AV400 standard Experiments setup
Expt
Standard dataset
2003/10/01
Parameters set
1H
C:\data\dual\nmr\1H
St_1D_1H_dual
13C
C:\data\dual\nmr\13C
St_1D_13C_dual
Dept135
C:\data\dual\nmr\dept135
St_1D_dept135
Dept90
C:\data\dual\nmr\dept90
St_1D_dept90
Cosy
C:\data\dual\nmr\cosy
St_2D_cosy
Hsqc
C:\data\dual\nmr\hmqc
St_2D_hmqc
Noesy
C:\data\dual\nmr\noesy
St_2D_noesy
Noesy.H2O
C:\data\dual\nmr\noesy.H2O
St_2D_noesy_H2O
Simple operation guide
Step 1: starting xwinnmr
1. login into computer.
2. double click on “xwin3.5” icon.
Step 2: loading and shimming a sample
1. adjust sample position ---2.0cm of sample gauge.
2. type “l” to open lock-display.
3. type “b” to open BSMS-display.
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4. in BSMS-display, select “sample” icon then “lift on/off”
then load a sample tube to magnet.
5. type “lock”, select D-solvent to lock magnetic field.
6. type “rshs” to directly read a standard shimming file eg.
shimnew.dual.
7. in BSMS-display, select “shim” icon to shim sample tube.
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Step 3: data collection
1. in xwinnmr, type “edc” to create a new file.
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only change NAME, EXPNO, DU and USER.
2. type “rpar st*”, select a experiment you need eg:
st_1D_1H_dual.
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3. type “rga” to find appropriate receiver gain.
4. type “ns” to enter the number of scan.
5. type “zg” to collect spectrum.
Step 4: data process and spectrum output
1. type “ft” to do Fourier Transfer.
2. Click on “phase” icon to phase spectrum then “store” .
3. type “abs” to automatic baseline correllection.
4. type “view” to check the plotting spectrum.
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5. type “edg” to adjust the plotting parameters eg: EDSPECT,
ed, change cx, cy parameter and so on and/or TITLE,
yes/no.
6. type “plot” to output the final spectrum from printer.
Other essential commands in xwinnmr
:
1. setres: change user interface eg. standard, extended,
horizontal, uxnmr. Or change zg safety by on/off.
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2. setti: set title text.
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