Empirical Formula of Copper (?) Oxide Lab (Due for 100% credit anytime during the week of 1/16/12. After that, -10 pts. per day.) Purpose: (what are we trying to determine in this lab??) To determine _______________________________________________________________________________ by calculating the ________________________________________of the unknown compound, copper (?) oxide. Precautions: (list as many as you can think of that actually apply to this situation) __________________________________________ __________________________________________ __________________________________________ __________________________________________ __________________________________________ __________________________________________ Materials: (list as many as you can think of that we actually use in this lab) 2.0 g black powder compound (the copper (?) oxide) __________________________________________ rubber tubing with L-shaped glass tubing attached __________________________________________ __________________________________________ __________________________________________ __________________________________________ __________________________________________ Procedure: (list as many steps as you can think of that we actually do in this lab) (this drawing needs to be on your formal lab report!) 1. _________________________________________________________ 2. _________________________________________________________ 3. _________________________________________________________ 4. _________________________________________________________ 5. _________________________________________________________ 6. _________________________________________________________ 7. _________________________________________________________ 8. _________________________________________________________ 9. _________________________________________________________ 10. _________________________________________________________ 11. _________________________________________________________ 12. _________________________________________________________ 13. _________________________________________________________ Data Table: mass of black powder given (g) A. mass of test tube and black powder BEFORE heating (g) B. mass of test tube and new color powder AFTER heating (g) C. description of powder in test tube AFTER heating D. mass of oxygen “lost” (g) E. mass of copper remaining (g) F. % oxygen G. % copper H. empirical formula I. name of empirical formula J. 2.0 g copper (___) oxide For the calculations: E=B–C F=A–E G=E÷A H=F÷A I = use G and H to calculate, compare to ideal data (below) J = use data from I to answer No, you do not include this instructions box on your final draft!!! Just the data table! Calculations: ideal data (percent composition): copper (I) oxide = ______________ copper (II) oxide = ______________ Cu = ___ (___________) = ____________ Cu = ___ (___________) = ____________ O = ___ (___________) = ____________ O = ___ (___________) = ____________ ____________ g/mol ____________ g/mol Cu = ____________ = __________% Cu Cu = ____________ = __________% Cu O = ____________ = __________% O O = ____________ = __________% O Caution! Unless your experiment had EXCELLENT results, your empirical formula may not turn out “normal.” You might end up with a strange ratio like Cu7O4. Remember, the only ratios that can possibly exist are Cu2O and CuO! Calculations: experimental data: Experimental Percent Composition: Experimental Empirical Formula: g Cu = H.__________% Cu H._________g Cu 2.0 g total F._______ A. E._______ g O = G.__________% O A. 2.0 g total 1 mol Cu 63.55 g Cu = _________ = 1 mol O 16.00 g O = _________ = G._________g O Note: Your empirical formula Difference between the Experimental Percent Composition and the Ideal Percent Compositions: calculation above may not clearly ________% Cu in copper (I) oxide – H.________% Cu experimentally – __________% difference _________% Cu in copper (II) oxide H._________% Cu experimentally __________% difference indicate to you what the correct formula is. So instead, think about which calculation here has the smaller difference. The formula with the smaller difference is the formula your experimental data is indicating. Graphs: (construct three pie charts showing the percent compositions of the ideal and experimental data) Each slice = 10% KEY = Cu =O Ideal copper (I) oxide Experimental copper (?) oxide Ideal copper (II) oxide * = Cu2O or CuO Conclusion: The compound that was decomposed in the test tube was ____*____, copper (___) oxide, because the percentages calculated from the actual data more closely match the ideal percentages of this compound (a difference of _______%) than they do the ideal percentages of the other copper oxide compound, ___*____ (a difference of _______%). Questions: (Answer the following questions with full sentences, meaning, you must re-state the question in your answer. Also, number your answers in the same way as the questions are numbered below.) 1. Write and balance the reaction that took place. (use your data to predict the product) To access an easy-to-use 2. Briefly (but specifically) describe what change(s) you saw occurring to the TEMPLATE for your lab, copper oxide powder as it was heated, and tell approximately how long it took. go to Mrs. Rigdon’s 3. Describe the color of your final product (be specific). website, then click on 4. Why do you think we ran the burner’s methane gas into and out of the test tube “Important Files.” Then during the heating process, rather than heat the compound in the open air? click “Other Important 5. Why do we call this reaction a “decomposition” reaction—what’s decomposing? Information.” You will find 6. Why did your instructor come around and tap on the test tube occasionally the template for this lab at during the heating process—what does this prevent from happening? the bottom of the list. 7. Where does the oxygen that is separated from the copper oxide go—what happens to it? 8. What were some possible sources of error in this lab (i.e. why didn’t you get exactly the same percentages as you calculated for the ideal data)? Rules for writing your lab report: MUST BE TYPED—hand-written reports will NOT be accepted double or 1.5-line spaced (no single spacing) MOST IMPORTANT: follow the format of this handout!!! 12 point “Times New Roman” or “Arial” or other normal font name, date, and period in top right-hand corner (like on a funsheet, for example) title: Empirical Formula of Copper (?) Oxide Lab (no separate title page, just make sure this title appears at the top of your 1st page) if more than one page (most likely, it will be), staple them together Mrs. Rigdon is looking for two main things: neatness and accuracy. Make sure your report has both! Due for 100% credit anytime during the week of 1/16/12. After that, -10 pts. per day. That means printed out and ready to turn in when you walk in the door sometime that week.