CHEM 4211 INSTRUMENTAL METHODS IN ANALYTICAL CHEMISTRY
SPRING 2004
COURSE DESCRIPTION
Time:
Classroom:
Instructor:
Office Hours:
TTR 9:00-9:50 AM
CRBL 303
Dr. Jorge Gardea-Torresdey
TTR 10:00-11:00 AM
COURSE PURPOSE
To familiarize the students of various fields of chemistry
with the impressive array of tools for obtaining qualitative and
quantitative information about the chemical composition and
structure of matter. Students must develop an appreciation for
these tools and how they are used to solve analytical problems.
The choice and efficient use of modern analytical instruments
require an understanding of the fundamental principles upon which
modern measuring devices are based. The basis of comprehension
of these principles will be emphasized so that the students more
efficiently will incorporate them in instrumental chemical
analysis and therefore will apply them for the solution of
problems.
TEXTBOOK AND OTHER STUDY MATERIAL
The textbook selected is "Principles of Instrumental
Analysis", fifth edition, by Skoog/Holler/Nieman (Saunders
College Publishing, 1998). Additional reference material will be
distributed in the classroom and students are always welcome to
request supplementary information from the instructor. The
instructor is always well-informed of current developments in the
instrumental chemical analytical field. Come and see me in my
office if you need to discuss a topic of your interest.
COURSE LECTURE OUTLINE
TOPIC
REFERENCE CHAPTER IN TEXTBOOK
Introduction
1, 4
TOPIC
REFERENCE CHAPTER IN TEXTBOOK
Introduction to Spectrometric
1
Methods
6
Components of Optical Instruments
7
An introduction to Molecular UV
Absorption Spectrometry
13
Applications of UV Absorption Spectrometry 14
Atomic Absorption Spectrometry
8-9
Atomic Emission Spectrometry
10
Atomic Mass Spectrometry
11
An Introduction to Infrared Spectrometry
16
Applications of Infrared Spectrometry
17
Molecular Mass Spectrometry
20
Electroanalytical Chemistry
22-25 (Summary)
An Intro. to Chromatographic Separations
26
Gas Chromatography
27
High-Performance Liquid Chromatography
28
Other Separation Methods
29-30
Supplemental Activities
If time allows, special topics will be discussed in the class.
Problems in most chapters covered in the lecture will be
assigned. These problems are for your benefit and it is strongly
suggested working through them. The assigned problems will not be
graded. In addition, homework which will involve the use of the
Internet will be assigned. This work will be related to new
developments in chemical instruments, instruments manufacturers
and costs. These assignments will constitute 10% of the final
grade.
EXAMS
There will be three written examinations, each one class
period long (except the final exam). The examinations will cover
2
the subjects of the preceding classes. The final examination
will be comprehensive.
The tentative dates for the examinations will be February 17,
March 30, and May 4.
The grading will be as follows:
First exam
Second exam
Third exam
Internet Homework
30%
30%
30%
10%
The overall grade will be determined by performance and
competency. There will be a "grading scale" and it will be
determined at the end of the spring semester. This scale will be
based on the distribution of the total scores for the class as a
whole in a similar fashion to a "curve". However, this is not to
be interpreted exactly as a "curve". The following scale (which
is subjected to change) is to be used as a general guideline:
Scale
91-100
81-90
71-80
61-70
0-60
Grade
A
B
C
D
F
NOTE: Excessive unexcused absences will prove to be detrimental
to the student's performance in the course. Student
participation in the class is encouraged.
Your instructor is available for help and advice in his office,
room 201, PSCI Building. My phone number is 747-5359 (e-mail,
jgardea@utep.edu).
CAVEAT: THE COURSE OUTLINE IS SUBJECT TO SLIGHT VARIATION WITHOUT
PRIOR NOTICE.
3
4