II. PETROGRAPHY a. Introduction Petrographic analyses were carried out on fifty-five [55] samples. The lithologies and reservoir characteristics of these samples are tabulated, Figs. 3 & 4, and the petrographic descriptions together with photomicrographs are provided Plates 1-55. b. Procedures The sidewall cores were impregnated with blue-dyed epoxy resin to facilitate porosity recognition. They were half-stained with a mixture of Alizarin Red “S” and Potassium Ferricyanide reagents. Two color photomicrographs were taken from each thin section to illustrate representative features of the samples. Carbonate rocks are classified according to the scheme introduced by Dunham [1962], while porosity types were identified according to Choquette and Pray [1970]. The clastic rocks are classified to the scheme of Folk [1971]. The amount of various components of rock samples was inferred with the help of the comparison chart for visual percentage estimation according to Terry and Chilingar [1955]. Modal analysis by point counting was not requested by Gulf. The following quantifiers petrographic data sheets: >15% 5-15% 1-5% <1% abbreviations are used in of the rock volume of the rock volume of the rock volume of the rock volume Lithost ratigra phy [Gulf] A abundant C common M minor Trace and Lithology Classified Lithology Tuban Limestone Wackestone 2 Rancak Limestone Wackestone 3 Kujung Limestone Pack-grainstone SWC Depth [feet] Plate No. 3738.0 1 4148.0 4760.0 the c. 4772.0 4 4782.0 I Limestone Packstone 5 Limestone Wackestone 4786.0 6 Limestone Wackestone 4792.0 7 Limestone Wacke-floatstone Depositional Environment & Reservoir Quality The following are some general comments, by formation, on depositional environments and reservoir quality of the rocks studied. The comments on depositional environment can only be regarded as tentative, without additional evidence from biostratigraphy etc. i. Tuban Formation Only one [1] sidewall core, 3738’, was analyzed from this formation and it is described as a limestone, Plate 1, which is a coarse grained, poorly sorted, skeletal wackestone, with a minor amount of lime mud matrix. The matrix has generally been replaced by very fine dolomite. Skeletal grains are predominantly benthic foraminifera with common molluscan and coral debris, minor red algae, echinoderm debris, and planktic foraminifera. Sand and silt-sized grains are sparsely distributed. Calcite cement occurs as fine to medium, crystals, in the chambers of skeletal components. It locally forms isopachous cement. There is good visible porosity [20% visual estimate], comprising a combination of primary intraparticle pores associated with coral and foraminifera, secondary pores resulting from dissolution, and intercrystalline pores between dolomite rhombs. Fractures are also significant, connecting the pores. The skeletal grain and depositional textures suggest that this limestone was deposited in a low energy shallow carbonate shelf environment. ii. Rancak Formation Only one [1] sidewall core, 4148’, was analyzed from the formation and it is described as a limestone, Plate 2, which is a lower coarse grained, poorly to moderately sorted, skeletal wackestone locally grading to packstone, with abundant lime mud matrix. The matrix has been selectively replaced by very finely, euhedral to subhedral dolomite. Skeletal grains are predominantly larger benthic foraminifera, with minor red algae, echinoderm debris, smaller benthic foraminifera, corals and micritized skeletal grains. Calcite cement is minor, occurring in finely to medium crystalline equant to blocky forms, in the chambers of skeletal components. This limestone is characterised by good porosity [12% visual estimate], consisting of a combination of primary interparticle pores between skeletal grains, secondary pores resulting from dissolution, and intercrystalline pores between dolomite rhombs. These pores are often well interconnected by fractures. The skeletal grain assemblages and depositional textures suggest deposition in a low energy, shallow carbonate shelf environment. iii. Kujung I Formation Sixteen [16] sidewall core samples from Kujung I were analysed, fourteen [14] of which are limestones and two [2] dolostones. Depositional Environment The Kujung I limestones from this well are dominantly wackestones, with minor grainstone, packstone and floatstone textures. The wackestones contain varying amounts of skeletal fragments, generally set in an abundant lime mud matrix. This matrix has been locally replaced by dolomite. The assemblage of skeletal grains is very similar in most of the Kujung I limestones. The sizes of skeletal grains range from fine to pebble, but are generally between coarse and very coarse, with poor sorting coefficients. The most common skeletal grains observed, in whole and fragmented forms, are larger benthic foraminifera, Plates 4A & B, 12, 13B, 15B. including lepidocyclinids, however, coral fragments are sometimes present in significant amounts and prevail over larger benthic foraminifera at 4792’, 5161’ and 5500’, Plates 7A & B, 14A. Other skeletal grains that are frequently present, but in varying amounts are red algae, Plate 4B, smaller benthic foraminifera including miliolids, echinoderms, Plates 6A, 7A, peloids, Plates 8B, 13B, molluscs and micritized skeletal grains. Green algae and planktic foraminifera, Plate 16B are also present in trace amounts in some samples. The dolostone at 5349’ is composed of finely crystalline euhedral dolomite rhombs, which forms a hypidiotopic fabric providing numerous porous zones. The original texture of this dolostone could not be determined with certainty, since no surviving depositional fabrics remain, Plate 17, due to the intensive dolomitization. The dolostone at 5500’ also resulted from the intensive dolomitization of a precursor limestone. It contains minor skeletal grains including molluscan and coral debris, and patches of lime mid matrix that are suggestive of a wackestone depositional texture, Plate 18. Based on the presence of miliolids, the low diversity of faunal assemblage and the abundance of lime mud matrix, the predominant palaeoenvironmental setting of Kujung I is interpreted as a low energy, relatively restricted, shallow marine shelf. The abundance of coral fragments in some of the limestones, such as 4792’, 5161’, indicates reefal or “near-reef” conditions, although evidence for the presence of in-situ reef facies is not conclusively seen in thin sections analysis. Visible Porosity and Reservoir Quality The Kujung I carbonates have variable visible porosity from poor to good, but most of samples [eleven of the sixteen] have fair to good porosity, ranging from 6% to 22% by visual estimate. The best reservoir zones identified by petrographic analysis are found at 4792’, 4896’, 5205’, 5349’ and 5500’ with visible porosity being greater than 15%. Porosity, in the limestones, consists generally of a combination of vuggy pores, Plates 11 A & B, 13B, resulting from dissolution, and tectonically generated fractures, Plates 13A, 16A & B, 18 A & B. Fractures, though volumetrically minor, are thought to provide considerable permeability assistance to the pore network. Mouldic pores and primary intraparticle [intraskeletal] pores associated with the chambers of foraminifera and corals, Plates 7A & B, 15B and intercrystalline pores are also present in some of the limestones. In the dolostones, 5349’ and 5500’, porosity is dominated by intercrystalline pores occurring between dolomite rhombs Plates 17 A & B, with minor amounts of vuggy pores, which sometimes form oversize pores ranging up to 2.30mm across. These oversize pores were probably created by vadose groundwater dissolution. The diagenetic processes that have affected the limestones and their reservoir quality from Well Jenggolo-1 include cementation, replacement and dissolution. The diagenetic processes commenced syn-depositionally in the marine phreatic environment, and were followed by major diagenetic changes and modifications in vadose and meteoric phreatic environments. Diagenesis continued with increasing overburden pressure and later tectonism caused the development of fractures and stylolites during deeper burial conditions. All of the limestone samples are considered to display a similar sequence of diagenetic fabrics. A generalized pattern of diagenesis of the limestones as interpreted from thin sections is presented below and they are listed in relative chronological order. However, not all of the events and diagenetic fabrics can be seen and found in all of the limestones. i. Early/Syn-depositional Lithification of Matrix and Micritization of Skeletal Grains: Most depositional lime mud matrix is thought to have lithified early, neomorphically stabilizing from lime mud to microspar Plates 34B, 40B, 41B. Matrix stabilization and micritization of skeletal grains probably took place in the marine phreatic environment, and is likely to have been accompanied by some minor early fringing and isopachous cements [a few such cements are locally recognized in thin section such as in samples 5848’, 6198’]. ii. Dissolution of Unstable Skeletal Grains: This process is considered to have occurred under freshwater vadose diagenetic conditions, forming moulds and enlarged moulds or vugular pores. Leaching was very extensive in places particularly in the Kujung I and II carbonates, and probably occurred due to flushing of the pore network by large quantities of meteoric water in a fresh water vadose environment. The development of vadose conditions is suggested from the existence of oversize pores in the limestones Plates 15A, 17A, 18A & B. Under this diagenetic regime, inversion of skeletal aragonite [e.g. coral and mollucan debris] has also probably taken place. iii. Calcite Cementation of Moulds and Vugs: Mouldic porosity resulting from the early stage dissolution of unstable skeletal grains, primary interparticle and primary intraparticle porosity was completely filled by finely to medium to locally large, mosaic calcite cement crystals, Plates 8B, 26B, 32B, 47A & B, 50A. This is thought to have occurred in a fresh water phreatic environment. However, not all porosity was cemented, and some mouldic and vuggy porosity survives. Some calcite cement crystals are large, and occasionally they are very slighty ferroan. This suggests that at least some of the calcite cement formed slowly, possibly after considerable burial. iv. Compaction and Collapse of Sediment: The limestones appear to have locally experienced compaction and possible collapse. This is evidenced by disordered vugs and by plastically deformed and broken skeletal particles, and the local presence of grain-to-grain contacts, Plates 4A, 31B. These fabrics suggest that compaction of the sediments took place before major calcite cementation. v. Dolomite Precipitation: Dolomite is present in significant amounts in a number of Kujung and Ngimbang carbonates occurring mainly as a very finely to finely crystalline replacive mineral, Plates 37A & B. Replacive dolomite has mainly affected the argillaceous lime mud matrix. Dolomite is also observed as porefilling material and tends to be minor in quantity and found in open vuggy pores as cement. These two types of dolomite may have formed relatively early during burial. Later stage dolomite formation probably occurred along stylolites as stylocumulate, and it appears to post-date calcite cementation in most cases, and may be related to dewatering of the rock due to stylolitization. vi. Stylolitization and Fracturing: Stylolites were observed, particularly in some of the Ngimbang limestones, Plates 42B, 43A, 44A, indicating that reductions in rock volume have occurred since deposition. They are generally low to moderately peaked, are generally lined with dark insoluble material including pyrite, clay and dolomite. Minor leaching associated with stylolites appear to have occurred prior to hydrocarbon migration. Open, tectonically generated extensional fractures are also present in most samples, Plates 14A & B, 16A & B, 20A, 43A, but they are generally volumetrically minor as estimated from thin sections. Locally laterstage calcite cement has selectively filled fractures, Plates 6B, 13A, 49B. vii. Late Dissolution: Some of the observed secondary porosity of small vugs in the limestones probably formed at a later diagenetic stage of burial due to non-fabric selective dissolution, as suggested by the presence of small vuggy pores that are completely free of any cement. The fact that the often well developed matrix intercrystalline pores have not collapsed or been compacted also suggests some leaching may have occurred during later stages of burial Lithology : Limestone Classification : Wackestone FRAMEWORK GRAINS Larger benthic foraminifera Smaller benthic foraminfera Molluscs Corals Red algae Planktic foraminifera Echinoderms Quartz MATRIX Lime mud 40% CEMENTS / REPLACEMENTS C Dolomite C Calcite C C M M M M 5% VISIBLE POROSITY M Pore Type % 35% A M 20% TEXTURE Grain Size Minimum Mode Maximum Grain contacts Sorting Abrasion : : : Fine Coarse Pebble : Floating : Poor : Abraded>unabra ded Intraparticle Fracture Vuggy Intercrystalline Mouldic 7% 5% 4% 3% 1% Summary: Lithology, Texture and Composition: Coarse grained, poorly sorted, skeletal [foraminiferal] wackestone, with a minor matrix of lime mud. The matrix has generally been replaced by very finely dolomite [Plate B]. Skeletal grains are predominantly benthic foraminifera [Plate A, DE7] with common molluscan and coral debris [Plate A: I14], minor red algae, echinoderm debris [Plate A: G-H4-5], and planktic foraminifera. Most skeletal grains are poorly sorted and abraded. Sand and silt-sized grains are sparsely distributed [Plate B: E15, J-K12]. Calcite cement occurs in finely to medium crystalline equant to blocky forms, in the chambers of skeletal components, and locally forms isopachous cement. Depositional Environment: Relatively low energy, unrestricted shallow carbonate shelf environment, with input of terrestrial quartz grains and redeposited coral debris. Main Diagenetic Sequences: Dissolution of unstable skeletal grains to form moulds, dolomitization of matrix, precipitation of calcite cement, non-fabric selective dissolution of carbonate components at a relatively late diagenetic stage, late-stage fracturing. Visible Porosity: Good [areas of blue-dyed resin in Plates A & B], comprising a combination of primary intraparticle pores in coral and foraminiferal chambers, secondary pores resulting from dissolution, and intercrystalline pores between dolomite rhombs [Plate B]. These pores are often connected by fractures and filled with indeterminate opaques resembling residual oil or bitumen. Plate A: Plane-polarized light, 1cm = 0.30 mm Plate B: Plane-polarized light, 1cm = 0.07 mm Lithology : Limestone Classification FRAMEWORK GRAINS Larger benthic foraminifera Smaller benthic foraminifera Red algae Corals Echinoderms Micritized grains MATRIX Lime mud : Wackestone 25% CEMENTS / REPLACEMENTS C Dolomite C Calcite M M M M 28% VISIBLE POROSITY A Pore Type % TEXTURE Grain Size Minimum Mode Maximum Grain contacts : : : Fine Lower coarse Very coarse : Floating Interparticle Intercrystalline Vuggy Mouldic 5% 4% 2% 1% 35% C C 12% Sorting Abrasion : Poor-moderate : Abraded>unabra ded Summary: Lithology, Texture and Composition: Lower coarse grained, poorly to moderately sorted, skeletal [foraminiferal] wackestone locally grading to packstone, with an abundant matrix of lime mud. The matrix has been selectively replaced by very finely, euhedral to subhedral dolomite [Plate B]. Skeletal grains are predominantly larger benthic foraminifera [Plate A: C6, F7], with minor red algae, echinoderm debris, smaller benthic foraminifera, corals and micritized grains [Plate B: F10-11]. Calcite cement is minor, occurring in finely to medium crystalline equant to blocky forms, in the chambers of skeletal components. Depositional Environment: The skeletal grain assemblages and depositional textures suggest that this limestone was deposited in a low energy, unrestricted [?], shallow carbonate shelf environment. Main Diagenetic Sequences: Dissolution of unstable skeletal grains to form moulds, neomorphic stabilization of lime mud, dolomitization of matrix, precipitation of calcite cement, non-fabric selective dissolution of carbonate components at a relatively late diagenetic stage, latestage fracturing. Visible Porosity: Good visible porosity [areas of blue-dyed resin in Plates A and B], comprising a combination of primary interparticle pores between skeletal grains, and secondary pores resulting from dissolution, and intercrystalline pores between dolomite rhombs. These pores are often well interconnected by fractures. Plate A: Plane-polarized light, 1cm = 0.15 mm Plate B: Plane-polarized light, 1cm = 0.07 mm Lithology : Igneous Rock [extrusive] Classification : Andesite PRIMARY MINERALS Plagioclase feldspar Pyroxene Opaques [ores] Hornblende 45% SECONDARY MINERALS A Pyrite C Chlorite C M 20% M C Quartz GROUNDMASS Altered Trace 30% VISIBLE POROSITY A Pore Type % 5% TEXTURE Porphyriti Dissolution 5% c This rock sample is a porphyritic andesite composed principally of phenocrysts of feldspar, with subordinate pyroxene [F-K3-7], opaque minerals [ores, A-B11, B-C2, F-G8], minor hornblende and traces of quartz, embedded in a widespread microlithic groundmass. The groundmass is composed mainly of secondary chlorite [yellowish brown interference color between plagioclase phenocrysts and microliths, small plagioclase laths [generally ranging from 0.07 to 0.18 mm, E7.5, E4-5, E-F14, etc] and other unidentifiable microcrystalline minerals. Feldspar is mainly plagioclase with minor potassium feldspar [orthoclase?]. Plagioclase phenocrysts [E-K1-2] range up to 2.0 mm, and are anhedral to subhedral and mostly unfresh but there are some are quite fresh, zoned types. The degradation of plagioclase is due to either the partial alteration to sericite or partial replacement by chlorite. Secondary chorite is also observed, occurring as a replacement of former unknown minerals [mafic minerals?]. Patches of oversize pores [up to 1.80.mm in diameter] are present [C6.5, I-J14] and interpreted to be related to the dissolution of unstable minerals such as mafic minerals. This andesite can be regarded as being moderately altered. Plate A: Plane-polarized light, 1cm = 0.15 mm Plate B: Cross-polarized light, 1cm = 0.15 mm Lithology : Siltstone Classification FRAMEWORK GRAINS Quartz : Quartzarenite 58.4 CEMENTS / % REPLACEMENTS 46.4 Calcite 29.2 % 25.6 Muscovite mica Plagioclase Chlorite Organic material Indeterminate heavy minerals Chert MATRIX Clay % Pyrite 4.4% 2.4% 1.6% 1.6% 1.2% 0.8% 12.4 VISIBLE POROSITY % 12.4 Pore Type % % % 3.6% 0% TEXTURE Grain Size Minimum Mode Maximum Grain contacts Sorting Roundness : : : N/A 0.06mm 0.18mm [fine] : Planar, point : Good : Subangular>ang ular Summary: Lithology, Texture and Composition: This sample is a well-sorted, massive, quartzarenitic silstone that has been well cemented by slightly ferroan calcite. Framework grains are predominantly quartz, with minor to trace amounts of muscovite mica, plagioclase, detrital chlorite, chert, organic material and indeterminate heavy minerals. Most grains are subangular to angular and have planar and point grain contacts. Detrital clay forms patches of interstitial matrix and laminated fabrics. Widespread ferroan calcite cement has filled available intergranular pore space. Pyrite occurs both as a minor secondary cement and replacement mineral. Depositional Environment: Diagnostic indicators environments of deposition were not observed. Main Diagenetic cementation. Sequences: Minor pyrite, relating early to stage the calcite Visible Porosity: The sandstone has no visible porosity, due to calcite cementation. Plate A: Plane-polarized light, 1cm = 0.15 mm Plate B: Cross-polarized light, 1cm = 0.15 mm Lithology : Claystone Classification FRAMEWORK GRAINS Quartz Mica flakes MATRIX Clay : Quartz arenit 2.4 CEMENTS / % REPLACEMENTS 1.2% Pyrite 1.2% 3.6% 93.2 VISIBLE POROSITY % 93.2 Pore Type % % 0.8% 3.6% TEXTURE Grain Size Minimum Mode Maximum Grain contacts Sorting Roundness : : : N/A Clay-size 0.06mm [silt] : N/A : N/A : N/A Fracture 0.8% Summary: Lithology, Texture and Composition: Claystone containing minor amounts of silt-sized quartz grains and mica flakes. The groundmass appears to be composed predominantly of illitic clays. Pyrite is the only secondary mineral observed, occurring as a replacive mineral [Plates A&B: E-F11-13]. Depositional Environment: Indeterminate [no diagnostic indicators of depositional environment observed]. Main Diagenetic Sequences: Early stage formation of pyrite, late stage fracturing. Visible Porosity: Negligible, only limited to few tiny fractures. Plate A: Plane-polarized light, 1cm = 0.07 mm Plate B: Cross-polarized light, 1cm = 0.07 mm Lithology : Claystone Classification : FRAMEWORK GRAINS Quartz Organic material Feldspar [plagioclase?] MATRIX Clay 2.8 % 1.6% 0.8% 0.4% 90.4 % 90.4 % CEMENTS / REPLACEMENTS Pyrite Calcite 5.2% VISIBLE POROSITY 1.6% Pore Type 4.4% 0.8% % TEXTURE Grain Size Minimum Mode Maximum Grain contacts Sorting Roundness : : : : N/A Clay size 0.30mm [medium] Fracture 1.6% N/A : N/A : N/A Summary: Lithology, Texture and Composition: The claystone is composed essentially of clay minerals, most of which are possibly of illitic composition. Organic material in disseminated forms, and silt to sand- sized quartz and feldspar grains are present in minor amounts. Pyrite [I-J7-8] and calcite occurs sporadically as minor replacement minerals. Depositional Environment: Indeterminate. Main Diagenetic Sequences: stage fracturing? Minor pyrite and calcite formation, late Visible Porosity: There is no visible porosity, except for few tiny fractures. Plate A: Plane-polarized light, 1cm = 0.07 mm Plate B: Cross-polarized light, 1cm = 0.07 mm Lithology : Siltstone Classification : Quartzarenite FRAMEWORK GRAINS Quartz Muscovite mica Plagioclase Chlorite Organic material Indeterminate heavy minerals Chert MATRIX Clay 58.4 % 46.4 % 4.4% 2.4% 1.6% 1.6% 1.2% 0.8% 12.4 % 12.4 % TEXTURE Grain Size Minimum Mode Maximum Grain contacts : : : N/A 0.06mm 0.18mm [fine] : Planar, point CEMENTS / REPLACEMENTS Calcite Pyrite 29.2 % 25.6 % 3.6% VISIBLE POROSITY Pore Type % 0% Sorting Roundness : Good : Subangular>ang ular Summary: Lithology, Texture and Composition: This sample is a well-sorted, massive, quartzarenitic silstone that has been well cemented by slightly ferroan calcite. Framework grains are predominantly quartz, with minor to trace amounts of muscovite mica, plagioclase, detrital chlorite, chert, organic material and indeterminate heavy minerals. Most grains are subangular to angular and have planar and point grain contacts. Detrital clay forms patches of interstitial matrix and laminated fabrics. Widespread ferroan calcite cement has filled available intergranular pore space. Pyrite occurs both as a minor secondary cement and replacement mineral. Depositional Environment: Diagnostic indicators environments of deposition were not observed. Main Diagenetic cementation. Sequences: Minor pyrite, relating early to stage the calcite Visible Porosity: The sandstone has no visible porosity, due to calcite cementation. Plate A: Plane-polarized light, 1cm = 0.15 mm Plate B: Cross-polarized light, 1cm = 0.15 mm