Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Page:771 Trimsize:8.5 in×11 in Appendix A A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS A-1 PROCESS FLOW DIAGRAMS USING VISIO 2002 SOFTWARE Figure 1-12b Process flow diagram (Feed and fuel desulfurization section). Figure 1-12c Typical process flow diagram for the production of Methyl Tertiary Butyl Ether (MTBE). Figure 1-14 Piping and instrumentation diagram for Ammonia plant CO2 removal. Figure 1-15 Piping and instrumentation diagram: Ammonia synthesis and refrigeration unit (2). A-2 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. PROCESS DATA SHEETS Air cooled heat exchanger process data sheet Centrifugal pump schedule: driver Centrifugal pump schedule: pump Centrifugal pump summary Column schedule Deaerator process data sheet: Deaerated water storage tank Deaerator process data sheet: Deaerator head Drum process data sheet Effluent schedule Equilibrium flash calculation Fabricated equipment schedule Fan/Compressor process duty specification Fractionator calculation summary General services and utilities checklist Hazardous chemical and conditions schedule Heat and mass balances 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. 33. 34. 35. 36. 37. 38. 39. 40. 41. 42. 43. 44. 45. Heat exchanger rating sheet Hydrocarbon dew point calculation Line list schedule Line schedule Line schedule sheet Line summary table Mass balance Mechanical equipment schedule Pipe line list Pipe list Piping process conditions summary Plate heat exchanger data sheet Calculation of pressure drop in fixed catalyst beds Process engineering job analysis summary Pump calculation sheet Pump schedule Relief device philosophy sheet Tank and vessel agitator data sheet Tank process data sheet Tank schedule Tie-in-schedule Tower process data sheet Tray loading summary Trip schedule Utility summary sheet Vessel and tank schedule Vessel and tank summary: driver Vessel schedule Water analysis sheet 771 Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:772 772 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS AIR COOLED HEAT EXCHANGER PROCESS DATA SHEET A.K.C. TECHNOLOGY Document No. Sheet of Item No.(s) No. Working Job Item Name Rev. Total No. Off Unless otherwise stated, fluid properties are for mean fluid temperature. For lines 30-36 this is mean from dewpoint to outlet temperatures. UNITS 1 2 3 4 5 6 7 8 9 10 11 12 13 TUBE SIDE DATA Fluid Circulated 14 15 16 17 18 19 20 GAS (AND VAPOR) 21 LIQUID IN 22 23 24 25 26 Total Flow of Liquid at Inlet Thermal Conductivity: In/Out Specific Heat Density Viscosity 27 CONDENSATION 28 29 30 31 32 33 34 35 36 Fluid Condensed Molecular Weight Thermal Conductivity Specific Heat Density Viscosity Latent Heat %Condensate Forming Film Temps. for Phase Change: In/Out 37 COOLING CURVE DATA 38 39 40 %Heat Load Condensing Fluid Temp. °C 41 AIR SIDE DATA 42 43 44 Design Inlet Temp. Max/Min No. of Fans Assumed Estimated Power per Fan 45 SITE DATA 46 47 48 49 50 Altitude Plot Size Limitations Noise Limits Atmospheric Contamination 51 52 53 54 55 NOTES MATERIALS Total Fluid Entering (Normal) Flow Margin Temperature: In/Out kg/h % °C Max. Pressure Drop at Line 4 bar psi Inlet Pressure: Operat./Design barg psig Normal Heat Load Heat Load Margin Design Temperature Corrosion Allowance Fouling Resistance Line N.B.: In/Out kW % °C mm Btu/h % °F in. Tubes Fins Header Boxes Tubesheets Stress Relief Yes/as Codes Radiography Yes/as Codes Sour Service Yes/No lb/h % °F °Fft2h/Btu in. m2 °C/W mm. PROCESS CONTROL REQUIREMENTS Flow of Vapor & Gas at Inlet Molecular Weight: In/Out kg/h Thermal Conductivity: In/Out Specific Heat Compressibility Factor Viscosity W/m °C kJ/kg °C 1 In / Out Local / Remote Set Hand / Automatic Adjustable Pitch Fans Variable Speed Motor Louvres Air Recirculation lb/h Btu/h.ft. °F Btu/lb. °F cP lb/ft.h kg/h W/m °C kJ/kg °C lb/h Btu/h.ft. °F Btu/lb. °F kg/m3 cP lb/ft3 lb/ft.h kg/h lb/h W/m °C kJ/kg °C Btu/h.ft. °F Btu/lb. °F lb/ft3 lb/ft.h Btu/lb % °F kg/m3 cP kJ/kg % °C °C °F kW Length: Date 2 Width: Date 3 Date 4 Date 5 Date Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines A.K.C. Job No.: Job Name: Document No. Project No. Client Location Plant ITEM No. TECHNOLOGY TYPE HP RPM ROTATION CW-CCW CENTRIFUGAL PUMP SCHEDULE: DRIVER ELECTRICAL CHARACTERISTICS Sheet of NEMA FRAME Issue No.: Description Made/Revised by Checked by Approved Process Approved STEAM CONDITIONS psig TEMP, ° F 1 MAKE Date MODEL 2 STEAM RATE Date WEIGHT 3 P.O. No. Date Elsevier US Job Code:CAPA Fonts used:Times & Universal 55 family Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:773 Text Width:41p6 Trimsize:8.5 in×11 in 773 Depth:65 Lines Job No.: Job Name: Document No. Project No. Client Location Plant ITEM No. No. OF UNITS A.K.C. TECHNOLOGY SERVICE MAKE CENTRIFUGAL PUMP SCHEDULE: PUMP MODEL PUMP Sheet of TYPE SIZE CONNECTION SUCTION DISCHARGE Issue No.: Description Made/Revised by Checked by Approved Process Approved WEIGHT 1 REFERENCE DRAWINGS Date PURCHASE ORDER No. 2 SEAL TYPE Date TYPE COUPLING 3 FILE REFERENCE Date Elsevier US Job Code:CAPA Chapter:0capaappA Fonts used:Times & Universal 55 family Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:774 Text Width:41p6 Trimsize:8.5 in×11 in 774 Depth:65 Lines Job No.: Job Name: Document No. Project No. Client Location Plant ITEM No. No. OF UNITS A.K.C. TECHNOLOGY SERVICE LIQUID Fonts used:Times & Universal 55 family °F OPERATING TEMPERATURE CENTRIFUGAL PUMP SUMMARY SpGr OPER. TEMP. Sheet of GPM OPER. TEMP. Issue No.: Description Made/Revised by Checked by Approved Process Approved NPSHA ft DISCHARGE PRESSURE psig 1 SPEED RPM Date BHP PUMP 2 HP DRIVER Date DRIVER TYPE 3 FILE REFERENCE Date Elsevier US Job Code:CAPA Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:775 Text Width:41p6 Trimsize:8.5 in×11 in 775 Depth:65 Lines A.K.C. Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Bottom Top Bottom Top Issue No.: Description Made/Revised by Checked by Approved Process Approved Bottom Top 1 Bottom Date Top 2 Bottom Date Top 3 Bottom Date 22-12-2006 mm °C barg mm/m3 kg/m3 Top Sheet of Chapter:0capaappA 17 Other Internals 18 19 20 21 Operating – Pressure – Temperature 22 Design – Pressure 23 – Temperature 24 25 Vacuum Design 26 Material: Shell Liner 27 Internals 28 29 30 Shell Corrosion Allowance 31 Sour Service 32 Stress Relieved for Process Reasons 33 Insulation 34 35 36 Notes 37 38 39 40 41 42 43 44 45 – Density mm Units mm mm mm mm COLUMN SCHEDULE Job Code:CAPA 16 Job No.: Job Name: Document No. Project No. Client Location Plant 1 Item Number 2 Item Name 3 Number Required 4 5 Shell Diameter (ID/OD) 6 Shell Length (T.L. - T.L.) 7 Overall Shell Length - (T.L. - T.L.) 8 Base Elevation 9 Trays – Type – Number 10 – Spacing 11 – Liquid Flow 12 Packing – Type 13 – Number of Beds 14 – Bed Height/Volume 15 TECHNOLOGY Elsevier US 5:26 p.m. Font Size:9/10 pt Page:776 Text Width:41p6 Trimsize:8.5 in×11 in 776 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:777 APPENDIX A A.K.C. TECHNOLOGY Document No. Sheet of DEAERATOR PROCESS DATA SHEET Job Item Name 777 Rev. Item No.(s) DEAERATED WATER STORAGE TANK No. Working Total No. Off NOTE: ∗ indicates delete as necessary: ∗∗ indicates for other than code reason. 48 49 50 51 52 53 54 55 STANDARD TANK DIMENSIONS ENGLISH METRIC LENGTH O.D. LENGTH VERTICAL TANK ONLY 10′–3″ 1600 3100 5′–3″ 15′–0″ 1800 5000 6′–0″ 18′–6″ 2000 6000 6′–9″ 21′–0″ 2200 6600 7′–0″ TANK SIZE 2 m3 5 m3 10 m3 15 m3 20 m3 C-3 C-1 FOR DETAILS AND MATERIALS OF DEAERATOR HEAD SEE SHEET 2. O.D. BAFFLE WALL CROSS SECTION C-4 C-9 C-8 C-6 R-2 C-2 NWL A-1 MANWAY R-4 R-3 NOTE 5 MANWAY R-1 R-4 C-10 C-7 R-3 C-5 VORTEX BREAKER Shell Diameter (O.D.) Center Line: ∗Horizontal Pressure: psig Shell Length: (T.L. - T.L.) bar g Operating 3.0 0.237 Design 10.0 0.73 emergency Vacuum Design: ∗Yes Material Shell CS Heads CS Liner Type of Heads Code: Stress Relieve∗∗: Yes Radiography∗∗: No joint Efficiency: Weight Empty: Is vessel subject to mechanical vibration? Insulation: Conservation ∗Yes NOTES 1) Corrosion Allowance on Tank Only Temperature: °F 223 241 °C 106 116 Corr. Allowance 1/16" (1.6mm) NOTE 1/16" (1.6MM) 1 No. Required Nozzles Inlet Steam In Vapour Out Mark No. C-1 C-2 C-3 Size In Sample Point Liquid Out Cond. Out C-4 C-5 C-6 1 1 1 Vent Drain Steam Out CC-7 C- 1 Pressure Relief Spill Back Start Up C-8 C-9 C-10 1 1 1 Manhole A-1 1 Thermocouple Pressure Gauge Gauge Glass Level Control R-1 R-2 R-3 R-4 1 1 2 2 Min. Base Elevation: 56 Date NOTE 4 NOTE 4 NOTE 3 NOTE 2 2) Water Hammer Only 3) Sparge Pipe To Have Delavan Type BB Nozzles and Terminate 1000mm Before Baffle. 4) Allow for Temp of Desuperheating Steam or condensate at Inlet Nozzles. 5) Normally at 0.67 Dia. Above Base. 1 Qty 1 1 1 Weight Full: by Inst. Gp. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 2 Date Material: 3 Date Incl.LAHL/LL Skirt Length: 4 Date 5 Date Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:778 778 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS A.K.C. TECHNOLOGY DEAERATOR PROCESS DATA SHEET Job Item Name DEAERATOR HEAD Document No. Sheet of Item No.(s) No. Working Rev. Total No. Off C3 MIN PERFORATED AREA NOTE 6 C1 1/2" SEAL PAN DETAILS OF C4 (12 mm) 1" N.B.S.S. PAD 1" S.S. FLANGE 11/4" (30 mm) ½" S.S. PIPE C4 GASKET 1. DESIGN FOR FULL VACUUM. OPERATING TEMPERATURE _______________ OPERATING PRESSURE __________________ 2. TRAYS TO BE SEALED TO SHELL WITH STEAM QUALITY RUBBER GASKETS. 3. C4 TO BE CAPPED FOR SITE INSTALLATION OF STANDARD SAMPLING EQUIPMENT. 4. HEAD TO BE IN S.S OR COATED M.S. BELOW 120°C MAX. EPOXY RESIN BELOW 180°C MAX. STOVED PHENOLIC RESIN (SAKAPHEN). PROCESS TO ADVICE ON SPECIFICATION & APPLICATION. 5. TRAYS TO BE IN 18/8 S/S. TRIANGULAR PERFORATION. PATTERN TO BE N.GREENING'S___ OR EQUAL. NOTE: Bubbling Area Is Any Part Of Tray Within 4" Distance Of A Hole NOZZLES MARK SIZE C-1 Water Inlet C-3 Vent C-4 STD Sample Point Perf. Area/Tray Bubbling Area/Tray No. Of Trays Tray Thickness Hole Diameter Pitch. Approx. No. of Holes/Tray 1 Date Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family 6. SPRAY NOZZLE TO BE IN 18/8 S/S. SIMILAR TO DELAVAN WATSON S. _______________ AND WITHDRAWABLE THROUGH C-1. QTY FLOWS (kg/hr) NORMAL 1 2 Margins:Top:3p6 Water Feed 1 Water Feed 2 Water Feed 3 Heating Steam Start-Up Steam Vent Steam Deaerated Feed Water ∗ No. Of Hole Is More Important Than Pitch Date 3 Date 4 Gutter:4p6 Font Size:9/10 pt Date DESIGN 5 Text Width:41p6 Date Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:779 APPENDIX A Doc. No: DRUM PROCESS DATA SHEET A.K.C. TECHNOLOGY Item No. Job: Distribution: 779 Sheet of Item Name: NOTE: ∗indicates delete as necessary; ∗∗indicates for other than Code reason 5 10 15 20 Shell Diameter (O.D. / I.D.): Center+C71 Line: ∗Horizontal / Vertical °F /°C g Pressure: Temperature: Item Number Operating Design Emergency Vacuum Design: ∗ Yes / No Material Corr. Allowance Shell Heads Liner Type of Heads Code: Stress Relieve∗∗: Radiography∗∗: Shell Length: Nozzles Inlet Mark No. C- Vapor Out C- Liquid Out: C- Thermocouple Pressure Gauge Gauge Glass Level Control Safety Valve RRRRR- Joint Efficiency: ∗°F / °C Density of Contents: at Weight Empty: Weight Full: Is vessel subject to mechanical vibration? ∗Yes / No Vent Type: ∗Frost and Personnel Protection / Cold insulation: Drain ∗Yes / No Steam Out / Anticondensation / Heat Conservation REMARKS: Manhole Issue No. Made/Revised by Checked by Approved - Process Approved by Fonts used:Times & Universal 55 family 1 Margins:Top:3p6 Date Gutter:4p6 2 No. Required: Size Number by Inst. Op. 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 CCCA- min. Base Elev'n: Material: Date Font Size:9/10 pt 3 Date 4 Text Width:41p6 Date Depth:65 Lines EFFLUENT SOURCE EFFLUENT SCHEDULE of FLUID Sheet TOTAL FLOWRATE tonne/h. Issue No.: Description Made/Revised by Checked by Approved- Process Approved MAIN CONTAMINANTS CONTAMINANT kg/h. QUANTITY 1 Date CONTAMINANT CONCENTRATION STREAM TEMP. °C. 2 Date Job Code:CAPA Fonts used:Times & Universal 55 family 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 Notes: 43 44 45 46 47 48 STREAM NUMBER Job No.: Job Name: Document No. Project No. Client Location Plant A.K.C. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:780 Text Width:41p6 Trimsize:8.5 in×11 in 780 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:781 APPENDIX A PROCESS DATA SHEET A.K.C. TECHNOLOGY 781 Job No. Item No. Sheet of Job: EQUILIBRIUM FLASH CALCULATION (Form 1 of 2) °F psia psia Temperature: Pressure: Pg: V = L Assumed m K K V +1 L K m V +1 L m V K L +1 K V +1 L K m V +1 L K 3 Date V +1 L K m V +1 L K 4 Date V +1 L K m V +1 L K 5 Date V +1 L H2 CO CH4 CO2 C2H6 C3H8 i-C4H10 n-C4H10 C2H4 C3H6 C6H6 ∑ K V +1 = m L Calculated V = L Calculated Issue No. Made/Revised by Checked by Approved - Process Approved by Fonts used:Times & Universal 55 family 1 V = L ∑K Date Margins:Top:3p6 1 −1 m V L 2 Gutter:4p6 +1 Date Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Page:782 Trimsize:8.5 in×11 in 782 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS Job No. PROCESS DATA SHEET A.K.C. TECHNOLOGY Item No. Job: Sheet of EQUILIBRIUM FLASH CALCULATION (Form 2 of 2) °F psia psia Temperature: Pressure: Pg: MOLES MOL. FRACTION Gas Vy Liquid Lx Feed m Liquid x Gas y H2 CO CH4 CO2 C2H6 C3H8 i-C4H10 n-C4H10 C2H4 C3H6 C6H6 Lx = Issue No. Made/Revised by Checked by Approved - Process Approved by Fonts used:Times & Universal 55 family m Vy = m − Lx K V +1 L 1 Date Margins:Top:3p6 2 Date Gutter:4p6 3 Date 4 Font Size:9/10 pt Date 5 Date Text Width:41p6 Depth:65 Lines A.K.C. No. OFF DESCRIPTION DIAMETER (m) FABRICATED EQUIPMENT SCHEDULE LENGTH (m) Sheet of SURFACE (m2/SHELL) (tonne/SHELL) WEIGHT S = Shell T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S T S (See Note 1) MATERIAL FLUID T = Tube Date 1 H.E. TYPE INTERNALS/ Issue No.: Description Made/Revised by Checked by Approved- Process Approved PRESSURE (kg/cm2.g) DESIGN 2 TEMPERATURE (°C) CONDITIONS Date REMARKS 3 Date Job Code:CAPA Fonts used:Times & Universal 55 family Notes: 1. H.E. Type Coding - A.C. = Air Cooler; K = Kettle; U.B. = U - Tube Bundle; F.H. = Floating Head; F.T.S. = Fixed Tube Sheet Job No.: Job Name: Document No. Project No. Client Location Plant ITEM No. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:783 Trimsize:8.5 in×11 in 783 Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:784 784 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS FAN/COMPRESSOR PROCESS DUTY SPECIFICATION A.K.C. TECHNOLOGY Document No. Sheet of Item No.(s)\ No. Working Job Item Name 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 Rev. Total No. Off OPERATING CONDITIONS PER UNIT UNITS Operating Case Mass Flowrate Standard Volumetric Flowrate Volume at Suction kg/h nm3/h m3/h lb/h std ft3/h ft3/h INLET CONDITIONS bara psia °F °C Pressure Temperature Molecular Weight Cp/Cv Compressibility DISCHARGE CONDITIONS bara psia o o C F Pressure Temperature Cp/Cv Compressibility GAS ANALYSIS Mol % Mol % Entrained Liquids/Solids PERFORMANCE Compression Ratio Estimated Efficiency Estimated Absorbed Power Recommended Driver Power % % kW hp kW hp MECHANICAL ARRANGEMENT Compressor/Fan Type Number of Stages Gas to be kept Oil Free SKETCH Yes / No Driver Type Casing Design Pressure Design Pressure Material - Casting - Impeller Yes / No Sour Service NOTES 1. Cooling medium available:- 1 Date 2 Date 3 Date 4 Date 5 Date Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:785 APPENDIX A Job No: Item No: Sheet ____ of _____ FRACTIONATOR CALCULATION SUMMARY A.K.C. TECHNOLOGY 785 Job: Item Name: Distribution 1 Operate at 2 Fractionation: psig 3 Ovhd Prod: C < Reflux Ratio: Actual: ; Use 4 Bottoms: C < Rectifying Plates: Theoretical: ; Use Stripping Plates: Theoretical: ; Use Reflux Ratio & No. of Plates: 5 Feed 6 7 8 Units: Metric / British (delete one) Net Bottoms Ksca o C Component 9 1 10 2 11 3 12 4 13 5 14 6 15 7 16 8 17 9 18 10 Mols Mol % Mols Mol % K KX psia o F Vapour o Pat oC F Pressure 19 Net Overheads 20 21 Component 22 23 1 24 2 25 3 26 4 27 5 28 6 29 7 30 8 31 9 32 10 Mols Mol % K Gross Overheads Ext. Rflx. Ksca o C psia o F KX or Y K Mols Mols Mol % K Ksca o C psia o F Y K 33 34 Thermal Conditions of Feed: Reboiler Vapour Quantity: 35 36 37 38 39 40 41 Stream 42 o API Sp.Gr. at 15oC o Temp. at 60oF 43 44 Feed 45 Net Bottoms 46 Net Overheads 47 Gross Overheads 48 Gross Bottoms 49 Reboiler Vapour o C F Sp.Gr. at To Sp. Vol. At T o cu. m/kg Mols/hr Mol. Wt. Kg/hr lb/hr Date 3 Date cu. Ft/lb 50 51 52 53 REMARKS 54 55 56 Issue No. 57 Made/Revised by 58 Checked by 59 Approved - Process 60 Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 1 Date Font Size:9/10 pt 2 Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:786 786 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS A.K.C. TECHNOLOGY GENERAL SERVICES AND UTILITIES CHECKLIST Job No.: Job Name: Document No. Project No. Client Location Plant PREPARED BY: Sheet of DATE: SERVICE SUSTAINED QUANTITY PEAK UNIT ELECTRICAL 13.8 KV * KVA ELECTRICAL 2300 V * KVA ELECTRICAL 440 V * KVA MISC. LIGHTING, ST. ETC., (110 V) WELL WATER (CITY) SEA WATER RIVER WATER – PROCESS RIVER WATER – FIRE PROT. * FUEL GAS ODORIZED GAS SCFM SCFM COMPRESSED AIR SCFM STEAM (400 OR 475) Psig 235 Psig 150 Psig 30 Psig CONDENSATE RETURN CONDENSATE USAGE PROCESS TRANSFER AND RAW MATERIALS CAUSTIC (–%) BRINE (–%) LPG lb/h lb/h lb/h lb/h lb/h lb/h lb/h OPERATING PRESSURE AND TEMPERATURE REMARKS KVA gpm gpm gpm gpm lb/h lb/h lb/h SITE DEV. (AREA FILL) RAIL ROADS BLOCK ACCESS ROADS gpm gpm SANITARY SEWERS WASTE WATER * ASSUME 1 HORSE POWER = 1 KVA NOTE: ONE COPY OF THIS LIST TO BE GIVEN TO SERVICE AND UTILITY SECTION. Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines 2 Chemical Symbol 3 Phase 4 Location in Plant Fonts used:Times & Universal 55 family 4. Column 11 Open Cup (Note 3) 7 6 Flash Point ° C Closed Cup 5 Issue No.: Description Made/Revised by Checked by Approved Process Approved Toxicity Sheet of HAZARDOUS CHEMICAL AND CONDITIONS SCHEDULE Lower A – Water E – Foam B – Powered Talc F – See Remarks C – CO2 D – Dry Chemical Upper 8 9 Fire Hazard Explosive Limits % by Volume in Air 1 12 Date Equipment Protective B.A. – Breathing Apparatus F.C. – Full Clothing F.W. – Footware G.O. – Goggles Extinguishing Agents Temp ° C 5. Column 12 Suitable 1 2 Autoignition 10 Date 13 G.V. – Gloves X – See Remarks. Remarks Job Code:CAPA Note: 1. This Schedule is given without any Legal responsibility on the part of AKC Technology. 2. Column 3: Vapor – V, Liquid – L, Solid – S 3. Toxicity: Denotes Threshold Limit (T.L.) under which it is believed nearly all workers may be exposed day after day without adverse effect. The figures relate to average concentration for a normal working day. 1 Chemical Hazard Job No.: Job Name: Document No. Project No. Client Location Plant A.K.C. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:787 Trimsize:8.5 in×11 in 787 Text Width:41p6 Depth:65 Lines Fonts used:Times & Universal 55 family 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 Stream HEAT AND MASS BALANCES Units →? Job Name: Job No.: °API K of M.W. Sheet SpGr FLOWING *barg psig *° F °C ? Issue No.: Made/Revised by Checked by Approved Process Approved by B.P.S.D. at 60° F 1 GPM FLOWING Date Mol % 2 Mol/h Date lb/h *kg/h 3 ? Btu/lb *kcal/kg Date ? 106 Btu/h *106 kcal/h Job Code:CAPA ↓ * delete unit as necessary A.K.C. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:788 Text Width:41p6 Trimsize:8.5 in×11 in 788 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:789 APPENDIX A 789 Document No. A.K.C. TECHNOLOGY HEAT EXCHANGER RATING SHEET Sheet of Items No. (s) PART 1 - TO BE FILLED IN COMPLETELY 1 Exchanger Name: 2 Job: * Location: * * Arrangement: Horiz = 0; Vert = 1 3 Type of Unit: F.T.S.=0; FLTG.HEAD=1; U-TUBE=2; FOR KETTLES ADD 3 4 Hot Side: Either=0; Shell=1; Tubes=2 5 Units Units: S.I. 0; Engineering = 1 S.I. Engineering 6 Fluid Circulated - - 7 Total Fluid Entering (Normal) kg/hr lb/hr 8 Flow Margin % % 9 Temperature In/Out °C °F bar psi 11 Inlet Pressure Operating/Design barA psia 12 Normal Heat Load kW 13 Heat Load Margin % % 14 Design Temperature °C °F 10 Max Pressure Drop at line 8 Rev. * HOT FLUID COLD FLUID Btu/hr 15 Corrosion Allowance mm ins 16 Fouling Resistance °Cm2/Wl °F hr ft2/Btu 17 Line N.B. In/Out mm ins 19 GAS (AD VAPOR) IN - - 20 Flow of Vapor and Gas at Inlet kg/hr lb/hr 21 Code Number - - 18 Part 2 22 Molecular Weight - - 23 Thermal Conductivity W/m °C Btu/hr ft °F 24 Specific Heat kJ/kg °C Btu/lb °F 25 Compressibility Factor - - 26 Viscosity cP lb/ft hr 27 LIQUID IN - - 28 Total Flow of Liquid at Inlet kg/hr lb/hr 29 Code Number - - 30 Thermal Conductivity W/m °C Btu/hr ft °F 31 Specific Heat kJ/kg °C Btu/lb °F 32 Density kg/m3 lb/ft3 33 Viscosity cP lb/ft hr 34 Viscosity at Ave. Temp. other side cP lb/ft hr 35 CONDENSATION AND VAPORIZATION - - 36 Fluid Condensed or Vaporized kg/hr lb/hr 37 Code Number - - 38 Molecular Weight - - W/m °C 39 Thermal Conductivity Btu/hr ft °F 40 Specific Heat kJ/kg °C Btu/lb °F 41 Density (Hot Fluid) kg/m3 lb/ft3 42 Compressibility Factor (Cold Fluid) - - 43 Viscosity cP lb/ft hr 44 Latent Heat kJ/kg Btu/lb 45 Surface Tension N/m lb/ft 46 Expansion Coefficient 1/ °C 1/ °F 47 % Condensate Forming Film % 48 Thermal Conductivity W/m °C % Btu/hr ft °F 3 3 49 Density kg/m lb/ft 50 Viscosity cP lb/ft hr 51 Temps for Phase Change Start/Finish °C °F 52 LMTD weighting Factor 'F' - - 53 PART 3 54 Number of Points in Table Below 55 % Heat Load % % 56 Hot Fluid Temperature °C °F 57 Cold Fluid Temperature °C °F 1 2 3 4 5 6 7 8 9 10 58 PART 4 - CODE NUMBERS TO BE FILLED IN COMPLETELY 59 Material for Description Code No. O.D. Thickness Length Passes Number Contents Lethal? Δ Yes/No 60 Tubes Yes/No 61 Shell 62 Floating Head Tube Pitch = mm/in. o 63 Channel 64 Tube Sheets NOTES Issue No. 1 Date 2 Date 3 Date 4 Date 5 Date Made/Revised by Checked by Approved- Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:790 790 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS HYDROCARBON DEWPOINT CALCULATION A.K.C. TECHNOLOGY Job No: Item No. Job: Heaviest Compound: y H2 N2 CO CH4 C2H4 CO2 C2H6 C2H2 C3H6 C3H8 Tb 67 130 172 201 305 330 332 340 406 416 Page PROPANE LIGHT COMPONENT TbFeL FeL 67.000 1.000 2.972 0.0229 0.797 0.0046 0.383 0.0019 HEAVY COMPONENT FeH TbFeH 0.105 0.180 0.244 0.548 0.638 0.646 0.676 0.954 1.000 Pressure: psia Convergence Pressure: psia o ASSUMED TEMPERATURE o o F F F K y/K K y/K K y/K o F K of y/K F x 13.61 31.00 49.02 167.0 210.6 214.3 229.9 387.3 416.0 Σ y/K 1.000 o 1.000 x for H2 Σ (yFeL/K) Σ (yFeH/K) E.B.PL E.B.PH Pg Estimate of Dewpoint: at Estimate Pg of: Issue No. Made/Revised by Checked by Approved - Process Approved by Fonts used:Times & Universal 55 family 1 Date 2 Margins:Top:3p6 Date Gutter:4p6 3 o F psia Date Font Size:9/10 pt Text Width:41p6 Depth:65 Lines A.K.C. TECHNOLOGY Fonts used:Times & Universal 55 family PRESSURE: barg SIZE psig kg/cm2 g 3 4 5 NOM. PIPING FLUID PIPE SPEC. DENSITY PHASE 6 Issue No.: Description Made/Revised by Checked by Approved Process Approved °C °F TEMP. 1 Date 2 mm 10 INSULATION CLASS NOM. THICK NOMINAL PIPE SIZE in. 7 8 9 ROUTING PLANT OPERATING DESIGN TO CONDITION PRESS. TEMP. PRESS. TEMPERATURE: LINE FROM Sheet of 11 CLASS TEST Date PRESS. TEST Date Insulation Thickness CLASS FIELD 3 in. CLASS 4 FIELD TEST 5 12 mm Date 6 Date 13 14 14a CHEMICAL REMARKS STRESS CLEANING CATEGORY PRESS. LIMITED BY Date No. 15 16 ELD ISO. DRG. DRG. No. Chapter:0capaappA Margins:Top:3p6 UNITS: 2 2A LINE LIST SCHEDULE Job Code:CAPA DATA CHANGES Job No.: Job Name: Document No. Project No. Client Location Plant 1 ISS LINE COLUMN No. Elsevier US 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:791 Text Width:41p6 Trimsize:8.5 in×11 in 791 Depth:65 Lines Job No.: Job Name: Document No. Project No. Client Location Plant LINE NUMBER A.K.C. TECHNOLOGY SIZE in. FROM LINE SCHEDULE TITLE: TO Fonts used:Times & Universal 55 family LINE CLASS OR CODE Sheet of INSULATION CODE TEST PRESSURE, psig Issue No.: Description Made/Revised by Checked by Approved Process Approved by SPECIAL REMARKS 1 Date 2 Date 3 Date Elsevier US Job Code:CAPA Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:792 Text Width:41p6 Trimsize:8.5 in×11 in 792 Depth:65 Lines Job No.: Job Name: Document No. Project No. Client Location Plant LINE FLOW NUMBER MEDIUM A.K.C. TECHNOLOGY QUANTITY QUANTITY FLOW, gpm FLOW or SCFH lb/h FLUID TEMP. °F Sheet of LINE SCHEDULE SHEET DENSITY lb/ft3 DENSITY lb/gal SpGr at 60° F Issue No.: Description Made/Revised by Checked by Approved Process Approved by Date SpGr EXPANSION AT FLOW COEFFICIENT TEMPERATURE 1 Date 3 Date CHEMICAL MOL. MW LINE SIZE PRESS. FORMULA DROP/100 ft 2 EST. LINE LENGTH 4 LINE PRESS DROP Date Date LINE LINE ORIGIN TERMINATION 5 Elsevier US Job Code:CAPA Fonts used:Times & Universal 55 family Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:793 Text Width:41p6 Trimsize:8.5 in×11 in 793 Depth:65 Lines Job No.: Job Name: Document No. Project No. Client Location Plant NUMBER MATERIAL A.K.C. TECHNOLOGY FROM TO LINE SUMMARY TABLE TITLE: Fonts used:Times & Universal 55 family of Issue No.: Description Made/Revised by Checked by Approved Process Approved LINE SIZE OPERATING OPERATING TEMP. PRESS. °F psig Sheet TEST PRESS. psig lb/h 1 GPM at 60° F QUANTITY Date GPM (HOT) 2 CFS (HOT) Date VEL. fps 3 PRESSURE DROP PER 100 ft TOTAL psi psi Date REMARKS NO. Elsevier US Job Code:CAPA Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:794 Text Width:41p6 Trimsize:8.5 in×11 in 794 Depth:65 Lines Fonts used:Times & Universal 55 family 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 Notes: 43 44 45 46 47 48 kg mol/h BALANCE MOL WT MASS Mol % kg mol/h of Mol % Sheet kg mol/h Mol % Issue No.: Description Made/Revised by Checked by Approved Process Approved kg mol/h Mol % 1 kg mol/h Date Mol % 2 kg mol/h Date Mol % 3 kg mol/h Date Mol % Job Code:CAPA STREAM NAME PHASE TEMPERATURE (° C) COMPONENT Water Hydrogen Nitrogen Carbon monoxide Carbon dioxide Methane Acetylene Ethylene Ethane Propyne Propadiene Propylene Propane Isobutane Isobutene n -Butane 1-Butene 1,3-Butadiene 1-Pentene neo-Pentane Isopentane n -Pentane Toluene m -Xylene Methanol MTBE TBA DIISO TOTAL (kg mol/h) STREAM NUMBER Job No.: Job Name: Document No. Project No. Client Location Plant A.K.C. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:795 Text Width:41p6 Trimsize:8.5 in×11 in 795 Depth:65 Lines CAPACITY PRESSURE (m3/h) (Turbine - Te/h) IN OUT (kg/cm2g) Issue No.: Description Made/ Revised by Checked by Approved Process Approved INLET TEMP. (° C) 1 NPSHA (m) Date TYPE (see Note 1) 2 MATERIALS Date Date ABSOLUTE SPEED (RPM)/ REMARKS POWER (kW) 3 Job Code:CAPA Fonts used:Times & Universal 55 family Notes: 1. Rotary Equipment Type Coding: A = Axial; C = Centrifugal; M = Metering; R = Reciprocating; S = Screw 2. All drives electric motor unless specified otherwise. FLUID S.G/M.W OFF SERVICE DESCRIPTION ITEM No. No. Sheet of MECHANICAL EQUIPMENT SCHEDULE Job No.: Job Name: Document No. Project No. Client Location Plant A.K.C. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:796 Text Width:41p6 Trimsize:8.5 in×11 in 796 Depth:65 Lines A.K.C. TECHNOLOGY FROM PIPE LINE LIST TITLE: TO TEMPERATURE (° F) OPERATING DESIGN Sheet of PRESSURE (psig) OPERATING DESIGN VELOCITY ft/s Issue No.: Description Made/ Revised by Checked by Approved Process Approved PRESSURE/100 ft PD/100 ft 1 FLOW 1 Date P&ID NUMBER 2 Date 3 Date Job Code:CAPA Fonts used:Times & Universal 55 family Note: 1. Flow Units: G = gpm; C = acfm; P = lb/h Job No.: Job Name: Document No. Project No. Client Location Plant LINE NUMBER Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:797 Text Width:41p6 Trimsize:8.5 in×11 in 797 Depth:65 Lines FROM PIPE LIST TITLE: TO Fonts used:Times & Universal 55 family TEMPERATURE (° F) OPERATING DESIGN Sheet of PRESSURE (psig) OPERATING DESIGN VELOCITY ft/s Issue No.: Description Made/Revised by Checked by Approved Process Approved PRESSURE/100 ft PD/100 ft 1 FLOW1 Date P&ID NUMBER 2 Date 3 Date Job Code:CAPA NOTE: 1. FLOW UNITS: G = gpm; C = acfm; P = lb/h Job No.: Job Name: Document No. Project No. Client Location Plant LINE NUMBER A.K.C. TECHNOLOGY Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:798 Text Width:41p6 Trimsize:8.5 in×11 in 798 Depth:65 Lines Fonts used:Times & Universal 55 family of FLUID SYMBOL Sheet Issue No.: Description Made/Revised by Checked by Approved Process Approved 1 Date 2 Date HAZARDOUS FLUID MAXIMUM CONTINUOUS PIPE NOTES MAXIMUM SPECIFICATION PIPE SIZE MATERIAL STATE RANGE OPERATING in. CLASSIFICATION LIQUID/GAS TEMPERATURE, ° F PRESSURE, psia PIPING PROCESS CONDITIONS SUMMARY Job No.: Job Name: Document No. Project No. Client Location Plant INDEX MATERIAL AND COMPOSITION NUMBER A.K.C. TECHNOLOGY 3 Date Elsevier US Job Code:CAPA Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:799 Text Width:41p6 Trimsize:8.5 in×11 in 799 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:800 800 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS PLATE HEAT EXCHANGER DATA SHEET A.K.C. TECHNOLOGY Job Item Name PROCESS DESIGN 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 UNITS Fluid Circulated Total Fluid Entering (Normal) Flow Margin Inlet Vapor and Gas (&MW) Inlet Liquid Fluid Vaporized/Condensed (&MW) Temperature In/Out Max. Pressure Drop Inlet Pressure (Operating) Normal Heat Load Heat Load Margin Fouling Resistance FLUID PROPERTIES Specific Heat Thermal Conductivity - kg/h % kg/h kg/h kg/h o C bar bar g kW % m2 ο C/W lb/h % lb/h lb/h lb/h o F psi psig Btu/h % ft 2 ο Fh/Btu kJ/kgοC cP cP kJ/kg Btu/lb οF ο Btu/hr ft F t3 lb/f lb/hr.ft lb/hr.ft Btu/lb bar g ο C mm in mm psig ο F in. in. in. W/m C kg/m3 Density Viscosity Liquid Viscosity (at Temp.) Latent Heat ENGINEERING DESIGN Process Design Pressure Process Design Temperature Corrosion Allowance (Header) Line N.B. In/Out Minimum Flow Passage Plate Material Frame Material Gasket Material Desgin Code FLUID 1 - ο Document No. Sheet of Item No.(s) No. Working Rev. Total No. Off FLUID 2 FLUID 3 3 Date NOTES 1. Unless otherwise stated fluid properties are for mean fluid temperatures. 2. Sour Service Yes / No 1 Date 2 Date Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:801 801 APPENDIX A Made Job No. Checked PROCESS DATA SHEET A.K.C. TECHNOLOGY Item No. Date Job Sheet of CALCULATION OF PRESSURE DROP IN FIXED CATALYST BEDS REQUIRED DATA VESSEL NO: SERVICE: CATALYST: GAS DATA: VOLUME REQUIRED MANUFACTURER & NO. DIMENSIONS EQUIV. PARTICLE DIA. SHAPE/SIZE FACTOR FLOW RATE MIN. MOLECULAR WEIGHT BED OUTLET PRESSURE MAX. BED TEMPERATURE ο ο ABS. TEMPERATURE ( K = C + 273) CALCULATION k1 = BED DIAMETER BED C.S.A. BED DEPTH SUPERFICIAL MASS FLOW MASS FLOW FACTOR DpG REYNOLDS NO. FACTOR k2 CLEAN PRESSURE DROP/UNIT DEPTH CLEAN OVERALL PRESSURE DROP SAFETY/FOULING FACTOR FLOW SHEET PRESSURE DROP SYMBOLS D A L G Gf Ref k2 ΔPc ΔPc f ΔP V ft3 Dp Sf ft. W W2 lb/h (lb/h)2 P psia ο C K T (T )(Sf ) = (M )(P ) UNITS ft 2 ft ft. 2 lb/h.ft psi/ft. psi psi = CALCULATION 0.7854D V/A W/A CASE 1 CASE 2 CASE 3 5 6 CASE 4 2 k1Ref k2Gf LΔPc 1.25/ fΔPc * IF VALUE OF DpG > 200 (750 FOR RING CATALYSTS) PUT Ref = 1.0 IF VALUE OF DpG < 200 (750 FOR RING CATALYSTS) CALCULATE Re = DpG/ μ (WHERE μ = DYNAMIC VISCOSITY OF GAS, lb/ft.hr) 1 2 3 4 Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Page:802 Trimsize:8.5 in×11 in 802 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS PROCESS ENGINEERING JOB ANALYSIS SUMMARY A.K.C. TECHNOLOGY Job Title Job No. Charge No. Date Based Upon Cost Estimated Dated or Actual Construction Cost Summary Prepared By Information Dated Production Basis (lb/day, tonnes/day, lb/month) SERVICE REQUIREMENTS: UNIT RATE 1 Steam (30 lb) lb/h 2 Steam (150 lb) lb/h 3 Steam (400 lb) lb/h 4 Steam ( lb) lb/h 5 Treated R.W. gpm 6 Untreated R.W. gpm 7 Fresh Water gpm 8 Sea Water gpm 9 Fuel Gas ( psi) cfm (60° F and 1atm) 10 Air ( psi) cfm (60° F and 1atm) 11 Power ( 12 Horsepower 13 Condensate lb/h RAW MATERIALS UNIT RATE UNIT RATE/ PRODUCTION BASIS ) 14 1 Chlorine 2 Hydrogen ( %) 3 Caustic ( %) 4 Salt 5 Sat. Brine 6 Natural Gas 7 Air 8 Ethylene 9 10 11 PRODUCTS AND BY- PRODUCTS 1 Chlorine 2 HCl ( %) 3 Salt ( %) 4 Caustic ( %) 5 Ammonia ( %) 6 H2SO4 ( %) 7 Gas ( UNIT RATE ) 8 9 10 11 Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:803 APPENDIX A PUMP CALCULATION SHEET A.K.C. TECHNOLOGY Document No. Sheet of Item No. (s) No. Working Job Item Name. UNITS CASE I CASE II + 803 Rev. Total No. off SKETCH OF PUMP HOOK-UP 1 2 Liquid Pumped 3 Corrosion/Erosion 4 Due To 5 6 7 8 9 Operating Temp. (T ) Specific Gravity at T Viscosity Vapor Pressure at T Normal mass Flowrate °C °F cP bara kg/h cP psia lb/h gpm 3 10 Normal Vol. Flowrate 11 Min. Vol. Flowrate m /h 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 Design Vol. Flowrate m3/h SUCTION CONDITION Pressure at Equipment barg Static Head bar Total – Lines 14 + 15 bar Suction Line bar ΔP ΔP Filter/Strainer bar gpm psig psi psi psi psi + +/– + – – + – – Total Suction Pressure barg DISCHARGE CONDITION Pressure at Equipment barg Static Head bar psig + + psig psi + +/– + +/– 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 Exchanger ΔP bar psi + + Furnace Orifice Control Valve ΔP ΔP bar bar bar psi psi psi + + + + + + Line ΔP bar psi + + Total Discharge Press. Differential Pressure Differential Head NPSH barg bar bar psig psi psi + + Total Suction Pressure Vapor Pressure NPSH – Lines 37 – 38 = Safety Margin NPSH – Lines 40–41 Hydraulic Power Estimated Efficiency Estimated Abs. Power Type of Pump Drive bara bara bara m m m kW % kW psia psia psia ft ft ft Hp % Hp NOTES 1. Pump shut-off head not to exceed……… 2. Relief valve on pump discharge to be set at …………… 3. Pump case design pressure………… design temperature…….. 4. Sealing/flushing fluid available: 5. Cooling medium available: 6. Insulation required: Material – Casing – Impeller – Shaft 7. Start-up/commissioning fluid SG. Sour Service 54 HEAD 55 VOLUME 56 57 58 59 60 61 62 ΔP Yes/No m = 10 × kg/cm 2/SG m = 10.2 × bar/SG 3 m /h × SG × 1000 = kg/h POWER 3 ft = 2.31 × psi/SG igpm × SG × 600 = lb/h kW = m /h × bar/36.0 1 Date 3 2 kW = m /h × kg/cm /36.71 2 Date Hp = igpm × psi/1427 3 Date 4 Date 5 Date Description Made/Revised by Checked by Approved Process Approved Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines A.K.C. Fonts used:Times & Universal 55 family ft3/h psig psig psi/ft ft. hp - m3/h bar g bar g bar /m m kW - 11 12 13 14 15 16 Margins:Top:3p6 Gutter:4p6 34 Seal / Flush Fluid 35 Quench 36 Notes 37 38 39 40 41 42 43 44 45 Services / Utilities Cooling Water Material: Casing Impeller Shaft Sour Service Packing Type / Mechanical Seal Type hp ft3/h ft3/h hp hp hp psi - Issue No.: Description Made/Revised by Checked by Approved- Process Approved 1 Date 2 Date 3 Date 22-12-2006 m3/h m3/h kW kW kW bar 20 21 22 23 24 25 26 27 28 29 30 31 32 33 Type of Driver Driver Rated Power ( per pump) Design Power Consumption ( per pump) Normal Power Consumption (per pump) Max. Shut-Off Head kW 18 Estimated Pump Efficieny 19 Estimated Shaft Power ( per pump) 17 R.P.M Sheet of Chapter:0capaappA - ft3/h m3/h 10 Design Capacity (per pump) Normal Capacity (per pump) Discharge Pressure Suction Pressure Differential Head Minimum NPSH Available / Required Hydraulic Power (per pump) F ο lb/ft.h psia Units cP bara 6 7 8 9 ο PUMP SCHEDULE Job Code:CAPA C Operating - Temperature Specific Gravity at Operationg Temperature Viscosity at Operating Temperature Vapor Pressure at Operating Temperature 1 2 3 4 5 TECHNOLOGY Job No.: Job Name: Document No. Project No. Client Location Plant Item Number. Item Name Number Off: No. Running /Total Installed Preferred Type Liquid Pumped Elsevier US 5:26 p.m. Font Size:9/10 pt Page:804 Text Width:41p6 Trimsize:8.5 in×11 in 804 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:805 APPENDIX A DOCUMENT / ITEM REFERENCE RELIEF DEVICE PHILOSOPHY SHEET A.K.C. TECHNOLOGY 805 EQUIPMENT No.: SHEET No.: DATE: CHECKED BY: OF 1 MADE BY: 2 DESIGN CODES: VESSELS LINES EXCHANGERS 3 4 OTHER REQUIREMENTS 5 6 BASIS FOR CALCULATION: 7 8 SET PRESSURE, PSIG: (a) BEFORE RELIEVING MAX. BACK PRESSURE: (b) WHILE RELIEVING 9 Calculated 10 NORMAL CONDITIONS UNDER RELIEF DEVICE: STATE: TEMPERATURE, °F: PRESSURE, PSIG: POSSIBLE FLUID RELIEF ORIFICE CAUSE? RELIEVED RATE, lb/h AREA, in2. 11 12 HAZARDS CONSIDERED 13 1. Outlets blocked 14 2. Control Valve malfunction 15 3. Machine trip/ overspeed/density change 16 4. Exchanger tube rupture 17 5. Power failure/ Voltage dip 18 6. Instrument air failure 19 7. Cooling failure 20 8. Reflux failure 21 9. Abnormal entry of volatile liquid 22 10 . Loss of liquid level 23 11. Abnormal chemical reaction 24 12. Boxed in thermal expansion 25 13. External fire 26 14. (specify) 27 15. (specify) 28 16. (specifty) 29 SELECTED DESIGN CASE: 30 31 RELIEVED FLUID: STATE DENSITY / MW: TEMPERATURE: COMPOSITION: RELIEF RATE REQUIRED, lb/h: AREA, in2: ORIFICE SELECTED: Cp/Cv: 32 FLASHING: 33 TYPE: 34 ACTUAL CAPACITY, lb/h 35 REMARKS/SKETCH 36 37 38 39 40 41 42 43 44 45 Issue No: 1 Date 2 Date 3 Date 46 Description 47 Made/Revised by 48 Checked by 49 Approved- Process 50 Approved 51 Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Page:806 Trimsize:8.5 in×11 in 806 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS TANK AND VESSEL AGITATOR DATA SHEET Project Name: PROCESS MIXING IMPELLER TANK OR VESSEL GENERAL ELEC T. DESI GN DEPT . INFORMATION Drawing No: Project No.: sheet …….. Of …….. Associated Vessel/Tank* Item No: Equipment No: No. Off: 1. Largest and smallest charge: 2. Components added during mixing: 3. Agitator operating while vessel is being filled or product withdrawn? Yes/No* 4. If continuous, throughput per hour: 5. Process duty: Mixing liquids/Dissolving/Suspensions/Emulsions/Gas absorption/Homogenisation* 6. Mixing effect: Violent/Medium/Moderate* Time available for mixing: 7. Working Pressure: Design Pressure: 8. Working Temperature: Design Temperature: 9. Special Remarks: 10. Components % by weight: Approved Approved Process Checked by Made/Revised by Description 1 Da te 2 Da te PROCESS DEPT. INFORMATION 3 Da te A.K.C. TECHNOLOGY 11. 12. 13. 14. 15. 16. Temperature during mixing: Specific gravity of components: Viscosity of mixing at mixing temperature: Specific gravity of product at mixing temperature: Size of solid particles: Special Remarks: 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. Type of impeller: Number of impellers on shaft: Position of impellers: Distance between shaft end & vessel: Preferred impeller speed: Type of drive: Direct/Vee belt/Fluid* Type of seal: Vapor/Packed gland/Mechanical/Easy replacement* Method of installation: Assembled in/Assembled out* of vessel Entry position: Materials of construction: Bottom bearing: Shaft diameter: 27. Absorbed HP/KW*: 28. Other information: Installed HP/KW*: 29. 30. 31. 32. 33. 34. Capacity: Dimensions: Coils, baffles, etc.: Fixing agitator (beams, flanges, etc.): If at atmospheric pressure: Closed/Open* Headroom available above agitator: Other information: Can stuffing box be greased? Yes/No* Motor enclosure: 35. Agitator installed: Indoors/Outdoors 36. Electrical specification: 37. Any other electrical information: 38. 39. 40. 41. 42. 43. 44. 45. Motor to be included: Yes/No* Motor Will/Will not* be sent to manufacturer for assembly and alignment. Threads: Unified /* All rotating parts must be strictly guarded to BS 1649/ASME Fixing bolts supplied by: Net weight including motor: Witnessed run in air: General notes: NOTE: * Indicates delete as necessary. Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:807 APPENDIX A TANK PROCESS DATA SHEET A.K.C. TECHNOLOGY Job: 807 Doc. No: Item No. Sheet of Item Name: NOTE: * indicates delete as necessary; ** indicates for other than Code reason 5 10 15 20 Issue No. Made/Revised by Checked by Approved - Process Approved by Fonts used:Times & Universal 55 family 1 Margins:Top:3p6 Date Gutter:4p6 2 Shell Length: No. Required: Nozzles Inlet Mark No. C- Vapor Out C- Liquid Out: C- Thermocouple Pressure Gauge Gauge Glass Level Control Safety Valve RRRRR- Vent Drain Steam Out CCC- Manhole A- min. Base Elev'n: Material: Date Size Number by Inst. Op. 25 26 Shell Diameter (O.D. / I.D.): 27 Center Line: *Horizontal / Vertical 28 Pressure: g Temperature: °F / °C 29 Item Number 30 Operating 31 Design 32 Emergency Vacuum Design: * Yes / No Material Corr. Allowance 33 34 Shell 35 Heads 36 Liner 37 Type of Heads 38 Code: 39 Stress Relieve**: Radiography**: 40 Joint Efficiency: * °F / °C at 41 Density of Contents: Weight Full: 42 Weight Empty: 43 Is vessel subject to mechanical vibration? *Yes / No Type: *Frost and Personnel Protection / Cold 44 insulation: Anticondensation / Heat Conservation 45 *Yes / No 46 REMARKS: 47 48 49 50 51 52 53 54 k-Skirt Length 3 Font Size:9/10 pt Date 4 Text Width:41p6 Date Depth:65 Lines 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 Fonts used:Times & Universal 55 family in. ft 3 ft 3 mm m3 m3 Total Volume Working Capacity Internals / Fittings Margins:Top:3p6 Gutter:4p6 in. Issue No.: Description Made/Revised by Checked by Approved- Process Approved 1 Date 2 Date 3 Date 22-12-2006 Notes Shell Corrosion Allowance Sour Service Stress Relieved for Process Reasons Insulation mm °F psig °F °C bar g °C Operating Temperature Design Pressure +/ - of Chapter:0capaappA Design Temperature Vacuum Design Material: Shell Liner Internals psig bar g Operating Pressure in. in. Sheet Job Code:CAPA mm mm Units TANK SCHEDULE Job No.: Job Name: Document No. Project No. Client Location Plant Item Number. Item Name Number Required Type Length x Width Height Diameter Minimum Base Elevation A.K.C. TECHNOLOGY Elsevier US 5:26 p.m. Font Size:9/10 pt Page:808 Text Width:41p6 Trimsize:8.5 in×11 in 808 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS Depth:65 Lines A.K.C. TECHNOLOGY SERVICE DESCRIPTION TIE-IN-SCHEDULE EXISTING LINE NUMBER of NEW LINE NUMBER Sheet EXISTING ELD* NUMBER NEW ELD* NUMBER Issue No.: Description Made/Revised by Checked by Approved Process Approved 1 REMARKS Date 2 Date 3 TIE-IN NUMBER Date Job Code:CAPA Fonts used:Times & Universal 55 family * ELD = ENGINEERING LINE DRAWING TIE-IN NUMBER Job No.: Job Name: Document No. Project No. Client Location Plant Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:809 Text Width:41p6 Trimsize:8.5 in×11 in 809 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:810 810 A LIST OF ENGINEERING PROCESS FLOW DIAGRAMS AND PROCESS DATA SHEETS Made by: Document No. TOWER PROCESS DATA SHEET A.K.C. TECHNOLOGY Date: Job Checked by: Item No:(s) Item Name Sheet of Tower Name: NOTE: * indicates delete as necessary; ** indicates for other than code reason Top Bottom Shell Diameters O.D. - I.D. No. of Trays Pressure Operating *psig Design Temperature Operating Design *oF / oC Material Shell Trays Caps Liner or Clad Corrosion Shell Allowance Heads Trays Tray Spacing Type of Liquid Flow Type of Trays Joint Efficiency Code Emergency Vac. Design *Yes / No Stress Relieved **Yes / No Radiography **Yes / No Is vessel subject to mechanical vibration *Yes / No Insulation Type: *Frost and Personnel Protection / Cold / *Yes / No /anticondensation / Heat Conservation / Min. Base Elevation: Skirt length: Weight Empty: Full: Nozzles Mark No. Size Number Feed COverhead Vpr. CReflux In CBottoms Reboiler Vpr Reboiler liq CCC- Thermocouple Level Glass Press Gauge Level Control Safety Valve RRRRR- Vent Drain Steam Out Manholes Handholes Cap Type: NOTES CCCAA- by inst. Gp. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 Tray Layout Ref: 1 Date 2 Date 3 Date 4 Date Description Made/Revised by Checked by Approved Process Approved by Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:811 APPENDIX A TRAY LOADING SUMMARY A.K.C. TECHNOLOGY Job: Tower Name: 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 Job No. item No. Sheet of Type of Tray Manufacturer Pressure at top of Tower Max. ΔP over Tower No. of Trays Tray location Tray Number* Tray Spacing Tower Internal Diameter I.D. Vapor to Tray Temperature Compressibility Density Molecular Weight Rate Liquid from Tray Temperature Surface Tension Viscosity Density Rate Foaming Tendency ** Number of Passes Minimum Hole Diameter *** Minimum DC Residence Time*** Maximum Rate as % Design Minimum Rate as % Design Design Rate % Flood Rate*** Tray Material Valve or Cap Material Corrosion Allowance Tray Thickness*** NOTES: 811 Mfr. Ref: barg bar psia psi Aboved Feed mm mm in. in. o o C kg/m units Used: METRIC/BRITISH (delete one) Below Feed F 3 lb/ft 3 kg/h lb/h °C dynes/cm cps kg/m3 kg/h °F lb/ft lb ft/hr lb/ft3 lb/h mm secs in. s mm mm in. in. * Trays are numbered from the bottom of the tower upwardstop of the tower downwards ** Indicate whether 'non', 'moderate', 'high' or 'severe' ∗ ∗ ∗ Data to be supplied by tray manufacturer unless special Process/Client requirement entered here. REMARKS: Fonts used:Times & Universal 55 family 1 Date 2 Date 3 Date Description Made/Revised by Checked by Approve - Process Approved by Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines A.K.C. Fonts used:Times & Universal 55 family 1 INITIATING VARIABLE Job No.: Job Name: Document No. Project No. Client Location Plant TECHNOLOGY 2 BASIC INST. No. 3 4 PRE- ALARM INST. No. SETTING TRIP SCHEDULE of 5 6 CUT OUT INST. No. SETTING Sheet 7 FIRST FAULT INDICATION Issue No. Decription Made/Revised by Checked by Approved Process Approved 8 INHIBIT SWITCH 1 9 TRIP LINKAGE Date 10 ITEM ACTUATED 2 11 PRIMARY PROCESS EFFECT Date 12 REMARKS Elsevier US Job Code:CAPA Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:812 Text Width:41p6 Trimsize:8.5 in×11 in 812 Depth:65 Lines A.K.C. TECHNOLOGY Fonts used:Times & Universal 55 family Source I is: NUMBER OFF Inst/d Work'g % Motor Efficiency UTILITY SUMMARY SHEET kW kW Electrical kW HT kW LT Total Consumption Electrical Issue No.: Description Made/Revised by Checked by Approved- Process Approved by Date 2 kg/h= T= kg/h= T= kg/h= T= STEAM/ CONDENSATE/ BOILER See Note 1 P= P= P= 1 kg/h= Condensate FEEDWATER Date kg/h= BFW 3 Flow m3/h Source Date kW ΔT °C Flow m3/h ΔT °C FUEL Date Absorbed 5 II Date COOLING WATER See Note 2 I Source 4 kW Fired 6 See Note 1 nm3/h P= COMPRESSED AIR Date REMARKS AND OTHER SERVICES Chapter:0capaappA Margins:Top:3p6 T is Source II is Electrical Shaft kW ELECTRICITY Per Machine Consumption Installed Sheet of Job Code:CAPA Note 1: State units - P is Note 2: Cooling water Job No.: Job Name: Document No. Project No. Client Location Plant Item No. Item Name Elsevier US 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:813 Text Width:41p6 Trimsize:8.5 in×11 in 813 Depth:65 Lines Job No.: Job Name: Document No. Project No. Client Location Plant ITEM No. No. UNITS A.K.C. TECHNOLOGY SERVICE DESCRIPTION VERTICAL OR HORIZONTAL VESSEL AND TANK SCHEDULE DIAMETER LENGTH Sheet of THICKNESS HEAD SHELL Issue No.: Description Made/Revised by Checked by Approved Process Approved LINING 1 INSULATION CODE Date Date WEIGHT 2 TEST PRESSURE, psig REFERENCE DRAWING 3 PURCHASE ORDER TO Date P.O. Number Elsevier US Job Code:CAPA Chapter:0capaappA Fonts used:Times & Universal 55 family Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:814 Text Width:41p6 Trimsize:8.5 in×11 in 814 Depth:65 Lines A.K.C. TECHNOLOGY Fonts used:Times & Universal 55 family O.D. HEIGHT GALLONS or LENGTH. CAPACITY AND TANK SUMMARY Driver Vessel and tank summary TYPE VESSEL Issue No.: Description Made/Revised by Checked by Approved- Process Approved 1 Date THICKNESS, INCHES CORROSION MATERIAL SADDLE SHELL HEAD SADDLE ALLOWANCE SHELL SKIRT SKIRT & HEADS INCHES SUPPORT SUPPORT Sheet of OPER'N 2 3 PRESSURE, PSIG DESIGN TEST Date 4 TEMP., °F OPER'N DESIGN Date CODE Date Date STAMP REFERENCE DRAWING No. 5 NOTES Job Code:CAPA Figure 1-38 ITEM No. EQUIPMENT Job No.: Job Name: Document No. Project No. Client Location Plant Elsevier US Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:815 Trimsize:8.5 in×11 in 815 Text Width:41p6 Depth:65 Lines Fonts used:Times & Universal 55 family Margins:Top:3p6 °F psig °F °C bar g °C 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 Gutter:4p6 1 Date 2 Date 3 Date 22-12-2006 Notes Shell Corrosion Allowance Sour Service Stress Relieved for Process Reasons Insulation in. psig bar g 15 Operating Temperature 16 Design Pressure Issue No.: Description Made/Revised by Checked by Approved- Process Approved Chapter:0capaappA mm in. in. mm mm Sheet of Job Code:CAPA Design Temperature Vacuum Design Material: Shell Liner Internals in. in. Units mm mm VESSEL SCHEDULE Job No.: Job Name: Document No. Project No. Client Location Plant 1 Item Number. 2 Item Name 3 Number Required 4 5 Shell Diameter (O.D/I.D.) 6 Shell Length 7 Center Line (H/V) 8 Boot Size 9 Base Elevation 10 Internals 11 12 13 14 Operating Pressure A.K.C. TECHNOLOGY Elsevier US 5:26 p.m. Font Size:9/10 pt Page:816 Text Width:41p6 Trimsize:8.5 in×11 in 816 Depth:65 Lines Elsevier US Job Code:CAPA Chapter:0capaappA 22-12-2006 5:26 p.m. Trimsize:8.5 in×11 in Page:817 APPENDIX A WATE R ANALYSIS SHEET A.K.C. TECHNOLOGY Submitted by: Address: 817 Location: Date: ** Analysis No. Date: pH Value Suspended Solids Total Dissolved Solids Total Dissolved Solids Alkalinity to Pp mg/l mg/l at 110° C mg/l at 180° C as mg/l CaCO3 Alkalinity to MO as mg/l CaCO3 Sulphate Chloride Nitrate as mg/l SO4 as mg/l Cl as mg/l NO3 Silica as mg/l SiO2 Phosphate as mg/l PO4 Total Anions as mg/l CaCO3 Total Hardness Calcium Magnesium Sodium* Potassium* Iron Manganese Free and Saline Ammonia as mg/l CaCO3 as mg/l Ca as mg/l Mg as mg/l Na as mg/l K as mg/l Fe as mg/l Mn as mg/l NH3 Total Cations Free Dissolved CO2 as mg/l CO2 Dissolved O2 Color Hazaen Units Turbidity Formazin Units+ Lead Copper Residual Chlorine Flouride Sulfite as mg/l CaCO3 as mg/l O FTU APHA as mg/l Pb as mg/l Cu as mg/l F as mg/l SO3 NOTES: 1. Please state if units other than milligrams per liter, or different conditions of test, are used. 2. * If Na and/or K form an appreciable amount of total cations, please state Alkalinity to Phenolphthalein (p), Alkalinity to Methyl Orange (MO), and Carbonate Hardness. 3. + DO NOT use Formazin Units as defined by British Standard BS. 2690 Pt. 9. 4. ** Tick if item definitely to be included in analysis. 5. 100 mg/L CaCO3 = 2 milliequivalents/(m val/L). Fonts used:Times & Universal 55 family Margins:Top:3p6 Gutter:4p6 Font Size:9/10 pt Text Width:41p6 Depth:65 Lines Elsevier US Job Code:CAPA Fonts used:Times & Universal 55 family Chapter:0capaappA Margins:Top:3p6 22-12-2006 Gutter:4p6 5:26 p.m. Font Size:9/10 pt Page:818 Text Width:41p6 Trimsize:8.5 in×11 in Depth:65 Lines