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Chemistry Updates and Scientific Endeavors
Vol 11, Winter 2014
Chair’s letter
To all our Chemistry friends
and alumnae,
New Year’s greetings from snowcovered Syracuse, and welcome to
the latest edition of the Chemistry
department newsletter. The end of
the fall semester coincided with the
season’s first major snowstorm, and
the campus is blanketed in white:
beautiful to behold, even if it is a
bit treacherous to navigate! For this
issue, it’s my pleasure to serve as
the stand-in for our chair, Prof. Karin
Ruhlandt, currently on sabbatical
leave as a Fulbright Fellow in Graz,
Austria. Prof. Ruhlandt has spent an
exciting semester abroad, teaching a
course, giving seminars and exploring
new research areas. Later this month
she will be traveling to Italy to spend
a week collecting data at the Elletra
Syncrotrone Trieste international
research facility. Prof. Ruhlandt will be
returning to Syracuse in late February
to resume her leadership of the
Chemistry department.
2013 has been a rewarding and
productive year for Chemistry faculty and
students. The month of May brought with
it the end of the academic year and our
annual departmental awards ceremony,
in which we celebrate the outstanding
performances of our undergraduates.
It’s always a bittersweet time for the
faculty, because we must say goodbye
to another class of talented seniors. This
year’s senior class was extraordinarily
accomplished, and included senior
class marshal and valedictorian, Jaime
Bernstein (’13). Jaime and her fellow
Syracuse Scholar, Anna Kahkoska
(’13), are long time members of
Prof. Robert Doyle’s research group;
both began their studies in medical
school this year. Read all about the
accomplishments of our amazing
undergraduate and graduate students
elsewhere in this issue!
Not to be outdone by their students,
our award-winning faculty has
continued to receive University
and national recognition for their
outstanding research and teaching
accomplishments. Among our
prominent faculty in 2013 were Prof.
Ivan Korendovych, recipient of a Ralph
E. Powe Junior Faculty Enhancement
award and Prof. James Spencer,
recognized with a Chancellor’s Citation
for Excellence.
The end of summer found our
department welcoming a class of 21
incoming graduate students from
all over the globe. We celebrated
their arrival and the completion of a
grueling week of breadth exams with
our traditional opening week lunch
in the Life Science Complex atrium.
Joining us for the event were alumnae
Dr. Philip Pivawer (G ‘60) and Prof.
Terry Morrill (‘61). Members of the
Bowne Hall generation of Syracuse
chemists, Phil and Terry received
personal tours of our new teaching and
research facilities in the Life Sciences
Center, including an up-close look at
the installation of the department’s
new 400 MHz NMR spectrometer that
arrived from Bruker in late August. On
the subject of spectrometers, we’ve
recently learned that a consortium
of institutions, including Syracuse
University, Upstate Medical Center and
the SUNY College of Environmental
Sciences and Forestry, has been
awarded NIH funding for an ultra highfield NMR instrument. At the time of
this writing, Prof. Phil Borer is visiting
the Bruker facility in Switzerland, to
kick the tires on a new 800 MHz NMR
spectrometer. Stay tuned for more
on this exciting development in the
months ahead!
In other news, the department’s
longstanding history of research into
the chemistry of pharmacologically
active compounds is one step closer
to a new phase with the College’s
approval of our Bachelor of Science
program in Medicinal Chemistry.
Scheduled for launch in the 20142015 academic year, this new course
of study will provide students with
training in the principles of both
chemistry and the biological sciences,
enabling them to understand the
design, evaluation and implementation
of pharmacologically relevant small
molecules and biologics. Students
in the Medicinal Chemistry program
will be assisted in their studies by the
addition of new upper division and
graduate level courses and access to
new, state-of-the-art instrumentation.
Our existing 300 MHz Bruker
instrument has been extensively
upgraded and will be dedicated
exclusively to teaching activities,
providing students in our organic,
physical and medicinal chemistry labs
with access to high-field, multi-nuclear
NMR technology. Two Agilent liquid
continued on next page
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UNDERGRADUATE ACHIEVEMENTS
Jaime Bernstein ’13 (chemistry) and Anna Kahkoska ’13
(biochemistry), students working in Robert Doyle’s lab, were
named as 2013 Syracuse University Scholars, the highest
undergraduate academic honor bestowed at the University.
Additionally, Bernstein, a dual chemistry and Spanish major,
delivered the student address at the 2013 Syracuse University/
SUNY ESF Commencement (see www.news.syr.edu/speakingof-syracuse-university-25131). Kahkoska, a biochemistry
senior working for Rob Doyle, was awarded Capstone Honors
Thesis of the Year for Science and Engineering at the Honors
Convocation.
Korrie Mack ’13, a biochemistry student working in Ivan
Korendovych’s lab in collaboration with Karin Ruhlandt, has
been awarded an NSF Graduate Research Fellowship for work
that she began this fall in the biochemistry and molecular
biophysics Ph.D. program at the University of Pennsylvania.
For her research at SU, Mack won the 2013 Norma Slepecky
Undergraduate Research Prize, as well as 2012 Beckman
Scholar Award. (More about her work can be seen in the online
article “From proteins to biosensors” http://asnews.syr.edu/
newsevents_2012/releases/2012_Beckman_Scholars_
SU.html.
Leann Miles ’14 and Allison Roberts ’14, biochemistry
majors, were two of the 35 students chosen as Remembrance
Scholars for 2013-14.
Kristopher Murray ’14, a biochemistry student, is an American
Chemical Society Scholar.
GRADUATE STUDENT ACHIEVEMENTS
Wenjie Wu, a chemistry graduate student working in Mathew
Maye’s lab, won the IPMI Colt Refining Student Award, an
international award from the International Precious Metal
Institute (IPMI). This award is given to a top graduate student
who uses precious metals in research that has direct
applications in industry.
Colleen Alexander, G’13, received the Division of Inorganic
Chemistry ACS Young Investigator Award for her work on the use
of gold nanoparticles for drug delivery in cancer chemotherapy.
Alexander presented her research findings at the Young
Investigator Symposium at the National American Chemical
Society meeting held in Indianapolis this fall. Mathew Maye and
James Dabrowiak were co-advisors on her research project.
Alexander also received the Sabin Metal Student Award from
the International Precious Metals Institute.
continued from cover
chromatography–mass spectrometry
systems, donated to the department
by Eli Lilly and Company through the
dedicated efforts of Dr. Jim Grace
(‘89), will be incorporated into the
laboratories of organic, biochemistry
and forensics courses next year.
There was some sad news in 2013,
as we bid farewell to two long time
members of our departmental
family. Professor Thomas Walnut,
a theoretical chemist and a member
of the Syracuse University faculty
for almost 40 years, passed away
in late September. And just before
Thanksgiving, we were saddened to
learn that Prof. Donald Dittmer died
Peter J. Rosado Flores, a fifth-year graduate student, received
a First Place honor for his presentation at the Emerging
Researchers National Conference in Science, Technology,
Engineering and Mathematics in Washington, D.C.
Susan Flynn was one of eight recipients nationally who
received a travel grant from Eli Lilly and the Women Chemists
Committee (WCC) to attend the American Chemical Society
meeting in Indianapolis. Flynn presented within her division and
at the awardee poster session and was recognized at the WCC
luncheon.
Joseph Darling, a third-year chemistry graduate student
working in James Hougland’s lab, has received a National
Science Foundation Graduate Research Fellowship.
at his home in Syracuse. Both Tom
and Don were emeritus professors
who stayed scientifically active well
into retirement and remained involved
in departmental activities until their
last days. We will remember them as
consummate scientists, our teachers
and mentors, our colleagues and our
friends.
The coming new year promises to be
an exciting time at Syracuse University,
as we prepare to welcome Syracuse
University’s 12th chancellor, Kent D.
Syverud, and, later in 2014, a new
Dean of the College. An ongoing search
for a new biochemistry faculty member,
jointly appointed between Chemistry
and Biology, promises to continue to
build the scholarly bridge between our
two disciplines. I hope that each of
you will keep us updated on events in
your lives and careers, and should the
occasion present itself, drop in and
see first hand what’s happening in the
department! On behalf of the faculty,
staff and students of Chemistry, I wish
each and every one of you all the very
best in the coming new year,
Warm regards,
Jim Kallmerten
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Alumni Corner
Preeti Sejwal G’08 received
her B.S. and M.S. in chemistry
at Delhi University, India,
and enrolled at Syracuse
University for her doctoral
studies. She graduated with
a Ph.D. in chemistry under
the supervision of Professor
Yan-Yeung Luk. While in the
Ph.D. program, she pursued
summer internships at BristolMyers Squibb in Syracuse
and worked in the bioprocess
and bioanalytical division.
Utilizing her expertise working
at the interface of biology
and chemistry, gained during
her Ph.D. studies, she made
significant improvement in the
existing analytical methods
at Bristol. Subsequently she
was offered a full-time position
as a bioanalytical scientist at
Bristol.
In 2010 she moved to Bristol’s
facility in Princeton, New
Jersey, and joined a discovery
analytical group as a research
investigator I. She provided
analytical expertise to support
multiple projects spanning
across small, ‘milla,’ and
large molecules, resulting in
recognition and awards, and
was promoted to research
investigator II. Recently
she accepted a senior
analytical scientist position
at AbbVie, a research-based
pharmaceuticals company in
North Chicago, Illinois. In this
capacity she is working as a
core analytical team member
to support clinical and
commercial manufacturing of
drug products.
She and her husband have
settled in Chicago and
welcomed a baby girl earlier
this year named Arya.
Where they are now . . .
Diane O’Connor G’77,
who received her M.S.,
is vice president for
environment, health, safety,
and sustainability at Xerox
Corporation, where she has
worked since 1977.
Daniel Zaleski ’08 received
his Ph.D. in chemistry from
the University of Virginia
and is a postdoctoral fellow
at Newcastle University in
England.
Patrick Carberry G’09,
who received his Ph.D., is
an assistant professor at
Columbia University Medical
Center.
Nerissa Villegas G’09,
who received her Ph.D., is a
research scholar at Memorial
Sloan-Kettering Cancer Center
in New York City.
Debjyoti Bandyopadhyay
G’11, who received his Ph.D.,
is a postdoctoral researcher
at the School of Chemistry
and Biochemistry at Georgia
Institute of Technology.
Adam Lau, a Research
Experience for Undergraduates
intern in 2011, is pursuing
an M.S. in mechanical
engineering at California State
University, Sacramento.
Laura Bateman G’12, who
received her Ph.D., is a Hazard
Review Specialist at UL
(Underwriter Laboratories).
Kari Darling G’12, who
received her Ph.D., is
an Advanced Placement
Chemistry teacher in
Massachusetts.
Congratulations
to all of our recent
Ph.D. recipients:
Christopher Fazen G’12,
who received his Ph.D., is
a postdoctoral research
associate at Princeton
University’s Department
of Chemical and Biological
Engineering.
Susan James G’12, who
received her Ph.D., is a
postdoctoral research fellow at
Harvard Medical School.
Yi Shi G’12, who received
her Ph.D., is a postdoctoral
researcher at the University of
North Texas Health Science
Center.
Debbie Valentin G’12, who
received her Ph.D., served an
internship in global regulatory
affairs for Bayer HealthCare
before becoming a regulatory
affairs specialist in medical
devices and diagnostics at
Johnson & Johnson.
Fall 2012: Laura Bateman, Kari Darling,
Susan James, Yi Shi, Dennis Viernes
Spring 2013: Sijie Yang
Summer 2013: Rebeka Alam, Colleen
Alexander, Pei Ma, Burkhardt Wilke,
Wenjie Wu, Joshua Zylstra
Dennis Viernes G’12, who
received his Ph.D., is a
postdoctoral researcher at
Syracuse University.
Rebeka Alam G’13, who
received her Ph.D., is a
postdoctoral researcher at
Notre Dame University.
Colleen Alexander G’13,
who received her Ph.D., is a
postdoctoral researcher at the
University of Massachusetts,
Amherst.
Wenjie Wu, G’13, who
received her Ph.D., is a
postdoctoral researcher at the
University of California, Davis.
Receiving their master’s degree:
Gregory Ganci, Rosemary Loftus,
Yi Luo, Luke Nye, Lu Yu
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INSTRUMENTATION ENHANCEMENTS FOR RESEARCH
AND TEACHING:
A major focus of the chemistry department’s planning for the future has been to greatly
expand our shared major instrumentation, for both research and teaching needs. In 2013
it has been particularly exciting to see a trio of news items that indicate these efforts are
bearing a bumper crop of fruit.
1. NIH Funding for 800MHz NMR awarded.
In September 2013, the National
Institutes of Health awarded a $2 million
grant to acquire a new 800 MHz nuclear
magnetic resonance spectrometer to
serve biomedical scientists in Upstate
New York. Syracuse University is one
of six universities in the consortium,
including SUNY Upstate Medical
University, SUNY College of Environmental
Science and Forestry (ESF), Cornell
University, University of Rochester, and
SUNY Buffalo. The new instrument will
be operational toward the end of 2014
and will be located on the ESF campus,
a short walk from SU. The instrument will
be the only one of its kind in Central and
Western New York, filling a void in the
region’s research infrastructure.
Professor Phil Borer in the chemistry
department worked to write the grant
with Principal Investigator Professor
Stephan Wilkens of SUNY Upstate.
Borer anticipates that the instrument
will be utilized mainly to determine the
structures of proteins, nucleic acids, and
their complexes with drugs and small
molecules. “An 800 makes it practical to
determine structures for molecules with
molecular weights of 30,000 (30 kDa),”
Borer said. “It is often hard to crystallize
interesting biomolecules for X-ray studies.
Also, NMR allows us to measure the rates
and amplitudes of motion that are critical
to understanding dynamic systems. The
new 800 will allow us to attack problems
that would be impossible on our existing
spectrometers and reduce acquisition
times from days to hours for many
studies.”
Two vendors offer 800 MHz NMR
systems, Bruker and Agilent, and
evaluation visits took place in December
and January. Profs. Borer and Wilkens,
and David Kiemle traveled to Switzerland
(Bruker) and Santa Clara, CA (Agilent).
Borer and Dr. Deborah Kerwood,
manager of SU NMR facility sent a
sample of a DNA aptamer that binds
tightly to the HIV-1 nucleocapsid protein;
Wilkens sent a protein from the vacuolar
ATPase; and Prof. Frank Schroeder
(Cornell) sent a complex mixture of
small molecules isolated from insects.
These are a few from the wide range of
problems that can be attacked using the
new instrument.
The new 400-Hz instrument has a
liquid-N2 cryoprobe optimized for 13C,
with the capability to observe 1H, 19F,
and other nuclei in the frequency range
from 15N to 31P. A room-temperature
probe covers the same set of nuclei but
with a wider temperature range. There is
a 60-sample changer, automated tuning
and matching, and z-axis pulsed field
gradients on each probe.
After the 300-MHz upgrade, only 1H and
13C are available on that instrument.
However, it is now equipped with a
16-sample changer and the same
software as on the 400-MHz instrument.
This allows for a much higher throughput
of samples and allows this instrument to
be used more effectively in the teaching
laboratories, including second-year
organic chemistry lab (CHE 276/326).
2. 400-MHz NMR installed. 3. Donated LC-Mass
spectrometers for teaching
In last year’s newsletter, we reported
and research.
that the department received funding
from the National Science Foundation
to purchase a new 400-MHz NMR
instrument with a liquid nitrogen
cryoprobe that will provide state-of-theart NMR technology, especially useful for
organic, inorganic, and physical chemists.
Funds were also included to upgrade
the existing Bruker 300-MHz instrument
with a new console, probe, and sample
changer and make it available for
the teaching laboratories as well as
an overflow instrument. Delivery and
installation of the 400-MHz instrument
was completed in August 2013, and
shortly thereafter the upgrades to the
300-MHz were completed.
We are grateful to Eli Lilly Corporation
for the generous donation of two Agilent
LC-MS instruments in summer 2013.
These instruments are capable of
both electrospray ionization (ESI) and
atmospheric pressure chemical ionization
(APCI), equipped with quadrupole
detectors, and carried a combined
original purchase price of more than
$100,000. In arranging this donation, the
role of Jim Grace, who received his B.S. in
chemistry from our department in 1989
and a Ph.D. from the University of Virginia
and has been at Eli Lilly since the mid
2000s, was instrumental.
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These LC-MS spectrometers will be
used primarily for teaching. One of
them is located in the organic teaching
laboratory (CHE 326) and one in a shared
instrument room immediately next to the
analytical teaching laboratory (CHE 335,
CHE/FSC 444). Since fall 2012, the CHE
335 course has been making use of a
different shared departmental LC-MS
to carry out one of the experiments,
designed by Professor Mark Braiman,
with substantial guidance from Professor
Rob Doyle, to analyze chymotryptic
fragments of insulin. The donated
instruments are immediately applicable
for helping our undergraduate students to
learn to perform powerful modern LC-MS
analysis.
Elements of Success
The department appreciates
contributions of any amount. However,
we provide special recognition of
donations of $5000 and above by
dedicating elements in our Periodic
Table display case to such supporters.
(A listing of the elements dedicated
so far is available on our department
website, at chemistry.syr.edu/
elementwall).
The College of Arts & Sciences Office
of Advancement is taking steps to
simplify making departmentally
targeted contributions. In particular,
such donations can now be accepted
at https://secure.syr.edu/giving/
thecollege_giving.aspx (select
“Chemistry” from the drop-down box).
Please consider making a year-end taxdeductible donation to the chemistry
department via this website.
OUR DEPARTMENT IN THE NEWS
Rob Doyle: Fighting Obesity (http://news.syr.edu/chemist-to- Mathew Maye: Stainless Nanoparticles(http://news.syr.
study-orally-effective-therapy-to-fight-obesity-66659/)
edu/su-chemists-develop-fresh-new-approach-to-makingalloy-nanomaterials-34372/)
Mathew Maye: ‘Smart’ Nanoparticles (http://news.syr.
edu/chemists-design-smart-nanoparticles-to-improve-drugdelivery-dna-self-assembly-11734/)
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2013 DEPARTMENT OF CHEMISTRY AWARDS
Gershon Vincow Award for
Excellence in General Chemistry
Susannah Oberly, Jianing Xu, Michael
Cruikshank
Department Award for Exceptional
Performance in Honors Chemistry
Tyler Smith
Department Award for Exceptional
Performance in Analytical Chemistry
Amiya Quidley
George Wiley Award for Exceptional
Performance in Organic Chemistry
Daniel Nguyen and Chan Nguyen
Department Award for Exceptional
Performance in Inorganic Chemistry
Jaime Bernstein
Willem Prins Award for Exceptional
Performance in Physical Chemistry
Shannon Walter and Shane Stone
Department Award for Exceptional
Performance in Biochemistry
Anna Kahkoska
Birge Award for Exceptional
Performance in Biochemistry Research:
Korrie Mack
Clayton Spencer Award for Exceptional
Performance in Undergraduate Research,
Sponsored by Alpha Chi Sigma:
Jaime Bernstein
Department Award for
Overall Excellence in Chemistry
Jaime Bernstein
William D. Johnson Award for
Outstanding Graduate Teaching Assistant
Susan Flynn
Welcome New
Students
The department welcomes:
Michelle (Mickie) Takacs, Harvey
Mosher, Elyse Kleist, Steven Ortiz,
Jayme Workinger, Tiffany Greenfield, Liz
Cleverdon, Yue Wu, Ricky McDonough,
Jay Tinklepaugh, Nivedita Mahajani,
Zsofia Lengyel, Peter McLaughlin,
Amanda Chan, Alex Dixon, Michael
Clark, Emily Carpenter, Patrick Heaphy,
Laxmikant (LP) Pathade, Hewen (Jung)
Zheng (missing from picture: Mercy Alila)
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FACULTY achievements
Ivan Korendovych was one of only 30 junior
faculty nationwide to receive a Ralph E.
Powe Junior Faculty Enhancement Award.
The award administered by Oak Ridge
Associated Universities supports innovative
research across all disciplines in science
and engineering.
Mathew Maye received a Meredith
Teaching Recognition Award in spring 2013
along with six other faculty members at the
University. Dr. Maye has a very innovative
approach to teaching both undergraduate
and graduate students.Mathew Maye also
received the Young Technologist of the
Year Award from the Technology Alliance of
Central New York.
Robert Doyle received the College
Technology Educator of the Year award from
the Technology Alliance of Central New York.
Jon Zubieta received the 2013 College of
Arts and Sciences Wasserstrom Prize Award.
The prize, in memory of English Professor
William Wasserstrom, is awarded to a faculty
member in the College of Arts and Sciences
who exemplifies outstanding success
teaching graduate students.
Karin Ruhlandt, distinguished professor and
chair, received a Fulbright award for travel to
Austria to further her research and to serve
as a guest lecturer.
Jon Zubieta was also honored by Inorganica
Chimica Acta with a special Festscrift
issue titled “Protagonists in Inorganic
Chemistry” (July 1, 2012, Volume 389).
The issue celebrated Professor Zubieta’s
career and achievements, highlighted by
750 publications, more than 21,000 total
citations, and an H index of 76. Scientists
from across the world– representing
academic, industrial and teaching
arenas–dedicated papers to Zubieta, with
contributions included from MIT, Oxford
University, Johns Hopkins University and
Max Planck among others, representing
more than a dozen countries.
Laurence A. Nafie, emeritus distinguished
professor, received the 2013 Pittcon Award
for Spectroscopy.
James Spencer received one of the five
2013 Chancellor’s Citation for Excellence
awards in spring 2013. Spencer was cited
for his “outstanding scholarship, superlative
teaching, extensive community engagement,
and commitment to the University
community.”
James Dabrowiak was awarded the
International Precious Metal Institute
Faculty Advisor Award, which is given on a
yearly basis for faculty advising of students
engaged in precious metals research. The
award also recognized his student Colleen
Alexander (see Graduate Achievements).
Faculty Grants/Patents:
Grants
Rob Doyle: Awarded National Institutes of
Health (National Institute of Diabetes and
Digestive and Kidney Diseases) R-15 grant
James Hougland: “Investigation of ghrelin
O-acyltransferase as a target for treating
for hyperphagia in Prader-Willi syndrome.”
Best Idea Grant, Foundation for PraderWilli Research.
Ivan Korendovych: National Science
Foundation Emerging Frontiers in
Research and Innovation. “Continuous
Liquid Fuel Production via Scalable
Biosynthesis of Enzyme-Quantum Dot
Hybrid Photocatalysts.”
Ivan Korendovych: Oak Ridge Associated
Universities. “Enzyme-Quantum Dot Hybrid
Catalysts for Artificial Photosynthesis to
Generate Liquid Biofuels.”
Patents
Rob Doyle: Awarded Patent on
Vitamin-B12 oral bioconugates with PYY
and GlP-1
Woven hydrogel based biosensor, Luk,
Yan-Yeung; Weldon, Mark; Shetye, Gauri;
Basner, Andrew; Simon, Karen; Burton, Erik
Bicyclic brominated furanones with low
toxicity for microbial control, Luk, YanYeung; Yang, Sijie
5
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Chemistry Updates and Scientific Endeavors
Department of Chemistry, Syracuse University
1-014 Center for Science and Technology
Syracuse, NY 13244-4100
Address Service Requested
Obituaries
DON DITTMER, a
professor emeritus, died
unexpectedly November
26, 2013, at his home in
Syracuse, NY. He earned
his B.S. in chemistry at the
University of Illinois, where he graduated
in 1950 as co-salutatorian with Bronze
Tablet recognition; and his Ph.D. from
Massachusetts Institute of Technology
in 1953. After one postdoctoral year
at Harvard University, he taught at
the University of Pennsylvania from
1954 to 1961. A one-year fellowship
at DuPont followed; then Dittmer
joined the faculty in our department
in 1962 and remained as professor of
chemistry until his retirement in 2001.
In October of that year, a retirement
dinner and Dittmer Symposium were
held. Since then, he had continued
research with both undergraduates
and with postdoctoral students, using
tellurium as an electron-transfer reagent
for in solvent-free organic syntheses.
Dittmer’s list of publications includes
more than 100 scientific articles,
many pertaining to organic synthetic
methods that utilize compounds of the
chalcogenide elements (sulfur, selenium,
and tellurium). A memorial service in
Hendricks Chapel will take place at 3pm
on February 21, 2014.
THOMAS H. WALNUT, a
professor emeritus, died
September 28, 2013,
in Syracuse of heart
failure. He earned his
A.B. at Harvard University,
interrupted by a spell serving with the
U.S. Army in the Pacific Theater during
World War II; and his Ph.D. from Brown
University. He did postdoctoral research
at the University of Chicago, then spent
more than 40 years of his professional
career as a professor in our department,
focusing on theoretical physical
chemistry, especially the theory behind
vibrational circular dichroism. He was
also active as a competitive runner with
the Syracuse Chargers Track Club.
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