AP Chemistry Notes/Chemistry Notes – Lab Safety I. INTRODUCTION Chemistry is a laboratory science. As part of your laboratory experience you will be asked to handle many chemical substances, manipulate specialized laboratory equipment, and safely carry-out many techniques and procedures specific to a chemistry laboratory. Many of these substances pose a health risk if handled improperly, while some laboratory equipment and techniques can cause severe injury if used/carried-out improperly. This unit will serve as a guide to safe laboratory practices you should use throughout the course. II. PREPARATION AND SAFETY Preparation is important not only to understanding, but most importantly to safety. If you are prepared for a laboratory it is much less likely that a laboratory accident will occur. To get the most out of your laboratory experience, you must be well prepared for each experiment by… o o o o o o o Reading the experiment thoroughly before coming to class Be sure you have a clear idea of what the experiment is about Be sure you understand each step of the procedure. DO NOT deviate from the procedure unless instructed to do so by your instructor. Ask your teacher if you have questions what the experiment is about or procedure questions. Be sure to note safety warnings and safety precautions listed in the safety section of each laboratory. Follow ALL laboratory rules outlined in your “CKHS Student Safety Contract.” You are expected to take the contract home, read it, have your parent(s)/guardian(s) read it, sign it (and have a parent/guardian sign it) then return it to me. The safety exam you take will include questions that refer to the rules in the safety contract. Start the year by viewing the ACS Laboratory Safety Video. 1 III. LABORATORY HAZARDS AND EMERGENCY PROCEDURES There are hazards that exist in the chemistry laboratory. This section will acquaint you with safety hazards and indicate what you can do to avoid these hazards. In all these cases, if the situation is serious, I may ask you to call 911. SITUATION AVOIDING SITUATION Thermal Burn Hold you hand near an item to feel for heat before touching it. Chemical Burn (Spills on Skin) Wear safety goggles and apron during all phases of the laboratoryeven during clean up. Do not wear open toed shoes Fainting Fire A fire may occur if chemicals are mixed improperly or flammable materials come to close to a burner or hot plate Poisoning SAFE RESPONSE Inform instructor immediately Immediately flush with cold water until burning sensation subsides Eye Exposure Inform instructor immediately Remove contacts and flush eye(s) with running water for 20 minutes. Skin Exposure Inform instructor immediately Using sink or emergency shower - flush exposed area with running water for 20 minutes. Inform instructor Immediately Provide fresh air (open a window). Move the person so that the head is lower than the rest of the body and initiate CPR if necessary. Fire on the Laboratory Bench Inform instructor Immediately Turn off all accessible gas outlets. Use fire extinguisher Follow all laboratory procedures Tie your hair back Do not ever reach over, around or any where near an open flame! Do not touch chemicals Never eat, chew gum or drink in the lab area. Never smell substances unless directed to do so by your instructor. Then ONLY use the proper “wafting” technique. Carry out labs that produce toxic or noxious gases in one of the fume hoods. Wash hands before leaving laboratory. Hair or Clothes Catch Fire Inform instructor Immediately Stop – Drop – Roll Use Fire Blanket to smother fire. Inform instructor Immediately Minor Cuts Always discard chipped and cracked glassware Chemical Spills Always work cautiously Inform instructor Immediately Acid Spill Neutralize spills with baking soda (NaHCO3) Base Spill Neutralize spills with baking soda (NaHCO3) or acetic acid (vinegar). Inform instructor Immediately Allow to bleed for a short time. Carry out necessary first aid. 2 IV. SAFETY EQUIPMENT, FIRE EXITS, AND THE CLASSROOM ENVIRONMENT Here is a list of the safety equipment that we have in our laboratory. You should know what each piece of equipment is, its use, and where it is found in the classroom. Safety Equipment: Equipment Goggles Aprons Eye Wash Picture Use Protect eyes Protect skin (and clothing) from exposure to chemicals. Rinse eyes of chemicals and/or foreign materials. Safety Shower Rinse the body free from chemicals. First Aid Kit Fire Blanket Carry-out minor first aid. Extinguish small fires on the desktop or hair or clothes fires. Fume Hood Carry out experiments that use or produce noxious or toxic fumes. Fumes are immediately removed to the outside of the building. Fire Extinguisher(s) Extinguish small fires on the desktop. Master Gas Shut-Off Telephone Material Safety Data Sheets Shuts off the gas to the entire classroom. Call 911 when directed by the instructor. Provides information on the chemical and physically properties of chemicals we use and provides information of treating The primary escape route in the event of a fire. The escape route in the event of a fire that should only be used if the primary route is not accessible. Primary Fire Exit Route (10) Secondary Fire Exit Route (20) 3 CLASSROOM MAP School Track Back Door Aprons Fire Extinguisher Safety Shower Chemical Storage Area Eye Wash Safety Goggles 0 1 Fire Exit Route Fume Hood First Fire Blanket Aid Kit MSDS Sheets Fume Hood Room 324 Front Bench Fume Hood Master Gas Shut-off (under sink) Telephone Front Door Fire Alarm 20 Fire Exit Route FIRE/ FIRE DRILLS: Leave the room in an orderly manner using the 10 fire exit route (if blocked use the 20 fire exit route). IN THE EVENT OF AN EARTHQUAKE -Duck, Cover (under desks, in doorway), Hold -Do not leave cover until directed to do so by your instructor or administrator. -When directed to do so by your teacher, proceed to the track and meet your ________ period teacher. 4 V. COMMON LABORATORY EQUIPMENT AND THEIR USES THAT YOU SHOULD KNOW: A. Equipment to Contain Solids and Liquids (NOT MEASURE) B. Equipment to Measure or Deliver a Given Volume of a Liquid 5 C. Miscellaneous Equipment You Should Know 6 VI. COMMON LABORATORY TECHNIQUES/PRACTICES THAT YOU WILL BECOME FAMILIAR WITH AND WILL LEARN TO SAFELY CARRY-OUT THIS YEAR: 1. a) Transferring Liquids from a Reagent Bottle b) Transferring Solids from a Reagent Bottle 2. Filtering and Decanting a Mixture (Precipitate) 3. Using a Gas Burner 4. Heating a Sample -Test Tube -Beaker -Evaporating Dish -Crucible 5. Using an Electronic Balance – Massing out a Solid 6. Using a Pipet (Including using a Safety Bulb) 7. Making Acid Solution (Add Acid) 8 . Titrating Techniques (Acid Base and Redox) 9. Safely Working with a Thermometer 10. Safely Working with a Centrifuge 11. Reading and Using a Graduated Cylinder or Burette 12. Properly Disposing of Chemicals After an Experiment. 13. Properly Preparing and Labeling Chemical Solutions -Using a Solid Reagent -Diluting a Stock Solution 14. Using Test Paper (pH) 15. Using Lab Tongs 16. Collecting a Gas Via Water Displacement 17. Recording Measurements and Carrying-Out Arithmetic Using the Appropriate Number of Significant Figures 18. Carrying Laboratory Equipment and Chemicals 7