filter (in Sample Closet)
Pressure regulating gauge, Autocan
PowerConnect 2324
Tekmar
MC242X1
R-OEC4 Computer
Rotators – Vol #3
Rotators – Vol #4
Rotators –#1
Rotators –#2
Rotators –#5
Rotators –#6
Safety Shower/eye wash station
Safety Shower/eye wash station
HADY #
53
280
288
259
49
230
5278201J91Y0HY
251
none
none
none
YT30-142-HW
none
197
198
199
208
209
Preisker Storage
none
none
none
Millipore 142mm dia
Millipore
Teledyne/Tekmar
14-3938-000
PT2
VOLS Room
(EST) Encon
VOLS
VOLS
VOLS
VOLS
VOLS
VOLS
(EST) Encon
(EST) Encon
(EST) Encon
(EST) Encon
(EST) Encon
(EST) Encon
165092601 E&P
31701403E & P
334011404E & P
286072103 E&P
313011404E and P
31601403E & P
VOLS Room
Velocity XPT
US04260003
VOLS Room
Velocity XPT
US03248004
Prep Room
VOLS Room
GAS Room
GAS Room
KC-laptop
SCRAP LAPTOP
RD- laptop
Cordley
Black & Decker
Resistotherm
Koehler #K11450
not available-in use
Dell Inc. Latitude
E5520
BR8RKQ1
Environmental Express
Environmental Express
Environmental Express
Environmental Express
unknown
unknown
SPEAKMAN
HAWS
None
None
None
None
VOLS Room
Room
Room
Room
Room
Room
Room
nc
U
R-OEC3 Computer
SERIAL #
610M6007
5706
4406
D04628
CNOP4194282984
C70155
91129018
10586765
Compaq Pro UPS500
on
Purge Router/Controller
Purge unit, coupled ports (out of
service)
Purge unit, coupled ports (MS11)
Purge unit, coupled ports (MS13)
Purge unit, coupled ports (MS5)
Purge unit, coupled ports (MS9)
Purge unit, coupled ports (out of svc)
Purge unit, coupled ports (out of svc)
Purge Unit, Tekmar/DOHRMANN
(GC4)
Purge Unit, Tekmar/DOHRMANN
(GC7)
Refrigerated Recirculator
Refrigerator, small (stds)
Regulator, temperature
Reid Vapor Pressure Bath
R-OEC1 Computer
R-OEC2 Computer
Model #
Gelson Mini Plus3
Fisher 'Acumet 910'
'SR601C' sympHony
‘SB90M5 sympHony’
lle
Power Connector, Dell
ROOM
METALS Rm.
Preisker Storage
Prep Room
Prep Room
Roemer Computer Closet
VOLS Room
GAS Room
Roemer Computer Closet
CLOSET'
CLOSET'
CLOSET'
CLOSET'
CLOSET'
tro
PROPERTY DESCRIPTION
Peristaltic Pump (ELAN 6100)
pH Meter
pH Meter, VWR
pH Meter, VWR
Revised 11/21/12 - LR
d
APPENDIX C – OEC EQUIPMENT LIST
JH - laptop
VOLS Room
VOLS Room
Old Rec. Rm.
Old Rec. Rm.
Preisker Storage
Preisker Storage
GAS Room
Metals Prep
PT2-063006001
not available-in use
R82640314-N
None
None
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16/17
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Oilfield Environmental & Compliance, Inc.
Scale – Balance, Top-Loading
Weigh Room
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale-Balance, Top loading (#14)
Weigh Room
Weigh Room
Weigh Room
Weigh Room
Weigh Room
VOLS Room
Sep. Funnel Shaker, Floor model
Prep Room
VOLS Room.
Prep Room
Prep Room
Metals Prep
57
28
7123260283
2741
8028041093
B224021292
B224021299
B211775945
B224021293
473480
not available-in use
3SGL297001
3SGE170004
162
289
289
32
GAS Room
105NO822
4093
311
282
GAS Room
Sievers 350B
none
86
GAS Room
Sievers SCD 350B
0393-378
VOLS Room
Prep Room
Prep Room
nc
GAS Room
GAS Room
Three wheel bike w/basket, Blue
Three wheel bike w/basket, Red
VOLS Room
VOLS Room
TOC Auto Sampler
Prep Room
U
HADY #
350401113803
033307993520
Syringe Pump
T-OEC1 Computer
Taft - Main Area
Torr Meter
VOLS Room
Total Organic Carbon (TOC)
Analyzer
Turbidimeter, HF Scientific
Turbidimeter, LciMOTTE
Typewriter
Universal Gas Flowmeter
Vacuum Pump
SERIAL #
7126211934
12843372
8329230036
089562
7123260661
7123260277
12843372
Corning 'PC-410'
Corning “PC-400D”
9 position
9 position
'Thermix 120S'
ASOMA 200
on
Sonicator, cleaning (in hood #17)
Spectrophotometer – SPEC 20
Spectrophotometer – SPEC 20
Stir Plate
Stirrer
Stirrer (in hood, Vols. #17)
Stirrer Hotplate, Cole-Parmer
Stirrer Hotplate, Cole-Parmer
Stirrer, Fisher Sci
Sulfur Analyzer, X-RAY Fluor.
Sulfur Detector, Chemiluminescen
(SCD1)
Sulfur Detector, Chemiluminescen
(SCD2)
Sulfur Detector, Chemiluminescen
(SCD3) (not in use)
Model #
OHAUS – Scout Pro
Mettler HF-400
Ohaus PA214
OHAUS – CS-200
OHAUS – Scout Pro
OHAUS – Scout Pro
A&D – HF-400
OHAUS – Scout Pro
(SP) 202
OHAUS – AS200
OHAUS – AV313
OHAUS – SP202
OHAUS – SP202
OHAUS – SP601
Ohaus SP202
Glas-Col 099A
VS5504
Fisher FS 30
4001/4
4001/4
lle
ROOM
Preisker Storage
Metals Prep
Prep Room
Prep Room
VOLS Room
VOLS Room
Weigh Room
tro
PROPERTY DESCRIPTION
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Scale – Balance, Top-Loading
Revised 11/21/12 - LR
d
APPENDIX C – OEC EQUIPMENT LIST
Prep Room
Prep Room
Prep Room
OFFICE
VOLS Room
Preisker Storage
Agilent Model
G6644A
KDS Scientific
#LEGATO 200
Shimadzu (ASI5000A)
Dell Inc. OptiPlex 390
Cole Parmer Model#
68801-03
Shimadzu (TOC5000A)
'Micro 100'
LciMOTTE '2020'
IBM 'Wheelwriter 5'
Agilent ADM1000
Edwards E2M2
US10849005
700605
36902235
JBC5LS1
120911002
36N01407A
406180
1156-1699
3 sets on bottom
US12C53096
84248
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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341
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Page 68 of 89
Oilfield Environmental & Compliance, Inc.
VGL Dolly
VOLS Room
VACUBRAND MZ2
Outside CageRoemer
VOLS Room
GAS Room
GAS Room
Prep Room
GAS Room
VOLS Room
VOLS Room
VOLS Room
VOLS Room
VOLS Room
VOLS Room
VOLS Room
Saf-T-Cart
Cat # 76000
Precision 183
HATR-T2
Spectro Phoenix II
Parker HPZA-30000
Millipore #1
Millipore #4
Millipore #5
Millipore #C
Millipore #13
Millipore #14
SERIAL #
39811
61462
96-2054565
none
63999
27475964
none
1218
1008622631
0308608627
972146650
016981995
996165850
046280950
982180770
016934709
156
30770001
14AN/2
9512-360
012702
15151
221
83
none
none
none
none
none
none
328
329
330
331
332
333
U
nc
HADY #
23
24
25
64
327
87
88
239
lle
Model #
Edwards, 2 Stage
Edwards, High Vac.
Edwards, High Vac.
GAST DDA-P184-AA
Edwards 2 Stage
Edwards RV3
GAST DDA-P184-AA
General Electric
DOA-P704-AA
DOA-P704-AA
Edwards
Edwards RV3
Edwards RV3
Edwards RV3
Edwards RV3
Edwards RV3
Edwards
GAST DDA-P704-AA
on
VGL Dolly
Water Bath, GCA
Water Bath, Stainless Steel
WILKS Infra Cal TOG/TPH Analyzer
X-Ray Diffractometer
Zero Air Generator
Zero Headspace Extractor
Zero Headspace Extractor
Zero Headspace Extractor
Zero Headspace Extractor
Zero Headspace Extractor
Zero Headspace Extractor
ROOM
Preisker Storage
Preisker Storage
Preisker Storage
Preisker Storage
Preisker Storage
GAS Room
GAS Room
GAS Room
Prep Room
Prep Room
Preisker Storage
VOLS Room
VOLS Room
VOLS Room
VOLS Room
VOLS Room
GAS Room
VOLS Room
tro
PROPERTY DESCRIPTION
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump
Vacuum Pump (MS11)
Vacuum Pump (MS13)
Vacuum Pump (MS5)
Vacuum Pump (MS8)
Vacuum Pump (MS9)
Vacuum Pump (not in use)
Vacuum Pump, Autocan
Vacuum Pump, Rough for Entec
3100A
Revised 11/21/12 - LR
d
APPENDIX C – OEC EQUIPMENT LIST
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Quality Assurance Manual
Rev 17 – June 2013
Page 69 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX D – SAMPLE TREATMENT:
8015 mod./LUFT by
GC or LUFT by GC/MS
GC (8015,8021)
GC/MS (8260)
Volatile Organic Compounds
TPH diesel, diluent, crude,
motor oil, (TEPH), C10-C40
PNA, BNA, PNA-SIM or
Pesticides/PCBs
TCLP Volatiles
TCLP Semivolatiles
Oil & Grease
(HEM) or (SGT-HEM)
Inorganic Analyte Analysis
Mercury
STLC or DI WET or
TCLP extraction
Anions by IC
Preserve
aq
soil
aq
soil
aq
524.2*/624/8260B
aq
soil
8015 mod./LUFT by
aq
GC or LUFT by GC/MS soil
625/8270C
aq
8081 / 8082
soil
aq
8260
soil
aq
8270
soil
2 VOAs
4 oz jar or tube
3 VOAs
4 oz jar or tube
3 VOAs
3 VOAs
4 oz jar
1 L amber
4 oz jar
1 L amber
4 oz jar
1 L amber
8 oz jar
1 L amber
8 oz jar
HCl
4 ± 2⁰C
HCl
4 ± 2⁰C
pH<2, HCl
4 ± 2⁰C
4 ± 2⁰C
1664A
aq
1 L amber
aq
soil
aq
soil
aq
soil
aq
soil
aq
soil
aq
soil
aq
soil
aq
soil
aq
aq
aq
soil
aq
aq
aq
soil
aq
aq
250 mL poly
4 oz jar
250 mL poly
4 oz jar
1 L amber glass
4 oz jar
250 mL poly
4 oz jar
250 mL poly
4 oz jar
1 L poly
4 oz jar
500 mL am poly
4 oz jar
250 mL poly
4 oz jar
250 mL poly
250 mL poly
500 mL poly
4 oz jar
250 mL am glass
250 mL poly
500 mL glass
4 oz jar
250 mL poly
1 L poly
200.7 / 200.8
6010B / 6020
7470
7471
CAL WET/DIWET
1311
on
Metals by ICP or ICP/MS
Container
300.0
SW-846: 7.3.3.2
& 7.3.4.2
4500CN-C/E
9014
nc
Reactive Cyanide &
Reactive Sulfide
Cyanide, Total/Amenable/Free
Sulfides, Total
9030B & 9034
Conductivity
Alkalinity
4500-H+ B/9040B
9045C
2510B
2320B
Ammonia or TKN
4500NH3-D
Total Organic Carbon
Turbidity
5310B
2130B
Flashpoint/Ignitability
1010
Residues, Total, TDS, TSS, TVS
Residue, Settleable
2540B, C, D
2540F
U
pH
Analytical Extraction
Hold Time Hold Time
14 days
n/a
14 days
n/a
14 days
n/a
14 days
n/a
14 days
n/a
7 days or 1 day (524.2)
14 days
n/a
40 days
7 days
40 days
14 days
40 days
7 days
40 days
14 days
14 days
14 days
14 days
14 days
40 days
14 days
14 days
14 days
d
TPH gasoline (TVPH),
C4-C10 or C4-C12
BTEX / MtBE / Oxygenates
Matrix
lle
Method
4 ± 2⁰C
4 ± 2⁰C
4 ± 2⁰C
tro
Organic Analyte Analysis
HOLDING TIMES & CONTAINERS
4 ± 2⁰C
HCl (prefer)or
H2SO4
HNO3
4 ± 2⁰C
HNO3
4 ± 2⁰C
4 ± 2⁰C
4 ± 2⁰C
4 ± 2⁰C
28 days incl. extraction
6 mo.
6 mo.
28 days
28 days
6 mo.
6 mo.
Hg 28 days Hg 28 days
Br, Cl, F, SO4: 28 days
NO2, NO3, PO4: 48 hr
14 days
NaOH;4±2⁰C
14d/24hr if S- present
4 ± 2⁰C
14 days
NaOH;Zn(C2O2H3)2;4±2⁰C 7 days
4 ± 2⁰C
4 ± 2⁰C
ASAP
4 ± 2⁰C
4 ± 2⁰C
H2SO4;4±2⁰C
4 ± 2⁰C
HCl; 4±2⁰C
4 ± 2⁰C
28 days
14 days
4 ± 2⁰C
n/a
4 ± 2⁰C
4 ± 2⁰C
7 days
48 hr
28 days
28 days
48 hr
*Contact OEC for complete sampling instructions
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Quality Assurance Manual
Rev 17 – June 2013
Page 70 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES
Matrix & Reporting Limit
DW (mg/L)
AQ (mg/L)
SO (mg/kg)
Bromide
0.05
0.4
5
Chloride
0.4
0.4
5
Fluoride
0.1
0.4
5
EPA 300.0
Nitrate & Nitrite as N
0.4
0.4
5
Orthophosphate as P
0.05
0.4
5
Sulfate
0.4
0.4
5
SM2320B
Alkalinity
10
--Ammonia as N
0.1
5
SM 4500-NH3 D
Total Kjeldahl Nitrogen
0.25
20
EPA 120.1 / SM2510B
Conductivity
2 μmhos/cm
--SM 4500CN-C,E / 9014 Cyanide, Total / Amenable
0.04 / 0.02
0.4
EPA 1010
Flashpoint (Ignitability)
1 ⁰F
1 ⁰F
EPA 1664A / 1664A SGC Oil & Grease / TRPH
5
100
EPA 9040B/9045
pH (Corrosivity)
0.1 unit
0.1 unit
SM5530 & EPA 420.1
Phenolics, Total
0.05
--Reactive Cyanide
0.1
0.5
EPA SW-846 7.3
Reactive Sulfide
0.4
2
SM2520B
Salinity
1
--SM2540F
Solids, Settleable (SETT)
0.1
--SM2540B
Solids, Total / % Moisture
10
0.5%
SM2540C
Solids, Total Dissolved (TDS)
10
--SM2540D
Solids, Total Suspended (TSS)
10
--SM2540G
Solids, Volatile (VS)
10
--EPA 9034
Sulfide, Total
2
--SM 5310B
Total & Dissolved Organic Carbon
0.5
1
EPA 180.1 / SM2130B
Turbidity
0.5 NTU
--Analyte
nc
on
tro
lle
d
EPA Method
INORGANICS
U
APPENDIX E – DATA CAPABILITY TABLES (continued)
Method
METALS
SM 3500 Cr-B & 7196A
SM2340B
SM 3500 Fe-B
245.1 /7470/7471
Analyte
Chromium, Hexavalent
Total Hardness
Iron, Ferrous
Mercury
Matrix & Reporting Limits
AQ (mg/L)
SO (mg/kg)
0.01
2.5
10
0.050
0.0002
----0.1
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Rev 17 – June 2013
Page 71 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
U
tro
nc
on
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Lithium
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Phosphorus
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
ICP/MS Methods
EPA 200.8 & 6020
DW / AQ (mg/L) SO (mg/kg)
0.05 / 0.1
1
0.005
1
0.002 / 0.005
0.2
0.001
0.1
0.001
0.5
0.05
1
0.001
0.2
0.1
10
0.002
0.2
0.001
0.2
0.001
0.2
0.025
2
0.001
0.2
0.003
0.3
0.1
10
0.005
0.1
0.0002
--0.001
0.2
0.01
0.2
0.05
0.5
0.1
10
0.002
1
0.05
--0.001
0.2
0.2
10
0.02
0.5
0.001
1
0.02
1
0.02
2
0.005
1
0.005
0.5
lle
Analyte
ICP Methods
EPA 200.7 & 6010B
AQ (mg/L)
SO (mg/kg)
0.05
5
0.01
5
0.01
1
0.05
0.5
0.002
1
0.05
20
0.005
0.5
0.2
50
0.002
0.5
0.002
0.5
0.005
0.5
0.025
2
0.005
1
0.025
10
0.025
5
0.005
1
----0.005
1
0.005
0.5
0.025
1
1
50
0.025
2
0.05
--0.005
1
0.1
25
0.005
0.5
0.01
1
1
10
0.01
2
0.05
2
0.1
0.5
d
Matrix & Reporting Limits
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Quality Assurance Manual
Rev 17 – June 2013
Page 72 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
Semi-Volatile
GCMS / LUFT
(where different from 8015)
TPH-Motor Oil
50
0.5
0.1
0.05
0.02
0.1
0.1
0.5
50
10
10
50
50
50
0.5
50
d
TPH-Gasoline
TPH-Crude Oil
TPH-Diesel
TPH-Diluent
TPH-Mineral Oil
TPH-Motor Oil
TPH-Crude Oil
Semi-Volatile
EPA 8015 / LUFT
Matrix & Reporting Limit
AQ (μg/L)
SO (mg/kg)
Analyte
lle
EPA Method
TPH ORGANICS
Volatile LUFT
EPA 8015 & GCMS
EPA 8015
Analyte
Matrix & Reporting Limit
DW (μg/L)
AQ (μg/L)
SO (mg/kg)
Benzene
Toluene
Ethylbenzene
Xylenes (total)
Methyl-t-butyl ether (MtBE)
on
EPA Method
VOLATILE ORGANICS
EPA 602 / 8021
tro
APPENDIX E – DATA CAPABILITY TABLES (continued)
Methanol
Total THM
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
U
nc
524.2 / 624 / 8260B
DW (μg/L)
1.0
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
0.5
0.5
0.5
0.5
0.5
0.5
AQ (mg/L)
1
AQ (μg/L)
0.005
0.005
0.005
0.005
0.005
SO (mg/kg)
5
SO (mg/kg)
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
0.5
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Quality Assurance Manual
Rev 17 – June 2013
Page 73 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
Matrix & Reporting Limit
DW (μg/L)
AQ (μg/L)
SO (mg/kg)
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
on
nc
U
0.5
0.5
0.5
1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.5
0.5
0.5
0.5
0.5
1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
lle
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,3-Dichloropropene (Total)
Ethylbenzene
1,2-Dibromoethane (EDB)
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyl Toluene
Methylene chloride
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
d
Analyte
tro
EPA Method
VOLATILE ORGANICS
524.2 / 624 / 8260B
(continued)
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Quality Assurance Manual
Rev 17 – June 2013
Page 74 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
Matrix & Reporting Limit
DW (μg/L)
AQ (μg/L)
SO (mg/kg)
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
DW (μg/L)
0.5
2
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.5
AQ (μg/L)
0.5
10
0.5
500
0.5
0.5
0.005
SO (mg/kg)
0.005
0.025
0.005
5
0.005
0.005
5
2
10
2
10
2
10
0.05
0.005
0.05
0.005
0.1
0.005
0.005
lle
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethane
Trichlorotrifluoroethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
Xylenes (Total)
d
Analyte
tro
EPA Method
VOLATILE ORGANICS
524.2 / 624 / 8260B
(continued)
t-Amyl Methyl Ether (TAME)
t-Butyl alcohol (TBA)
Diisopropyl Ether (DIPE)
Ethanol (EtOH)
Ethyl t-Butyl Ether (EtBE)
Methyl-t-butyl ether (MtBE)
on
6 Oxygenates
Appendix IX (8260)
nc
Appendix IX (8260)
(continued)
Acetone
Carbon Disulfide
Acrylonitrile
Vinyl Acetate
2-Butanone (MEK)
Methyl Isobutyl Ketone
2-Hexanone
U
Appendix II (8260)
Acetonitrile
Acrolein
Allyl Chloride
Chloroprene
Ethyl Methacrylate
Isobutyl Alcohol
Methylacrylonitrile
Methyl Methacrylate
Propionitrile
0.5
0.5
5
0.5
10
5
5
5
100
100
10
20
10
100
100
30
150
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
307 Roemer Way | Santa Maria | CA 93454
Quality Assurance Manual
Rev 17 – June 2013
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Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
Acetone
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane (EDC)
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichloro-1,1,2,2Tetrafluoroethane (Freon 114)
Diisopropyl Ether (DIPE)
1,4-Dioxane
Ethanol
Ethyl Acetate
Ethylbenzene
Ethyl t-Butyl Ether (EtBE)
0.5
0.5
0.5
0.5
0.5
2
0.5
0.5
0.5
0.5
0.5
0.5
1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
U
nc
on
tro
lle
TO-15 Full List
Matrix & Reporting Limit
AIR (ppbv)
Analyte
d
EPA Method
VOLATILE ORGANICS
0.5
0.5
0.5
0.5
0.5
0.5
0.5
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Quality Assurance Manual
Rev 17 – June 2013
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Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
4-Ethyltoluene
Heptane
Hexachlorobutadiene
Hexane
2-Hexanone
Isopropyl alcohol (IPA)
Methylene chloride
Methyl Ethyl Ketone (MEK)
Methyl Isobutyl Ketone (MIBK)
Methyl-t-butyl ether (MtBE)
Naphthalene
Propylene
Styrene
t-Amyl Methyl Ether (TAME)
t-Butyl alcohol (TBA)
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Tetrahydrofuran
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane (TCA)
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethane (Freon 11)
1,1,2-Trichlorotrifluoroethane
(Freon 113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylenes (total)
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
U
nc
on
tro
lle
TO-15 Full List
(continued)
Matrix & Reporting Limit
AIR (ppbv)
Analyte
d
EPA Method
VOLATILE ORGANICS
TPH
Gasoline (C4 – C12)
0.5
0.5
0.5
0.5
0.5
0.5
200
phone (805) 922-4772 or (661) 762-9143 | fax (805) 925-3376 | visit www.oecusa.com
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Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
d
Matrix & Reporting Limit
AQ (mg/L)
SO (mg/kg)
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
5
0.1
10
0.1
10
0.1
5
0.1
10
0.1
10
0.1
10
0.1
10
0.1
5
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
5
0.1
10
0.1
10
0.1
5
0.1
5
0.1
10
0.1
10
0.1
10
0.1
10
0.1
U
nc
on
tro
lle
EPA Method
Analyte
SEMIVOLATILE ORGANICS
EPA 625 / 8270C
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Azobenzene
Benz(a)anthracene
Benzo (b) fluoranthene
Benzo (k) fluoranthene
Benzo (a) pyrene
Benzo (g,h,i) perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chlorophenyl phenyl ether
Chrysene
Dibenz (a,h) anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
Diethyl phthalate
Dimethyl phthalate
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
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APPENDIX E – DATA CAPABILITY TABLES (continued)
d
Matrix & Reporting Limit
AQ (mg/L)
SO (mg/kg)
10
0.1
5
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.25
10
0.1
5
0.1
5
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
5
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
0.1
10
10
U
nc
on
tro
lle
EPA Method
Analyte
SEMIVOLATILE ORGANICS
EPA 625 / 8270C
Hexachlorobutadiene
(continued)
Hexachlorocyclopentadiene
Hexachloroethane
Indeno (1,2,3-cd) pyrene
Isophorone
2-Methylnaphthalene
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Phenanthrene
Pyrene
Carbazole
1,2,4-Trichlorobenzene
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
4,6-Dinitro-2-methylphenol
2-Methylphenol
3 & 4-Methylphenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,5-Trichlorophenol
Pyridine
2,4,6-Trichlorophenol
Specialty 8270
Creosote
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Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
lle
d
Matrix & Reporting Limit
AQ (mg/L)
SO (mg/kg)
0.1
0.005
0.1
0.005
0.1
0.005
0.1
0.005
0.1
0.005
0.1
0.005
0.1
0.005
0.1
0.01
0.1
0.005
0.1
0.01
0.1
0.005
0.1
0.005
0.1
0.005
0.1
0.01
0.1
0.005
0.1
0.005
AQ (μg/L)
on
tro
EPA Method
Analyte
SEMIVOLATILE ORGANICS
PNA-SIM
Acenaphthene
EPA 8270M
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo (b) fluoranthene
Benzo (k) fluoranthene
Benzo (a) pyrene
Benzo (g,h,i) perylene
Chrysene
Dibenz (a,h) anthracene
Fluoranthene
Fluorene
Indeno (1,2,3-cd) pyrene
Naphthalene
Phenanthrene
Pyrene
1,4-Dioxane
1
U
nc
1,4-Dioxane
EPA 1625M
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Page 80 of 89
Oilfield Environmental & Compliance, Inc.
APPENDIX E – DATA CAPABILITY TABLES (continued)
alpha-BHC
alpha-Chlordane
Aldrin
beta-BHC
delta-BHC
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Endrin Ketone
gamma-BHC
gamma-Chlordane
Heptachlor
Heptachlor Epoxide
Methoxychlor
Chlordane, Technical
Toxaphene
d
PESTICIDES
608 / 8081A
Matrix & Reporting Limit
AQ (μg/L)
SO (mg/kg)
Prod (mg/kg)
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.1
0.003
0.9
0.5
0.02
6
0.5
0.02
6
lle
Analyte
on
tro
EPA Method
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.02
0.02
0.02
0.02
0.02
0.02
0.02
4
4
4
4
4
4
4
U
nc
PCBs
608 / 8082
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APPENDIX F – QC DATA EVALUATION FLOWCHARTS
Evaluation of Initial Calibration
lle
d
Analyze calibration blank and
calibration standards
tro
Calculate either the correlation
coefficients or the average
response factors for each
analyte.
Does the correlation coefficient
or the average response factor
meet method specified limits?
Isolate and correct the source of
the non-linearity.
on
Yes
No
nc
Analyze initial calibration
verification (ICV) standard and
calculate % recoveries or %D of
average response factors for
each analyte.
U
Is the % recovery or %D data
within method specified limits?
No
Is the % recovery or %D data
within method specified limits?
No
Yes
Isolate and correct ICV recovery
problem then reanalyze ICV.
Yes
Begin analysis of method blanks,
samples and QC spikes
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Oilfield Environmental & Compliance, Inc.
APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
d
Evaluation of Continuing Calibration
tro
Is the % recovery or %D data
within method specified limits?
No
Isolate and correct the source of
the problem.
Reanalyze the CCV and
calculate % recoveries or %D of
average response factors for
each analyte.
on
Yes
lle
Analyze continuing calibration
verification (CCV) standard and
calculate % recoveries or %D of
average response factors for
each analyte.
U
nc
Continue sample analysis.
Yes
Is the % recovery or %D data
within method specified limits?
No
Reanalyze CCV and/or
reanalyze calibration standards
to generate a new calibration
curve. Then reanalyze ICV.
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Oilfield Environmental & Compliance, Inc.
lle
d
APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
Evaluation of Method Blank and Instrument Blank Results
Reanalyze blanks and samples
as appropriate.
tro
Are method blank and/or
instrument blank results less
than the RL (Reporting Limit) for
a target analyte?
Yes
No
on
Isolate and remove the source of
the contamination.
nc
Yes
No
Report blank results with an
appropriate footnote.
U
Report blank results as ND (not
detected).
Has this contamination affected
the sample results? (Is the
blank response >5% of any
related sample response?)
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APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
Evaluation of Sample Results for Inorganic Analytes
d
Is the appearance of the sample
or the prepared sample normal?
Is the sample result within
the calibration range?
No
Dilute sample to midrange and re-analyze.
on
Yes
Consider filtering or diluting the
sample before analysis. (If diluted,
raise the RL appropriately.)
tro
Yes
lle
No
Is the precision of the
duplicate analysis within
method-specified limits?
No
Reanalyze the sample
and the sample duplicate.
nc
Yes
Is the matrix spike
recovery within method
specified limits?
U
Yes
Report the results.
No
Is the post-digestion MS
recovery within methodspecified limits?
Yes
Report the results, but
qualified due to matrix
interference.
No
Consider qualifying the
sample(s) using the
method of standard
additions.
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Oilfield Environmental & Compliance, Inc.
APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
Evaluation of Sample Results for Organic Analyses
For GC/MS analyses, are
samples analyzed within the
12-Hour Tune window?
Reanalyze outlying samples.
d
No
Review peak integration and
retention limits.
No
No
Yes
Correct problem and
reanalyze appropriate
samples.
No
Yes
Correct problem and
reanalyze appropriate
samples.
Has this change affected
sample results?
tro
Are retention times consistent
and within retention time
windows (0.06 RRT units for
GC/MS methods?
lle
Yes
Are internal standard areas
within method-specified limits?
Yes
No
on
Are surrogate recoveries within
method-specified or laboratoryestablished control limits?
Refer to flowchart for
evaluation of surrogate
recoveries.
Yes
nc
Are target analyte
concentrations within the initial
calibration range?
No
Dilute samples to mid-range
and reanalyze.
Yes
Are obvious matrix
interferences present?
Yes
Cleanup the sample using the
appropriate technique(s) and
reanalyze using the same or
modified procedure.
U
No
If there are positive results,
are they confirmed in the
conformational analysis?
(Req’d for GC/PID/ECD only;
MS is considered
confirmatory.)
Yes
Report the results.
Adjust RL values to reflect any
changes (dilutions, etc.) in the
modified analytical procedure.
No
Report the negative confirmation
results as Not Detected (ND).
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Oilfield Environmental & Compliance, Inc.
APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
Evaluation of Surrogate Compound Recoveries
Yes
No
Yes
Reanalyze the affected samples
to confirm the interference.
tro
Is there matrix interference
present for any analyte?
Report the results.
lle
Are the surrogate % recoveries
within method-specifies or labestablished control limits?
d
Calculate surrogate % recoveries
for each sample batch.
No
Yes
on
Are all the surrogate recoveries
above the upper limit and the
sample result(s) all ND?
No
Did the sample produce an
emulsion, or did a precipitate
form during the extraction step?
Yes
Report the results qualified with
appropriate footnote.
nc
No
U
Reanalyze the sample(s) and
calculate the surrogate
%recoveries.
Are the surrogate % recoveries
within method-specifies or labestablished control limits?
No
Report the results from the
second analysis.
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d
APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
lle
Evaluation of Laboratory Quality Control Sample & Duplicate
tro
Analyze LCS (& LCSD as
appropriate).
Are % recovery data within
method-specified or laboratoryestablished control limits?
No
Isolate and correct the source of
the problem. Reanalyze
LCS/LCSD.
No
on
Yes
No
Are % recovery & RPD values
within method-specified or
laboratory-established control
limits?
Report LCS results.
Reanalyze (or re-extract &
reanalyze) all associated
samples.
Are RPD values within methodspecified or laboratoryestablished control limits?
Yes
U
nc
Yes
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APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
Evaluation of Matrix Spike Recoveries
lle
Is the matrix spike % recovery
data within method-specified or
lab-established control limits?
Yes
Report the results.
Report results with a qualifier
indicating that native sample
analyte levels are too high to
reflect any degree of accuracy.
tro
No
d
Calculate % recoveries of all
matrix spike analytes in the MS
& MSD samples.
Is the matrix spike level at least
five times the level of a spike
analyte found in the un-spiked
sample?
No
Yes
Yes
Reanalyze the sample
and its MS/MSD.
Are any of the matrix-spiked
analytes positive detections
(above RL) in the samples?
on
Subtract related
sample contribution.
nc
No
U
Are there matrix interferences
present?
Dilute if necessary and
reanalyze.
Yes
Report the results with a
qualifier indicating that matrix
interference is present.
No
Are the results for the associated
LCS within control limits?
or
Yes
Report the results qualified
with an appropriate footnote.
No
Reanalyze all the samples and
the matrix spiked sample in the
batch.
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APPENDIX F – QC DATA EVALUATION FLOWCHARTS (CONT.)
Evaluation of Duplicate Sample and/or Matrix Spike Duplicate Results
No
Is the sample homogenous?
lle
No
on
Yes
Yes
Report the results.
tro
Is the RPD data within methodspecified or lab-established
control limits?
d
Calculate the relative
%difference (RPD) for duplicate
sample results or for duplicate
matrix spike results.
Are the sample results less than
five times the RL?
Yes
Report the results with a
qualifier concerning the nonhomogenous nature of the
sample.
Report the results with a
footnote indicating that the high
RPD is due to the results being
near the PQL.
nc
No
U
Reanalyze the duplicates or
duplicate matrix spikes.
If reanalysis also produces
similar out-of-control results,
report the results qualified with
an appropriate footnote.
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