Electroceramics Laboratory (Jong-Sook Lee) http://myweb.jnu.ac.kr/~jongsook/ Professor Jong-Sook Lee finished her education at Seoul National University, Korea (B.S. in 1989, M.S. in 1991, Ph. D. in 1994 in Inorganic Materials Science and Engineering). After some postdoctoral career at the university and then at KIST, she joined the group of Prof. Dr. Maier at Max Planck Institute for Solid State Research, Stuttgart, Germany. She was selected for a fellowship from Alexander von Humboldt Foundation. After a two and half years stay in Germany she came back to join the Creative Research Initiative Center for Microstructure Science of Materials, run by Prof. Doh-Yeon Kim. Another two and half year work, also with a fruitful collaboration with MPI, Germany, she decided to go abroad again this time to National Institute of Standards and Technology, USA, hosted by Dr. S. Wiederhorn. After two years she flew over the Atlantic and rejoined the Prof. Maier’s group in Stuttgart, Germany, as staff scientist. During her stay she also served as Editorial Assistant in the Editorial board of the Journal Solid State Ionics. Since July 2006 she is the faculty member of School of Materials Science and Engineering, Chonnam National University, Gwangju, Korea. Through years devoted to many research projects in collaboration with major research institutes, industry partners, and other research groups from different universities and in campus, the Electroceramics Laboratory in JNU has gained a world-leading expertise in in-depth electrical characterization of materials (ionic conductors, mixed conductors, semiconductors, ferroelectrics) and the devices with those materials as key components (batteries, fuel cells, solar cells, transducers, MLCCs). What we investigate or are trusted with are often the issues long-time unsolved and suggested to be of a great scientific and technological importance. Research Interests: Electrical (conducting and dielectric) properties of electroceramics: solid electrolytes, semiconductors, and mixed conductors, dielectrics, ferroelectrics Impedance spectroscopy for energy and electronic applications Surface/grain-boundary effects in electroceramics Interface thermodynamics and kinetics Interface structure – property relationship Nanoscale effects in solid state ionics High-temperature versus low-temperature defect chemistry Application of electroceramics: solid oxide fuel cells, Li-ion batteries, ceramic sensors, catalysis, photoelectrochemical cells, solar cells, ceramic capacitors, ferroelectric devices Selected publications: Moving boundary diffusion problem for hydration kinetics evidenced in nonmonotonic conductivity relaxations of proton conducting perovskites, Solid State Ionics 272 (2015) 60-73 Photoelectrochemical Performance of ZnO Thin Film Anodes Prepared by Solution Method, Int. J. Hydrogen Energy, (2014) 20764-20770 Electrical Characterization of Polycrystalline Sodium "-Alumina: Revisited and Resolved, Solid State Ionics, 264 (2014) 22–35 Chemical Diffusivity for Hydrogen Storage:Pneumatochemical Intermittent Titration Techniques, J. Phys. Chem. C, 117 (2013) 19771-19785 Pneumatochemical Immittance Spectroscopy for Hydrogen Storage Kinetics, J. Phys. Chem. C,117 (2013) 19786-19808 A physicochemical mechanism of chemical gas sensors by an AC analysis, Phys. Chem. Chem. Phys. 15 (23) (2013) 9361-9374 A new diagnostic tool for the percolating carbon network in the polymer matrix, Polymer 54 (2013) 999-1003 Polarization mechanism of high temperature electrolysis in a NiYSZ/YSZ/LSM solid oxide cell by parametric impedance analysis, Solid State Ionics, 232 (2013) 80-96 Mixed Conduction in Ceramic Hydrogen/Steam Electrodes by Hebb-Wagner Polarization in the Frequency Domain, Fuel Cells 12 (6) 1070-1084 (2012) Effect of Crystallographic Anisotropy and Lanthanum Stoichiometry on Microstructural Evolution of Lanthanum Silicate Electrolytes, J. Am. Ceram. Soc. 95[8] 2439-2450 (2012) Nano Energy Laboratory (Jaekook Kim) Jaekook Kim(Dept. of Materials Science and Engineering, JNU) - Ph.D Materials Science & Eng.(with Outstanding Dissertation Award), The University of Texas at Austin, Texas, 1995-1997. - Title of Dissertation: Synthesis of Electrode Materials for Rechargeable Lithium Batteries by Oxidation-reduction Reactions in Solutions (Supervised by Prof. A. Manthiram). - M.S. Inorganic Materials Eng., Chonnam National Univ. Korea, 1989-1991. - B.S. Inorganic Materials Eng., Chonnam National Univ. Korea, 1985-1989. Research Feild Our group intensively pursues to explore the world of nanomaterials for a variety of technological applications. Chemical synthesis plays a critical role in accessing nanomaterials with desired morphology and microstructures. In specific, we are engaged in developing novel solution-based synthetic procedures to produce nanostructured metal oxides, alloys, and carbon. The nanomaterials synthesized are explored for electrochemical energy conversion and storage (batteries, fuel cells, and solar cells) and electronic applications. 1. Nanomaterials Synthesis Synthesis design greatly influences particle size/morphologies/distribution and hence remains critical to achieve materials with enhanced properties and performances though, in a variety of cases, equally vital factors as cost-effectiveness and fast synthesis favoring commercialization stands compromised. Our group pursues various synthetic techniques as polyol-based, Co-precipitation, Solvothermal, Hydrothermal, Sol-gel, Micro-emulsion, Spray Pyrolysis, and Microwave Assisted methods to develop nanomaterials for energy storage devices as Lithium-ion Batteries, Solar Cells, and Fuel Cells. 2. Energy Materials(Electrode materials for battery, Solar cell, Fuel cell) Rechargeable Li-ion batteries have hugely contributed as reliable power sources for modern day portable electronics and presently appear poised to influence high power applications as plug-in hybrid electric vehicles. With respect to Li-ion batteries, nano-sized electrodes have been intensively investigated for high power density applications as the advantage of using such electrodes remains two-fold. Firstly, nanomaterials provide a favorable structural framework that ensures shorter diffusion paths for the Li-ions to traverse from the core of the particles to the surface through the lattice, thereby yielding excellent electrochemical properties. Secondly, the large surface area of nanomaterials ensures enhanced electrode/electrolyte interfacial contact, thus leading to higher charge/discharge rates and good capacity retentions. We synthesized the following nano-structured electrodes as shown below: 3. Nano material Characterization Thermal Analysis, Rietveld Refinement, In-situ XRD, Ex-situ TEM, Ex-situ XPS, In-situ XAFS, Ex-situ 7Li Solid NMR, In-situ Mass Spectroscopy. Cathode Anode SELECTED PUBLICATIONS: - Vinod Mathew, Sungjin Kim, Jungwon Kang, Jihyeon Gim, Jinju Song, Joseph Paul Baboo,Wangeun Park, Docheon Ahn, Junhee Han, Lin Gu, Yuesheng Wang, Yong-Sheng Hu, Yang-Kook Sunand Jaekook Kim, “Amorphous iron phosphate: Potential host for various charge carrier ions”, NPG Asia Materials., 6, e138 (2014) Jungwon Kang, Vinod Mathew, Jihyeon Gim, Sungjin Kim, Jinju Song, Won Bin Im, Junhee Han, Jeong Yong Lee and Jaekook Kim,“Pyro-synthesis of a high rate nano-Li3V2(PO4)3/C cathode with mixed morphology for advanced Li-ion batteries”, Nat. Sci. Rep., 4, 4047 (2014). Jihyeon Gim, Vinod Mathew, Jinsub Lim, Jinju Song, Sora Baek, Jungwon Kang, Docheon Ahn, Sun-Ju Song, Hyeonseok Yoon and Jaekook Kim, “Pyro-Synthesis of Functional Nanocrystals”, Nat. Sci. Rep., 2, 946 (2012). Jungwon Kang, Sora Baek, Vinod Mathew, Jihyeon Gim, Jinju Song, Hyosun Park, Eunji Chae, Alok Kumar Rai and Jaekook Kim, “High rate performance in a Na3V2(PO4)3/C cathode by pyro-synthesis for sodium-ion batteries”, J. Mat. Chem., 22, 20857 (2012). Jinsub Lim, Vinod Mathew, Kangkun Kim, Jieh Moon, and Jaekook Kim, "OnePot Synthesis of Multi-Morphous LiFePO4 Nanoparticles in Polyol Medium", J. Electrochem. Soc., 158(6), A736 (2011). A. Manthiram and J. Kim, “Low Temperature Synthesis of Insertion Oxides for Lithium Batteries”, Chem. Mater., 10, 2895-2909 (1998). Jaekook Kim and Arumugam Manthiram, "A manganese oxyiodide cathode for rechargeable Lithium batteries", Nature, 390, 265 (1997). - - - - - SELECTED PATENTS: - J. Kim, “Method for preparing electrode material using polyol process, electrode material prepared thereby, and battery including the electrode material,” Korean Patent No. 10-1181323. Issued in 2012. J. Kim, “Anode material with high rate-capability and high capacity for lithium secondary battery and process for synthesizing the same,” Korean Patent No. 101134474. Issued in 2012. J. Kim, “Lithium batteries electrode and method for manufacturing the same,” Korean Patent No. 10-1117967. Issued in 2012. J. Kim, “Electrode material synthetic method using ultra fast combustion method and electrode material thereby,” Korean Patent No. 10-0999163. Issued in 2010. - - SELECTED AWARDS: National R&D Excellent Performance 100(Best performance TOP5), KISTEP, 2013. Best Paper Award, Korean Battery Society, 2013. Young Investigator Award, 16th International Meeting on Lithium Batteries, 2012. Best Paper Award, The 23rd Synchrotron Radiation User's Workshop & KOSUA Meeting, 2011. R&D 100 Award, R&D Magazine, 2009 (with Argonne National Laboratory) Yongbong Academic Achievement Award, Chonnam National University, 2008. Best Researcher Award, Chonnam National University, 2007. Best Dissertation Award, The University of Texas at Austin, Doctoral Convocation, May 20, 1998. Corrosion & Energy Materials Laboratory(Chan-Jin Park) http://myweb.jnu.ac.kr/~parkcj/ Corrosion & Energy Materials Laboratory is a group of researchers working in Department of Materials Science and Engineering headed by Professor Chan-Jin Park Dr. Park received his bachelor, master and doctoral degree in the area of Materials Science and Engineering from KAIST, then he was research associate in Institute for Physical Chemistry and Electrochemistry, Heinrich-Heine University Düsseldorf, Germany for 1 year. After that he worked at POSCO Research Institute as senior researcher. In 2005, he joined as faculty member in School of Materials Science and Engineering at Chonnam National University, where he initiated his independent academic career. From the starting of his research career, he has contributed to the building and reinforcing of department and enhancing the ranking of the university as well. Presently, his group comprises 15 active members including 2 postdoctoral researchers, 3 doctoral and 8 master students along with the other undergraduate students. Dr. Park has achieved recognition as a leader in the areas of corrosion, electrochemistry, energy storage and materials science. With excellent achievements, he has served as a Director of The Corrosion Society of Korea and Director of Korean Hydrogen and New Energy Society. Currently, he is working as an Editor of Metals and Materials International (SCI Journal). Moreover, Dr. Park has published over 80 SCI papers, patents and contributed numerously in national and international conferences. He has been invited to deliver seminars and lecture in various countries. Dr. Park is the recipient of several academic and professional honors and awards, including International Biographical Centre (IBC) “TOP 100 SCIENTISTS 2008”, “IBC Foremost Scientists of the World 2008”, Marquis Who's Who in the World (2008-2009), Marquis Who's Who in Science and Engineering (20082009), American Biographical Institute (ABI) “MAN of THE YEAR 2009”. His current research focuses on: Energy Storage & Conversion Materials Surface Treatments for Energy Materials Corrosion & electrochemical Techniques In particular, the research is intensively concentrated on rechargeable batteries, hydrogen storage materials, electro-catalysts, corrosion & protecting metals from corrosion. Research and Education training achievements: Education Training: Since the beginning, the corrosion and energy materials lab. has trained successfully 02 Ph.D and 20 M.S Scholars. Publications: 82 SCI papers (such as Adv. Func. Mater. Nanoscale, etc), several patents and plenty of national and international conference papers where the quality as well as the productivity is being enhanced. * Recent Representative publications 1. "Carbon-interconnected Ge Nanocrystals as an Anode with Ultra-long-term Cyclability for Lithium Ion Batteries", Advanced Functional Materials (2014) 2 "Facile and cost effective synthesis of mesoporous spinel NiCO2O4 as an anode for high lithium storage capacity", Nanoscale (2014) 3. "B2O3 added Lithium Aluminum Gernanium Phosphate solid electrolyte for LiO2 rechargeable batteries", Dalton Transactions (2014) 4. "Conducting, additive-free, amorphous GeO2/C composite as a high capacity and long-term stability anode for lithium ion batteries", Nanoscale (2015) 5. "Citrate gel synthesis of aluminium-doped lithium lanthanum titanate solid electrolyte for application in organic-type lithium-oxygen batteries", Journal of Power Sources (2015) Projects: Under Prof. Park’s supervision, the Corrosion & Energy Materials Lab have implemented successfully a lot of projects including the projects granted by Korean government and other industrial projects with highly practical applications which were financial supported by big companies in Korea such as POSCO, HYNDAI Motors etc. Annually, the Laboratory receives financial support from 3-5 projects independent or in collaboration. Facilities (Synthesis, Analysis and Manufacture): The Lab has grown as a modern global-extent laboratory with many purchased and collected modern instruments and manufacture facilities such as: 01 Won-A-Tech battery cycler with 40 channels 03 Electrochemical measurement instruments (02 Gamry potentiostat and 01 Zive) 02 Reaction chambers 03 Modern furnaces 02 Glove boxes 01 Salt spray chamber 01 TG-DSC/DTA instrument Other modern analysis instruments in common facility centers: SEM, TEM, XRD, XPS, FTIR … Clean Energy Technology Laboratory(Sung June Cho) http://cetl.jnu.ac.kr/ Prof. Sung June Cho Professor of Chemical Engineering, School of Applied Chemical Engineering, Chonnam National University, Yongbong 300, Gwangju 500-757, KOREA Contact Information - Tel : +82-62-530-1902 - Cell Phone : +82-10-3464-3528 - FAX : +82-62-530-1819 - E-mail : sjcho@chonnam.ac.kr Professional Preparation: - Korea Advanced Institute of Science and Technology, B. A., Chemistry 1992 - Korea Advanced Institute of Science and Technology, M. A., Chemistry 1994 - Korea Advanced Institute of Science and Technology, Ph.D., Chemistry 1997 Appointments: - Professor of Chemical Engineering, CNU - Associate Professor of Chemical Engineering, CNU - Assistant Professor of Chemical Engineering, CNU - Senior Researcher, Korea Energy Research Institute 2012 4. - present 2007 4. - 2012 3. 2003 1. - 2007 3. 1997. 5 - 2002.12 Awards: - Young Scientist Prize (International Association of Catalysis Societies) 2004 - Best Paper Award (IUMRS-ICA-2006) 2006 Recent Publications - Ik Jun Jang, Hye Sun Shin, Na Ra Shin, Su Hyun Kim, Su Kyum Kim, Myoung Jong Yu,Sung June Cho, “Macroporous–mesoporous alumina supported iridium catalyst for hydrazine decomposition” Catalysis Today 2012, 185, 198– 204 - Ja Hun Kwak, Russell Tonkyn, Diana Tran, Donghai Mei, Sung June Cho, Libor Kovarik, Jong H. Lee, Charles H. F. Peden, and János Szanyi “Size-Dependent Catalytic Performance of CuO on γ-Al2O3: NO Reduction versus NH3 Oxidation” ACS Catal. 2012, 2, 1432−1440 - Ja Hun Kwak, Do Heui Kim, Ja´nos Szanyi, Sung June Cho, Charles H. F. Peden " Enhanced High Temperature Performance of MgAl2O4-Supported Pt–BaO Lean NOx Trap Catalysts" Top Catal 2012, 55, 70–77 - Abdelaziz Rahy , Chen Zho, Jie Zheng a, S.Y. Park , Moon J. Kim , Ikjun Jang ,Sung June Cho, Duck J. Yang "Photoluminescent carbon nanoparticles produced by confined combustion of aromatic compounds" Carbon 2012, 50, 1298-1302. - Sunbum Kwon, Hye Sun Shin, Jintaek Gong, Jae-Hoon Eom, Aram Jeon, Sung Hyun Yoo, Im Sik Chung, Sung June Cho, and Hee-Seung Lee "Self-Assembled Peptide Architecture with a Tooth Shape: Folding into Shape" J. Am. Chem. Soc. 2011, 133, 17618–17621. About the Laboratory The Clean Energy Technology Laboratory, CETL was founded at Graduate School of Engineering in 2003. Energy related materials are the major objective of CETL starting from the synthesis to the application. The CETL maintained the state of art research facilities for the characterization of the materials and also the corresponding catalytic application. In 2010, the CETL was succeeded in the commercialization of the catalytic material for the propulsion system implemented in Korea Multi-purpose Satellites. Recent research interests are the synthesis and characterization of nano-structured materials for energy conversion and storage using X-ray absorption fine structure, solid nuclear magnetic resonance, transmission electron microscopy etc. Very recently, the CETL started the new research project for carbon dioxide capture and storage funded by KCRC. Major Interest: - Synthesis and characterization of nano-structured materials using X-ray absorption fine structure, solid nuclear magnetic resonance, transmission electron microscopy etc. - Structural determination using lab XRD or synchrotron XRD pattern with the Rietveld method for inorganic and microporous material. - Technology of energy conversion and storage using nano-structured material Current Research Topics - Structural investigation of nano-structured materials, zeolite, MOF, etc. and those catalytic and environmental application. - The state of art characterization technique for the polycrystalline structure using Synchrotron X-ray Powder Diffraction. Ongoing Research Grants - Material for Carbon dioxide capture and storage funded by Korea carbon dioxide capture and sequestration R&D center - Green propellant synthesis and characterization funded by Agency for Defense Development - Catalyst Granulation funded by LG Chemical Research Park. Synergistic Activities: - Principal researcher in 21st Century Frontier program funded by Korea Science Engineering Foundation, 2006-2008 - Researcher in Global Partnership Program funded by Korea Foundation of International Cooperation of Science and Technology, 2006-present. - Principal researcher in hydrazine decomposition technology for KOMSAT-[n] series: Catalyst development and testing for satellite attitude and altitude control, 2004-present. Energy Conversion & Storage Processing laboratory (Yun-Sung Lee), http://myweb.jnu.ac.kr/~leeys Energy Conversion & Storage Processing Laboratory is a group of researchers working in Department of Advanced Chemical Engineering headed by Professor YunSung Lee. In our laboratory, we currently performs a variety of research on lithium secondary battery, Capacitor, lithium-air batteries for the next-generation energy systems such as conversion of eco-friendly and energy-saving systems. Prof. Yun-Sung Lee is current working as Professor at Chonnam National University in Korea. He received his M.S from Chonbuk National University in 1998 and the research work was carried out about lithium secondary battery. He received Ph.D in 2001 in Applied Chemistry from Saga University in Japan under the direction of Prof. Masaki Yoshio. He joined in 2001 as a Post- Doctoral Fellow as Doctoral Researcher at Kanagawa University in Japan. He joined in 2003 at Chonnam National University as Assistant Professor. He has authored and co-authored over 150 peer-reviewed international publications including Chemical Review (IF = 45.661) and is an active member of the lithium secondary battery field. His research interests are in the fields of Li-ion battery, Li-air battery, and hybrid capacitor systems. Presently, his group comprises 7 active members including 3 doctoral and 4 master students along with the other undergraduate students. Research Interests: Synthesis and improving properties of electrode materials for lithium secondary batteries Development of solid electrolytes for all-solid-state batteries Development of electrode materials for lithium air battery Hybrid Capacitor system and development of electrode materials Selected publications: (155 papers) “Insertion type electrodes for non-aqueous Li-ion capacitors”, Chemical Review, 14(23), 11619-11635 (2014) (IF=45.661). “Constructing of high energy density supercapacitors from pinecone derived high surface area carbons”, ChemSUSChem, 7(5) 1435-1442 (2014) (IF=7.117). “A novel high-energy hybrid supercapacitor with an anatase TiO2-reduced graphene oxide anode and an activated carbon cathode”, Advanced Energy Materials, 3(11) 1500-1506 (2013) (IF=14.385). “Graphene-nanotube-iron hierarchical nanostructure as lithium ion battery anode", ACS Nano, 7(5) 4242-4251 (2013) (IF=12.033). “High performance hybrid capacitor with Li2CoPO4F cathode and activated carbon anode”, Nanoscale, 5(13) 5958-5964 (2013) (IF=6.739). “Flexible energy storage devices based on graphene paper”, Energy & Environmental Science, 4(4) 1277-1283 (2011) (IF=15.49). Facilities (Synthesis, Analysis and Manufacture): The Lab has grown as a modern global-extent laboratory with many purchased and collected modern instruments and manufacture facilities such as: Battery cycler Electrochemical measurement instruments Vacuum chambers Tube and box furnaces Glove boxes TGA/DTA instrument Above this, other modern analysis instruments in common facility centers: SEM, TEM, XRD, XPS, FTIR … Electrochemical Energy Materials Laboratory (Jeong Woo Yun) Electrochemical Energy Materials Laboratory is a group for researching on a variety of energy materials and its applications in School of Chemical Engineering. Professor Jeong Woo Yun, who is leading the group, received Ph.D degree in the Department of Chemical Engineering, University of Missouri, USA (2007). After the graduation, he joined in Laboratory for Transformation Fuels and Polymer Processing, Missouri University of Science and Technology in USA as a post-doctoral fellow. After 1 year, he came back to Korea and joined in Fuel cell Research Center at Korea Institute Science & Technology (KIST), Korea. In 2011, he joined as a faculty member in School of Applied Chemical Engineering, Chonnam National University, Korea. Dr. Yun is currently a member of the Society of the Korean Institute of Chemical Engineers, the Korean Electrochemical Society and the Korean Society of Industrial and Engineering Chemistry. Dr. Yun achieved recognition as a leader in the area of Solid Oxide Fuel Cells for electrochemical reaction, analysis of internal reforming, alternative electrode development, and fuel cell system. He is also renowned in the area of permeability analysis in ceramic bodies, supercritical fluids for binder extraction, plasma coatings for anti-corrosions, and a comprehensive process technology of biomass to hydrogen conversion. His emerging research group, currently, comprises 7 active members (5 master students and 2 undergraduate students) and they are researching on fuel reforming, alternative electrode development in SOFCs, plasma coating for heat exchangers, etc. Research Interests - Solid Oxide Fuel Cells (SOFCs) - Proton Exchange Membrane Fuel Cells (PEMFCs) - Alternative electrode materials development - Electrochemical catalyst developments - Internal Reforming in SOFCs - Analysis of carbon deposition and sulfur poisoning - Plasma coatings for hydrophilic and anti-corrosions and its applications - Interface thermodynamics and kinetics Research Facilities - Uniaxial presser, Impedance, DC loader, High temperature furnaces, Gas chromatograph, Reforming reactors, Button cell SOFCs test systems, Spot welder, Ball millings, ovens, etc. Selected publications 1. Seung Jin Lee, Jeong Myeong Lee, Yoon Gon Kim, Soon Do Yoon, Jeong Woo Yun*, “Thermal cycle development of PMMA pore former removal for honeycombtype SOFC supports” Ceramics International, 40, 4879-4887 (2014) 2. Jeong Myeong Lee, Yoon Gon Kim, Seung Jin Lee, Hee Su Kim, Sung Pil Yoon, Suk Woo Nam, Soon Do Yoon, Jeong Woo Yun*, “Carbon-tolerance effects of Sm0.2Ce0.8O 2-d modified Ni/YSZ anode for solid oxide fuel cells under methane fuel conditions” Journal of Applied Electrochemistry, 44, 581-588 (2014) 3. Jeong Woo Yun, Hyung Chul Ham, Hee Su Kim, Shin Ae Song, Suk Woo Nam, Sung Pil Yoon*, “Effects of the Sm0.2Ce0.8O2-d Modification of a Ni-based Anode on the H2S Tolerance for Intermediate Temperature Solid Oxide Fuel Cells” Journal of the Electrochemical Society, 160(2), F153-F161, (2013) 4. Jeong Woo Yun*, The Effect of Plasma Surface Treatment on a Porous Green Ceramic Film with Polymeric Binder Materials, Plasma Science and Technology, 15(6), 521-527 (2013) 5. Kug-Seung Lee, Song Jong Yoo, Yoon-Chae Nah, Hee Su Kim, Kyu-Sung Park, Jeong Woo Yun*, “Oxygen Reduction Reaction of Pt Supported on Y-Doped SrTiO3” Electrochemical and Solid-State Letters, 15(5) B61-B64 (2012) 6. Jeong Woo Yun, Sung Pil Yoon*, Hee Su Kim, Jonghee Han, Suk Woo Nam, “Effect of Sm0.2Ce0.8O1.9 on the carbon coking in Ni-based anodes for solid oxide fuel cells running on methane fuel” International Journal of Hydrogen Energy, 37, 43564366 (2012) 7. Sung Jong Yoo, Kug-Seung Lee, Seung Jun Hwang, Yong-Hun Cho, Soo-Kil Kim, Jeong Woo Yun, Yung-Eun Sung, Tae-Hoon Lim*, “Pt3Y electrocatalyst for oxygen reduction reaction in proton exchange membrane fuel cells” International Journal of Hydrogen Energy, 37, 9758-9765 (2012) 8. Jeong Woo Yun, Sung Pil Yoon*, Sang Gyun Park, Hee Su Kim, Suk Woo Nam, “Analysis of the regenerative H2S poisoning mechanism in Ce0.8Sm0.2O2-d coated Ni/YSZ anodes for intermediate temperature solid oxide fuel cells” International Journal of Hydrogen Energy, 36, 787-796 (2012) Polymer Energy Materials Laboratory (Chang Kook Hong) Prof. Chang Kook Hong Associate Professor, Department of Chemical Engineering, Chonnam National University Samsung Electronics (2004 ~ 2006) Postdoctoral Fellow, U. of Delaware, (2001 ~ 2003) Ph.D.: The University of Akron, USA. B. S.: Chonnam National University, Korea Research Interest Polymer Energy Materials Laboratory is devoted for nanomaterials synthesis and application towards low cost efficient solar cells, redox flow batteries, supercapacitors and polymer electronic materials. Solar cell In solar cell research, our laboratory focus on perovskite solar cells and polymeric flexible solar cells. Recently, we have achieved variety of composition of perovskite like MAPbI3, MAPbBr3, FAPbBr3 and FAPbI3 and successfully used for mp-TiO2, and low temperature processed 1D/3D hydrothermally grown TiO2 nanostructures having ~16% power conversion efficiency. Currently our research is focused on flexible perovskite solar cells and results are promising. Redox flow Battery Our group also focus on V2O5 based redox flow battery using graphene, polymer membrane and carbon felt. Supercapacitors: Graphene and r-GO based supercapacitors have been developed and tested successfully for energy storage applications. Selected publications: “Once again, organometallic tri-halide perovskites: Efficient light harvester for solid state perovskite solar cells”, Materials Today (2015) “Ultrathin Atomic Layer Deposited TiO2 for Surface Passivation of Hydrothermally Grown 1D TiO2 Nanorod Arrays for Efficient Solid-State Perovskite Solar Cells”, Chemistry of materials (2015) “Novel hybrid solar cells based on alpha-copper phthalocyanine-cadmium sulfide planar heterojunction”, Journal of materials science (2014) “Low-Cost Electrospun Highly Crystalline Kesterite Cu2ZnSnS4 Nanofiber Counter Electrodes for Efficient Dye-Sensitized Solar Cells”, ACS applied materials & interfaces (2014) “Synthesis and characterization of planar heterojunction hybrid polymer solar cells based on copper pthalocyanine (CuPc) and titanium dioxide”, Ceramics international (2014) “Successive ionic layer adsorption and reaction deposited kesterite Cu2ZnSnS4 nanoflakes counter electrodes for efficient dye-sensitized solar cells”, Materials research bulletin (2014) “Polyvinylpyrrolidone (PVP) assisted single-step synthesis of kesterite Cu2ZnSnS4 nanoparticles by solvothermal process”, Physica status solidi-rapid research letters (2013) Surfactant free most probable TiO2 nanostructures via hydrothermal and its dye sensitized solar cell properties, Scientific reports (2013) Facilities (Synthesis, Analysis and Manufacture): The Lab has grown as a polymer energy material laboratory with many purchased and collected modern instruments and manufacture facilities such as: Glove box with programmable spin coater Solar Simulator Modern furnaces Electrochemical work station Paste mixer Electrospinning VRFB testing cell Vacuum dry oven Chemical Hood High temperature nitrogen tube furnace Photonic and Electronic Thin Film Laboratory (Jin Hyeok Kim), http://pvsolar.chonnam.ac.kr/ Professor Jin Hyeok Kim received his bachelor, master and doctoral degree in the area of Materials Science and Engineering from KAIST, then he was research associate at UC Santa Babara, USA, and ISIR-Sanken, Osaka University in Japan. In 1999, he joined as faculty member at Chonnam National University. He is Permanent Member of the Materials Research Society of Korea and the Korean Ceramic Society. He is also General Affairs Director of the Materials Research Society of Korea. He has also served as Editorial Board Member of the Materials Research Society of Korea and EML Research Activities: Professor Jin Hyeok Kim is leading a very successful research group with an established international reputation for its work in chalcogenide thin films and functional metal oxides. The aim of the Lab is to improve existing thin film technologies and to develop low cost solar cells. Areas of research include: Fabrication and characterization of chalcogenide thin film solar cells by various methods. Fabrication and characterizations of TCO thin films. Synthesis of functional oxide materials by low cost hydrothermal synthesis method at 90 oC. Materials characterization using TEM. Planner light wave circuits (PLC) Quantum dot sensitized solar cells (QDSSC) More than 60 master students and 10 Ph.D. students are graduated. Currently 7 Ph.D. students and 3 Post doctorate students are working in the lab along with 12 mater students. Research Facilities: The full structure solar cell and device characterization in Lab allows students to study all aspects of the device performance. The facilities are as follows: Thin film fabrications: Physical method: RF and DC co-sputter, RF sputters (2), DC sputter, PLD, evaporator, metal sputter Chemical method: spin coaters (2), electro-deposition system, buffer deposition bath system Material processing: Several furnaces, RTA (rapid thermal annealing), Ion milling system (IMS), centrifuge, polishing machine for TEM, hot-injection, RTA for sulfurization and selenization of thin film precursors, CIP, ball milling, hot plate, agitator, water distiller Characterization: UV visible spectrometer, Solar simulator, XRD, Several furnaces, RTA (rapid thermal annealing), Ion milling system (IMS), centrifuge Research Highlights: Intensive research has been focused on the synthesis on CZTS thin film solar cells by various physical and chemical methods. Namely, sputtering, pulsed lased deposition, electrodeposition, SILAR, hydrothermal, hot injection and sol-gel In particular, we have achieved the photon conversion efficiency (PCE) of 9.24% for the sputtered CZTS absorber layer prepared from the metallic stacking and 4.5% by metal sulfide stacking. Our aim is to achieve CZTS thin film solar cells (TFSC) with PCE >10% for large area. Selected Publications: 1. Jin Hyeok Kim, Eun Mi Kim, David Andeen, Daniel Thomson, Steven P. DenBaars, and Fred. F. Lange, "Growth of heteroepitaxial ZnO thin films on GaN-buffered Al2O3 (0001) substrates by low temperature hydrothermal synthesis at 90oC," Advanced Functional Materials 17, 463-471 (2007). 2. S e u n g W o o k Shina,InYoungKimb,Gyoung Hoon Leeb, G.L.Agawaneb, A.V.Mohokarc, Gi-Seok Heod, Jin Hyeok Kimb,*and Jeong Yong Leea,**,“Design and grow th of quaternary Mg and Gaco-doped ZnO thin films with transparent conductive characteristics” Crystal Growth & Design 11 (11), (2011) 4819–4824 3. Uma Ghorpade, Mahesh Suryawanshi, Seung Wook Shin, Kishor Gurav, Pramod Patil, Sambhaji Pawar, Chang Woo Hong, Jin Hyeok Kim and Sanjay Kolekar, “Towards environmentally benign approaches for the synthesis of CZTSSe nanocrystals by a hot injection method: a status review”. Chemical Communications 50 (2014) 11258-11273 4. M. P. Suryawanshi, S. W. Shin, U. V. Ghorpade,K. V. Gurav, C. W. Hong, G. L. Agawane, J. H. Moon, Jae Ho Yun, P. S. Patil, J. H. Kim, A. V. Moholkar, “Improved photoelectrochemical performance of Cu2ZnSnS4(CZTS) thin films prepared using modified successive ionic layer adsorption and reaction (SILAR) sequence”, Electrochimica Acta 150 (2014) 136-145. 5. Seung Wook Shin, Woo Ri Bae, Jun Hee Han, K.V. Gurav, Hyo Rim Jung, M.P. Suryawanshi, P.S.Patil, Jeong Yong Lee, JinHyeok Kim, “Size and shape controlled hydrothermally synthesis of kesterite Cu2ZnSnS4 nanocrystals without toxic chemicals” RSC Advances 4 (2014) 32530-32533 6. Umakant M. Patil,Ji Soo Sohn, Sachin B. Kulkarni,Su Chan Lee,Hyung Goo Park,Kishor V. Gurav, J.H. Kim, and Seong Chan Jun, “Enhanced Supercapacitive Performance of Chemically Grown Cobalt–Nickel Hydroxides on Three-Dimensional Graphene Foam Electrodes,” Applied Materials & Interfaces, 6 (2014) 2450-2458, (2014.02) 7. M.P. Suryawanshi, P. S. Patil, S. W. Shin, K. V. Gurav, G. L. Agawane, M.G. Gang, Jin Hyeok Kim, A. V. Moholkar "The synergistic influence of anionic bath immersion time on the photoelectrochemical performance of CZTS thin films prepared by modified SILAR sequence" RSC Advances 4 (201404) 18537-18540 Functional Inorganic Materials for Energy Laboratory (Won Bin Im), http://fine.jnu.ac.kr Functional Inorganic Materials for Energy Laboratory is a group of researchers working in Department of Materials Science and Engineering headed by Professor Im, Won Bin. Dr. Im received his master and doctoral degree in the area of Materials Science and Engineering from KAIST, then he was research associate in Solid State Lighting and Energy Center, University of California, USA for 3 years. In 2010, he joined as faculty member in School of Materials Science and Engineering at Chonnam National University, where he initiated his independent academic career. From the starting of his research career, he has contributed to the building and reinforcing of department and enhancing the ranking of the university as well. Presently, his group comprises 12 active members including 1 postdoctoral researcher, 4 doctoral and 6 master students along with the other undergraduate students. Dr. Im has achieved recognition as a leader in the areas of designing new phosphors for white-LED by integrating Rietveld refinement, fabrication of high efficient white-LED using new LED structure, analysis on structure of ceramic materials using diffraction techniques (synchrotron, neutron, X-ray), energy storage and materials science. Dr. Im has published over 70 SCI papers, patents and contributed numerously in national and international conferences. He has been invited to deliver seminars and lecture in various countries. Dr. Im is the recipient of several academic and professional honors and awards, including, Outstanding Postdoctoral Research Achievement Award (2009), Marquis Who's Who in Science and Engineering (2011-2012). His current research focuses on: Designing of new phosphors for white-LED by integrating Rietveld refinement with experiments. Fabrication of high efficient white-LED using new LED structure. Novel synthesis technique, characterizing properties of nanoparticle materials used for white-LED. Development of new ceramic materials in view of crystal chemistry and physics. Analysis on a structure of ceramic materials using diffraction techniques (synchrotron, neutron, X-ray). Cathode/anode materials for battery application. Research and Education training achievements: Education Training: Since the beginning, the functional inorganic materials for energy lab have trained successfully 06 M.S Scholars. Publications: 74 SCI papers (such as ACS Appl. Mater. Interfaces, Scientific Report, Chem. Mater, etc), several patents and plenty of national and international conference papers where the quality as well as the productivity is being enhanced. * Recent Representative publications 1."Vapor-phase deposited conductive polypyrrole composite papers: effects of co-vapors", Scientific Report (2015) (accepted) 2 “Stacked quantum dot embedded silica film on phosphor plate for superior performance of white LEDs", ACS Appl. Mater. Interfaces (2014) 3. “Pyro-synthesis of a high rate nano-Li3V2(PO4)3/C cathode with mixed morphology for advanced Li-ion batteries” Scientific Report, (2014) 4. "Facile synthesis of electrospun Li1.2Ni0.17Co0.17Mn0.5O2 nanofiber, and its enhanced high-rate performance for lithium-ion battery applications", ACS Appl. Mater. Interfaces (2013) Projects: Under Prof. Im’s supervision, the functional inorganic materials for energy laboratory have implemented successfully a lot of projects including the projects granted by Korean government and other industrial projects with highly practical applications. Annually, the Laboratory receives financial support from 3-4 projects independent or in collaboration. Facilities (Synthesis, Analysis and Manufacture): The Lab has grown as a modern global-extent laboratory with many purchased and collected modern instruments and manufacture facilities such as: Nagano BTS 2004H battery cycler with 30 channels Electrochemical measurement instruments Reaction chambers Modern furnaces Glove boxes Photoluminescence spectroscopy with hand-made thermal controller UV-Vis spectroscopy Electroluminescence spectroscopy Quantum dot synthesis instrument Centrifuge Other modern analysis instruments in common facility centers: SEM, TEM, XRD, XPS, FTIR … Nano Photonic Devices Lab (Jun-Seok HA) http://npdl.jnu.ac.kr/ Nano Photonic Devices Lab. is a group for the research about nano devices and nano materials related with photonics and energy. Especially compound semiconductor materials are focused on for the application of Light Emitting Diodes, Solar Cells and Hydrogen Generation. Currently, 3 Ph.D. students, 4 master course students, and 3 undergraduate students are advised by Professor Jun-Seok HA. Professor Jun-Seok HA got his Ph. D. from Seoul National University, majoring in materials science and engineering in 2002. During his Ph. D. courses he visited Professor King-Ning Tu’s group in University of California at Los Angeles, USA for the joint research on microstructural investigation for electronic packaging. After graduation, he started to work for LG Electronics Institute of Technology, Seoul, Korea until 2006 as a chief research engineer. There, he worked for the development of novel LED devices. In 2006, he moved to Tohoku University, Sendai, Japan, as an assistant professor. During the period in Japan, he taught graduate students and researched the epitaxial growth of compound semiconductor. Also, he managed a Tohoku University Research Consortium for free standing bulk GaN which consisted of 5 international companies. In 2008, he joined the department of materials science and engineering of University of California, Santa Barbara USA, as a faculty staff. In UCSB, he also worked as a project scientist to manage LED research group under a guidance of Professor Shuji Nakamura who is a Nobel Laureate in physics, 2014. Since 2010, he is working as a faculty member in School of Applied Chemical Engineering at Chonnam National University, Gwangju, Korea. Professor Jun-Seok HA has published over 60 SCI papers, over 10 international patents and over 25 Korean domestic patents. Professor Jun-Seok HA is listed as a prominent researcher in several biographical dictionaries including International Biographical Centre (IBC), Marquis Who's Who for many years. Also, He is the recipient of Outstanding Research Achievement Award (2009) from SSLEC, UCSB. NPDL’s research fields are related with nano photonic devices and materials and their applications. Research topics are listed below. • • • GaN based Lighting Emitting Diodes (LEDs) : Epitaxial Growth, GaN on Silicon, Semipolar/Non-polar issues, Novel LED structure and process, Contacts, Simulation, and Thermal Managements Hydrogen generation by Photoelectrochemical reaction : Direct solar water splitting using compound semiconductor photo-electrode Hybrid LEDs and Solar Cells : Hybrid devices with Polymer/inorganic materials and its applications • • Graphene/Carbon Nanotube applications : Transparent Conductive Film application, Heat Dissipation Module, etc. Analysis of nano materials and nano photonic devices Selected publications: Enhanced Solar Hydrogen Generation of High Density, High Aspect Ratio, Coaxial InGaN/GaN Multi-quantum Well Nanowires, NANO ENERGY 12, (2015) 2211-2855 Effect of Double-Layered n-Type GaN on the Photoelectrochemical Properties in NaOH Aqueous Solution, JOURNAL OF THE ELECTROCHEMICAL SOCIETY 162, (2015) H19 - H22 Stress relaxation of GaN microstructures on a graphene-buffered Al2O3 substrate, PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS 8, (2014) 341 - 344 The effect of ITO/Mo/MoO3 anode multilayer film on efficient hole extraction in MEH–PPV/ZnO NP hybrid solarcells, CERAMICS INTERNATIONAL 40, (2014) 16281 – 16285 Effect of oxygen incorporation in a-plane GaN on p-type ohmic contact property, JAPANESE JOURNAL OF APPLIED PHYSICS 53, (2014) 090307(1) - 090307(2) The Effect of Rapid Temperature Annealing with N2 and H2 on Photoelectrochemical Properties of u-TiO2, JOURNAL OF THE ELECTROCHEMICAL SOCIETY 160, (2013) H800 - H802 Enhanced luminous efficacy in phosphorconverted white vertical lightemitting diodes using low index layer, OPTICS EXPRESS 21, (2013) 6353 - 6359 The polarization field dependence of Ti/Al based Ohmic contacts on Ntype semipolar GaN, APPLIED PHYSICS LETTERS 100, (2012), 091104(1) - 091104(3) Facilities: NPDL is possible for full line of cleanroom facilities as below. Especially, Chemical Vapor Deposition chambers (MOCVD, HVPE) are available for the growth of compound semiconductor materials. • • • Metal Organic Chemical Vapor Deposition Chamber Hydride Vapor Pressure Epitaxy Chamber Physical Deposition Tools : E-beam evaporator, PECVD, Sputter • • • • Etcher : Metal ICP-RIE dry etcher, Oxide Etcher, GaN ICP-RIE dry etcher Photolithography : Spin Coater, Mask Aligner, Baking facility Photoelectrochemisty Facility : Potentiostat P-4000, Xe-lamp, Temperature Dependent Hall measurement system etc. Other modern analysis instruments in common facility centers: SEM, TEM, XRD, XPS, Raman Spectroscopy, Photoluminescence system etc.