SYLLABUS CHEM 202 Lab - Inorganic Chemistry 2 Laboratory

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SYLLABUS
CHEM 202 Lab - Inorganic Chemistry 2 Laboratory
Spring, 2012
Instructor: Dr. J. Scott McConnell
Office and Office Hours: The lab director’s office is 519A. Office hours are 3:00 - 5:00
Monday; 1:00 - 4:00 Thursday; and 4:00 - 6:00 Friday. Call the Chemistry Department
(309-298-1538) or e-mail JS-McConnell@WIU.edu, and make an appointment prior to
meeting.
Laboratory Manual: “CHEM 202: Inorganic Chemistry II,” by R.R. Bahr and J.S. McConnell.
Thomson Custom Solutions, publishers.
Laboratory Times: As scheduled.
Laboratory Location: Currens 319, 323
Laboratory Assistants:
Mr. Varun Debetti, Ms. Brianna Norris, Ms. Karen Ribordy, and Ms.
Nikhila Voleti.
Expense Materials Required: Costs for these materials are the responsibility of the student.
Laboratory Manual. “CHEM 202: Inorganic Chemistry II,@ by R.R. Bahr and J.S.
McConnell. Thomson Custom Solutions, publishers.
Material Safety Data Sheets (MSDS) of all chemicals utilized in the laboratory can be
found at the following web site. http://physchem.ox.ac.uk/MSDS/#MSDS. E-copies are
free of charge.
Approved eye protection used for the laboratory component of this class.
A simple scientific calculator without extensive memory functions (i.e. Texas Instruments
model 30, equivalent, or less sophisticated models).
Information Regarding CHEM 202 Lab:
Lab work is an integral part of the CHEM 202 course. Lab attendance is important and you
must attain a minimum of 130 total lab points to pass the course regardless of the lecture
grade. It is important that you complete the pre-lab assignment BEFORE the day of the lab
so that you are familiar with:
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 The lab procedure and can conduct the lab in a time efficient manner ,
 The equipment used and the lab techniques involved, and
 The calculations used in the lab.
All labs are worth 25 points and the grade will be based on the best 10 out of 12 labs. There
are NO MAKE UP LABS. Lab reports are due by 5:00 p.m. the day after the lab session is
completed. A penalty of five points per day will be levied for late labs. Lab reports may be
turned into the Teaching Assistant or Graduate Assistant or at Currens 214 to the Teaching
Assistant’s or Graduate Assistant’s mail box. Labs MUST BE marked with the following:
Student’s Name, Course Number, Section Number, TA/GA’s Name. Failure to exclude this
information may result in a zero for the lab.
Important Dates:
Date (Spring, 2012)
January 16
January 17
February 13
February 14
March 12-16
March 19
May 7-11
Event
Dr. Martin Luther King Day - University closed
Classes Begin
Lincoln's Birthday - University closed
Classes resume
Spring Break - No Classes
Classes resume
Final Exam Week
Any situation, condition, or circumstance not
covered in the syllabus is subject to the decisions of
the instructor, only.
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Date
Lab No.
Experiment
Jan 24 and
26
Lab #1
LAB CHECK IN / AVOGADRO’S NUMBER
Prelab–Read background information, procedure and answer
prelab questions 1-3 on pg. 13. (Worth 5 points if turned in before
lab starts). Lab–Complete procedures I, II and III and record
results in data tables. Do calculations and post-lab questions 1-5
on pg. 7-11.
Jan 31 and
Feb 2
Lab #2
MOLECULAR MODELS
Prelab–Read introduction and procedure on pg.13-15. Do prelab
questions 1-4 on pg.17 (Worth 5 points if turned in before lab
starts). Lab–Do procedure on pg. 16-18 and complete report form
on pg. 21-24, do post lab questions 1-4 only on pg. 25.
Feb 7 and 9
Lab #4
LEWIS STRUCTURES AND MOLECULAR SHAPES
Prelab–Read introduction on pg.43-48 and complete chart #1 only
on pg. 49 for prelab assignment. (Worth 5 points if turned in before
lab). Lab–Read procedure and use model kits to complete the
following: Part I A and B on pg. 51. Part II A and B on pg. 54. No
post-lab questions.
Feb 14 and
16
Lab #5
CHARLE’S LAW
Prelab–Read introduction and procedures on pg. 63-66 .Do
prelab questions 1-4 on pg. 67. (Worth 5 points if turned in before
lab starts). Lab–Do procedure and record data on report form on
pg. 69. Do calculations and post lab questions 1-7 on pg. 71-72.
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Feb 21 and
23
Lab #6
GRAHAM’S LAW
Prelab–Read background information and procedures on pg. 7375. Do prelab assignment 1-4 on pg. 83-84. (Worth 5 points if
turned in before lab starts). Lab–Do procedure and record data on
pg. 81. Answer post lab questions 1-5 on pg. 79-80.
Feb 28 and
March 1
Lab #7
COLLIGATIVE PROPERTIES
Prelab–Read introduction and procedure on pg. 85-90. Do prelab
questions 1-4 on pg. 91-92. (Worth 5 points if turned in before lab
starts). Lab–Do procedure and calculations on pg. 86-90 and
record data on pg. 93-96. Do post lab questions on pg. 97-98.
March 6
and 8
Lab #9
ACID-BASE TITRATION
Prelab–Read background information and procedure on pg. 109116. Do prelab assignment 1-2 on pg. 125-126 (Worth 5 points if
turned in before lab starts). Lab–Do procedure and calculations on
pg. 113-116. Record your data and prepare titration plots. pg. 119123. Answer post lab questions 1-4 on pg. 118-119.
March 20
and 22
Lab #11
A STUDY OF REACTION RATES
Prelab–Read chemical overview and procedure on pg.143-145.
Do advanced study assignment 1-3 on pg.147. (Worth 5 points if
turned in before lab starts). Lab–Do procedure on pg. 144-145 and
record results on work pages 149-150. Use results to complete
graphs on pg. 151 and 155.
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March 27
and 29
Lab #12
CHEMICAL EQUILIBRIUM
Prelab–Read introduction and procedure on pg. 157-162. Answer
prelab questions 1-3 on pg. 163-164. (Worth 5 points if turned in
before lab starts). Lab–Do procedure and record data on report
form pg. 165-167. Do post lab questions 1-3 on pg. 169-170.
April 3 and
5
Lab #13
ENERGY CHANGES IN CHEMICAL REACTION
Prelab–Read introduction and procedure on pg. 171-173. No
prelab assignment. Lab–Do procedure and record data with
calculations on pg. 171-178. Do post lab questions 1-11 on pg.
179-180.
April 10 and
12
Lab #10
ASCORBIC ACID IN VITAMIN C
Prelab–Read background and procedure on pg. 129-135. Do
prelab assignment on pg. 141-142. (Worth 5 points if turned in
before lab starts). Lab–Do procedure and record data on pg. 139140 and do calculations. Do post lab questions 1-4 on pg. 137138.
April 17 and
19
Lab #14
ELECTROCHEMICAL CELLS/CHECK OUT
Prelab–Read background and procedure on pg. 181-188. Do
prelab assignment 1-5 on pg. 195-196 (Worth 5 points if turned in
before lab starts). Lab–Do procedure and record data on pg. 185194 and do calculations on pg. 194. Do post lab questions 1-3 on
pg. 189.
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