OPERATION & MAINTENANCE MANUAL FOR LAB-PURE 150 WATER PURIFICATION SYSTEM SIN - CAN INC. #3, 4015 - 1 STREET SE CALGARY, ALBERTA CANADA, T2G 4X7 Toll free 800-565-2345 Direct 403-565-2345 Fax# 403-287-1355 Email: sincaninc@telus.net Website www.sincaninc.com Revision 11-12-06 Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 1) System Description 2) Operational Procedures 2.1) RO Polished Water Withdrawal 2.2) Operational Notes 3) Maintenance Procedures 3.1) Service Schedule 3.2) Maintenance Procedures 3.2.1) Pre filter, Polishing and Final Filter Change 3.2.2) Reverse Osmosis Membrane Exchange 3.2.3) Pure D.I. Test Monitor 4) Trouble Shooting 5) Spare Parts Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 1) System Description Sin-Can Inc’s LAB-PURE line are designed to supply laboratories with cost-effective, reliable systems to produce RO polished water. The LAB-PURE systems are designed to produce RO water directly from city water supplies and will achieve a resistivity of greater than 5 megohm/cm (typically 10-15 megohm range) when properly operated and maintained. The water quality generated by the LAB-PURE systems are greater than ASTM Type II and NCCLS/CAP Type II water making the systems ideal for general laboratory use and for feed water to polishing systems, Aries and Gemini systems, for production of ASTM Type I water. This is water for HPLC, Cell culture, AA etc type applications. The LAB-PURE systems consist of a 10 inch pre filter PF1C-10 for the removal of chlorine, particulates and organics from the city water supply. In areas of high silt or dirty feed water supplies, the PNP2-20 pre-filter assembly is used. The SCMF005-20 AND SCMF001-20 PRE-FILTERS ARE USED IN THIS ASSEMBLY TO REMOVE SILT AND OTHER PARTICULATE DEBRIS. Water passes through the pre-filters to the booster pump that maintains a constant pressure on the reverse osmosis membrane ( TFC 150) where the water is separated into product water and reject water. Product water has approximately 98% of the inorganics and organics above 200 M.W. removed at this point in the process. Product water is sent to the storage tank for later polishing via the 10 inch polishing cartridge ( PC 2000 ) when water is required from the system. Reject water is sent to the drain from the system via the reject water line and needle valve (old units) or the pressure flow regulator that automatically sets the proper backpressure and reject to permeate ratios.(New models) System description continued…. The LAB-PURE system incorporates two pressure sensing devices which automatically shut off the booster pump when low pressure conditions are present and when the reservoir tank is filled. There is a solenoid valve located at the inlet of Pre Filter PF1C-10 that operates in conjunction with the booster pump and the automatic controls. It shuts off all flow to the system when the tank is full to avoid water wastage. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 2) Operational Procedures The LAB-PURE water purification systems come complete with all valves, fittings, reservoirs, filters and RO membranes and fully operational once they are installed. The system will automatically start and stop as water is required to maintain the reservoir tank in a filled condition. 2.1) RO Water Withdrawal -Place the pure water outlet line into an appropriate container and open the PC 2000 polishing cartridge outlet valve ( blue handled valve ) to take water from the system. - Depress the RED button on the PURE D.I. TEST monitor to determine if the water quality is good ( green lite on ) or poor ( red service lite is on ). - If water quality is good release the RED button and use the water as required. - When completed close the valve ( blue handled valve ) on the polishing cartridge PC 2000 to stop the flow of RO water. - If the PURE D.I. TEST monitor indicates a RED service light water quality has dropped below 2 megohms, close PC 2000 valve, ( blue handled valve ) service is required, go to Maintenance Section 3 of this manual. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 2.2) Operational Notes - While the pump is operating ( system reservoir is filling ) check the reject water line ( black tubing ) pressure regulator gauge. - Standard pressure setting should be approximately 80 psig on the reject water line pressure gauge. This pressure setting may vary between 70 and 90 psig. Reject flow rate should be in the 1000mls/min range - If the pressure is not within parameters adjust the reject water pressure by carefully adjusting the brass pressure regulator and observing the reject water pressure gauge to the correct value of approximately 80 psig. -New model Labpure 150 are not adjustable as the values are automatically set by the pressure/flow restrictor valve. -The RO system will automatically shut off when the reservoir Tank is full and the tank gauge is in the 60-65 psi range. -The RO system turns on automatically when water is taken and the Pressure gauge reads in the 30-40 psi range. - Reservoir is 12g (45L) capacity and the Labpure produces 150 gpd at temperature of 12oC and 80 psi. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 3) Maintenance Procedures Maintenance of your LAB-PURE water system is critical to its ability to produce high quality water for your laboratory’s operations. Failure to properly maintain the system will degrade the RO membrane, produce sub standard water or no water for your laboratory and may damage the Labpure 150 system. New cartridges should always be handled with gloves when removed from packaging to prevent contamination. 3.1) Service Schedule - Pre filter : PFC1-10 2 months ( depending on the quality of the feed water and particulate and organics composition ) its - Polishing : PC2000 Filter :( as indicated by the PURE D.I. TEST monitor, typically when the pre-filter is changed under normal operations) - RO Membrane : TFC 150 2 to 3 years when the permeate values fall significantly below the 150 gpd or the water quality deteriorates to less then 90 % rejection of the TDS levels in the feed water . continued: - Final filter ZEMSB020MMPS3 every 2 months. -Prefilters SCMF005-20 AND SCMF001-20 EVERY 2 MONTHS OR WHEN THE PRESSURE DIFFERENTIAL ON THE FILTER HOUSING IS 15 PSI. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 3.1) Service Schedule Pre-filter life will be affected by changes in the feed water quality that typically take place during spring breakup, heavy rains, snow melt down conditions. Also any current construction projects associated with the water supply system or city water supply in your local area, will require more frequent changes of the prefilter. The final filter is a 0.20 micron absolute filter for removal of any bacteria that maybe in the purified water stream leaving the system. The accepted standard is replacement every 2 months to prevent bacteria build up and pyrogen release from trapped bacteria in the filter membrane. The replacement will be at the discretion of the laboratory manager, to decide if the release of pyrogens into the purified water stream is important to the laboratory’s general operation. 3.2) Maintenance Procedure 3.2.1) Pre filter, Polishing and Final Filter change - Close city water feed by closing Pre filter valve on the Labpure 150 or the valve on the SCMF002-20/SCMF001-20 (REFERRED TO AS PNP2-20) filter housing. - Close reservoir valve. This is the ½” ball valve on the reservoir tank. - Disconnect power supply - Open Polishing cartridge valve PC 2000 ( blue handled valve ) to release system pressure. - Open the ball valve on the PNP2-20 bowl to drain the water and release pressure. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 3.2.1) Maintenance Procedure ( continued ) - Note: Hydrogen Peroxide is a hazardous solution, wear safety glasses, lab coat and gloves. Should skin contact occur flush with water immediately. Use standard 3% hydrogen peroxide for all procedures. - Unscrew the pre filter bowl, PF1C-10 and remove the filter. Rinse the filter bowl and interior of the upper housing with hydrogen peroxide. - Install a new pre filter element in the bowl and reattach to the system. - Unscrew the polishing filter bowl PC 2000 and remove cartridge. Rinse the filter bowl and interior of the upper housing with hydrogen peroxide. - Install a new polishing PC 2000 cartridge in the bowl (ARROW POINTING UP) and reattach to the system. Do not touch the cartridge with your hands as the dirt and oils from your hand will ruin the cartridge. Use gloves. - Unscrew the DemiCap final filter from the product outlet line. - Open the polishing cartridge valve PC 2000 ( blue handled valve ) - Open both the pre filter inlet valve. - Reconnect power supply - While holding the product outline where the final filter is located, open the polishing filter outlet valve PC 2000 ( blue handled valve ) and flush the system to drain. - Close polishing filter outlet valve PC 2000 ( blue handled valve ) and attach a new final filter element. Flush the final filter with 3-4 liters. Operation & Maintenance Manual for LAB-PURE Water Purification Systems 3.2.1) Maintenance Procedure ( continued ) - Open vent valves located on the side of the DemiCap final filter and open the polishing filter outlet valve PC 2000, ( blue handled valve ) flushing the air from the DemiCap final filter. When water appears at the vents, close the vent valves and the polishing filter valve PC 2000 ( blue handled valve ). - Open the reservoir valve ( blue handled valves or ½” ball valve ) - The system is ready for operation. - Check the Reject line pressure regulator and adjust pressure setting via the brass pressure regulator to approximately 80 psig on the gauge. Old systems. Done automatically on new models by the pressure/flow restrictor valve. 3.2.2) Reverse Osmosis Membrane Exchange - Close city water feed by closing Pre filter (PF1C-10 valve) OR valve on the PNP2-20 prefilter housing. - Close reservoir valve. This is the ½” ball valve on the reservoir. - Disconnect power supply. - Open Polishing cartridge valve PC 2000 ( blue handled valve ) to release system pressure. - Carefully remove inlet, permeate and reject lines from the RO membrane. ( These are slip connections, simply press the ring at the fitting end toward the fitting and pull the tubing out of the housing fitting. ) Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 3.2.2) Maintenance Procedure ( continued ) - Remove the RO membrane cartridge from its holder and install the new RO cartridge so that flow is in the same direction as before. - Carefully reattach the inlet, permeate and reject lines to the appropriate positions on the RO cartridge. - The slip fittings require that you push the tubing all the way to make a seal. - Close the polishing cartridge valve PC 2000. ( blue handled valve ) - Open the pre filter inlet valve on the PF1C-20 OR PNP2-20 HOUSING. - Remove the tubing from the pressure tank valve slip fitting ( blue handled valve closed ) and place to drain or open the drain valve on the reservoir tank. - Reconnect power supply. - Allow the system to flush for 20 minutes. - Carefully inspect the system for any leakage from the fitting. - Check the Reject line pressure regulator and adjust pressure setting via the brass pressure regulator to approximately 80 psig on the gauge. (Old Models) New models it is automatically set. - Disconnect the power supply and reconnect the pressure tank tubing to the blue handled valve at the pressure tank. - Open the pressure tank valve. ( blue handled valve ) - Reconnect the power supply. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 3.2.2) Maintenance Procedure ( continued ) - Procedure is now completed. 3.2.3) Pure Test D.I. Water Monitor - Generally located on the front of the LAB-PURE system, the D.I. Test Monitor contains a 9-volt battery that should be changed once per year. Purchase the battery from any local supplier and use a reputable manufacture. - Remove the D.I. Test monitor ( it is attached with Velcro ), carefully remove the back cover, disconnect and reconnect a new battery. Check to see that only the #7 switch is in the on position, all other switches should be in the off position. Replace cover, reinstall monitor and test the monitor by pushing the red button. Red light will go on indicating you have power. Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 4) Trouble Shooting. 4.1) Basic Check list: - Is the power to the unit connected and is there actually power at the outlet! - Is the water turned ON and is there actually any water at your location! - Is there adequate water pressure to operate the system 20 to 50 psig! - The system must be connected only to a COLD WATER system or room temperature D.I. systems, NOT HOT WATER! Check that there are no cross connection to a hot water system within the building. - Check that the pre filter inlet and reservoir tank valves are open. ( blue handled valves ) - Determine if the booster pump is operational by placing your hand on the pump when it should be in operation to feel for a slight vibration that indicates that the booster pump is functional. ( No vibration, no pump operation ) - No water flow from reservoir ( tank valves all open ) reservoir may have lost pressure check tank pressure gauge. Call SIN - CAN. - make sure that the final .22um Demi-cap filter is not Air-Locked. Open the vent ports on the side of the housing to remove the air. Close when finished. - All other problems call Sin-Can Inc. for assistance 1-800-565-2345 Operation & Maintenance Manual for LAB-PURE 150 Water Purification Systems 5) Spare Parts Component a) Catalog Number Pre-Filter Cartridges: - 5 micron prefilter SCMF005-20 - 1 micron prefilter SCMF001-20 b) Carbon Block filter PF1C-10 c) Polishing Cartridge: PC 2000 d) Reverse Osmosis Membrane: - 150 US gallons/day TFC 150 e) Final Filter or ZEMSB-020NN-PS3 ZEMSB-020-MM-PS3 f) Battery 9V ( Pure D.I.Test Monitor ) Purchase locally g) System booster pump. SCX2.