CHEM 108 Elementary Chemistry Syllabus and Lab Manual Spring 2006 Dr. Kristy Miller Department of Chemistry TABLE OF CONTENTS PAGE NUMBER Course Syllabus 3 Lecture Schedule 7 Laboratory Schedule 8 How to get the Most out of lab 9 Laboratory Evaluation / Equipment 10 Laboratory Procedures and Safety 11 Stockroom Procedures 16 Equipment Checklist 17 Laboratory Measurements 18 Molecular Models of Covalent Compounds 22 Stoichiometry 26 Rates of Reaction 30 Acetic Acid in Vinegar 33 Which Antacid Works Best? 36 Synthesis of Aspirin 42 Synthesis and Analysis of Soap 46 Chromatography 49 Enzyme Activity 53 Alcohol Fermentation 59 DNA Isolation 62 Appendix 1: Precipitation Diagram & Acid-Base Properties of Ions 65 Appendix 2: Acid-Base Properties Strength Chart 66 CHEM 108 ELEMENTARY CHEMISTRY Professor: Dr. Kristy K. Miller (B.S. and Ph.D.) e-mail: km123@evansville.edu Phone: 488-1077 Office: Koch Center 328 Office Hours: Monday 10:00 – noon Tuesday 8:00 – noon Wednesday 10:00 – noon Friday 10:00 – noon or by appointment (or just stop by) NOTE ABOUT OFFICE HOURS: Students are more than welcome to stop by anytime other than the listed office hours. HOWEVER, if office hours are not scheduled and the office door is closed, please come back another time! Class Time/Room: Lecture: Lab (A) Mon, Wed, Fri Tuesday 9:00 – 9:50 AM 7:00 – 9:00 PM KC 101 KC 338 Lab (B) Lab (C) Thursday Wednesday 7:00 – 9:00 PM 7:00 – 9:00 PM KC 338 KC 338 Description: (4) Considers fundamental concepts of chemistry, organic chemistry and biochemistry and their applications in science, technology and society. Prerequisite: Chemistry 100 or two semesters of high school chemistry. Text and Materials: Elements of General, Organic and Biological Chemistry (Ninth Edition) by J. R. Holum, John Wiley & Sons, Inc., 1995. Laboratory safety goggles. Calculator capable of handling numbers in exponential notation and take logarithms and antilogarithms of numbers. General Course Objectives: Specific 1. Gain factual knowledge such as terminology, methods, and an overall general understanding of general and organic chemistry and biochemistry. 2. Learn fundamental principles, generalizations and theories. Course Objectives: 1. To introduce some fundamental principles of general, organic chemistry and biochemistry, emphasizing the general and biochemistry material. 2. To illustrate the relevancy of chemistry in various areas of life. 3. To develop good laboratory techniques. Methods of Instruction: Classroom instruction will be primarily lecture and discussion. The laboratory periods will be used to give students “hands on” experience with material presented in lecture. Expectations and Responsibilities of Students: Students will treat the instructor and fellow students with respect by: 1. Thoughtful listening and interaction 2. Respecting others’ views which may differ from their own 3. Using appropriate language 4. Support the instructor’s ability to teach and other student’s ability to learn (THIS INCLUDES TURNING OFF ALL CELL PHONES!!!!!) Students will participate actively in the academic experience by: 1. Reading, understanding, and adhering to policies outlined in class syllabus 2. Attending class regularly and punctually 3. Taking responsibility for own learning by preparing for each class appropriately and completely 4. Contributing to class discussions 5. Adhering to the University Honor Code Registration/Withdrawal: Last day to register or add a course Last day to drop a course without a “W” Last day to withdraw with a “W” Attendance: Friday January 13 Friday January 20 Friday March 31 Attendance is required for all scheduled laboratory sessions and exams. NO MAKEUP EXAMS OR LABORAOTRY SESSIONS WILL BE GIVEN! Students who are required to miss an exam for a documented reason (such as an illness or university event), will be excused from that exam. A student’s score for that exam will be the average of the other hour exams and the final exam. Attendance is required for all labs. Labs cannot be made up. Data report forms will be collected at the beginning of the next laboratory period unless otherwise directed by the laboratory instructor. Late lab report forms, if accepted at all, will receive a lower grade. There are NO provisions for laboratory make-ups. Students who miss a laboratory for the same reasons given for missing exams, the student must contact the laboratory instructor. A student’s score on that particular laboratory experiment or quiz will be the average of the scores on all other experiments or quizzes. Homework: Homework will be collected and evaluated as announced by the instructor. Doing the assigned problems can only benefit you. Homework will account for 100 points of the final grade. Quizzes: There will be unannounced quizzes. Quizzes will be designed to be helpful in exam preparation. Quizzes will account for 100 points of the final grade. NO MAKEUP QUIZZES WILL BE GIVEN! Exams: There will be four exams. The exams will be weighted equally and account for a total of 400 points of the final grade. Exams will consist of a mixture of multiple choice, fill-in-the-blank, short answer, and essay questions. A majority of the test questions will be derived from (but not limited to) material covered in class lecture and discussion. Final Exam: There will be a comprehensive final exam. Two hours will be allowed for the examination. The final exam will be Tuesday, May 9 at 10:15 am. It will account for 200 points of the final grade Course Grades: Your grade will be based on the total points that you accumulate during the semester. Letter grades are not assigned to individual exams. Points can be accumulated through the work in the laboratory, on exams and quizzes, and on homework. The point scale is: Homework: Quizzes: Hour exams (4) Final exam: Laboratory: Total: Final Grades: Academic Honor System: A B C D F 90-100% 80-89% 70-79% 60-69% < 60% 100 100 400 200 200 1000 points 900-1000 total points 800-899 total points 700-799 total points 600-699 total points <600 total points Under this system, your submission of any work (e.g. exams, papers, lab reports, lab samples) implies that you have adhered to the Honor Code (which states: I understand that any work which I submit for course credit will imply that I have adhered to this academic honor code: I will neither give nor receive unauthorized aid nor will I tolerate an environment which condones the use of unauthorized aid). In other words, by turning in your work for credit you reaffirm your adherence to the Honor Code. As a general guideline, "unauthorized aid" includes work that is not your own and is not explicitly credited to the person who made or developed it. This work might include 1. answers to questions or problems 2. wording of concepts, descriptions or explanations 3. ideas or perspectives (in contrast to generally known facts or theories) 4. experimental data, products or interpretations 5. basically in summary, plagiarizing or copying any work that is not your own CHEAT (verb): to be dishonest or deceitful Therefore, sharing information on tests with fellow students is also a violation of the honor code. Cheating will not be tolerated in this class. Under most cases, a zero will be given and your name will be submitted to the Dean of Students and such action may be cited on your academic record. HOWEVER, collaboration with other students is not ruled out by this Code. Neither is the use of ideas or words of others. What is ruled out is such collaboration or use without explicit credit or acknowledgment being given. I invite your questions at any point where the Code or your responsibilities under it are not clear. Strong Statement Concerning Study Time: Students should be aware that a 12-18 credit hour semester amounts to a full time job. That is, the average student taking a 15 semester hour load is expected to spend about 30 hours per week in study and preparation outside of class and laboratory. On a Monday-Friday basis that amounts to 9 hours per day! Budget study time first, don’t put it off until the weekend. The University faculty have high standards. Students who make the commitment, can come up to those standards. CHEMISTRY 108 SPRING 2006 LECTURE SCHEDULE AND ASSIGNMENTS January 11 January 13 Introduction & Chapter 1 Chapters 1 & 2 Course Goals, Methods Measurements, Atomic Theory January 16 January 18 January 20 NO CLASS Chapter 2 Chapter 3 Martin Luther King Jr. Day Atomic Theory, Periodic Law Compounds January 23 January 25 January 27 Chapter 3 and 4 Chapter 4 Chapter 5 Bonds, Polarity and Chemical Equations, Moles Moles, Molar Concentrations Gas Laws January 30 February 1 February 3 Chapter 5 and 6 Chapter 6 Chapter 7 Kinetics and Water and Solutions Solutions Solutions and Acids, Bases, Salts February 6 February 8 February 10 Chapter 7 Chapter 22 Exam 1 Acids, Bases, Salts Radioactivity Chapters 1-6 and 22 February 13 February 15 February 17 Chapter 8 Chapter 8 and 9 Chapter 10 Acid- Base Chemistry Acid- Base Chemistry and Introduction to Organic Chemistry Organic-Alkanes February 20 February 22 February 24 Chapter 10 and 11 Chapter 11 Chapter 12 Organic-Alkenes, Alcohols Organic-Alcohols, Ethers and Amines Organic-Aldehydes and Ketones February 27 March 1 March 3 Chapter 12 and 13 Chapter 13 Exam 2 Organic-Ketones and Carboxylic Acids Organic-Carboxylic Acids Chapters 7-13 March 6 March 8 March 10 NO CLASS NO CLASS NO CLASS Spring Break Spring Break Spring Break March 13 March 15 March 17 Chapter 14 Chapter 14 and 15 Chapter 15 Intro to Biochemistry and Carbohydrates Biochemistry-Carbohydrates and Lipids Biochemistry-Lipids March 20 March 22 March 24 Chapter 21 Chapter 21 and 16 Chapter 16 Biochemistry-Nucleic Acids Biochemistry-Nucleic Acids and Proteins Proteins March 27 March 29 March 31 Chapter 17 Chapter 17 Exam 3 Enzymes Hormones and Neurotransmitters Chapters 14, 15, 21, 16 April 3 April 5 April 7 Chapter 18 Chapter 18 Chapter 19 Extracellular Fluids Extracellular Fluids Energy of Life April 10 April 12 April 14 Chapter 19 Chapter 19 NO CLASS Energy of Life Energy of Life Easter Recess April 17 April 19 April 21 NO CLASS Chapter 20 Chapter 20 Easter Recess Metabolism Metabolism April 24 April 26 April 28 supplemental supplemental Exam 4 Biotechnology Bioctechnology/Human Genome Project Chapters 17, 18, 19, 20 supplemental May 1 May 3 Review for final exam Reading/Study Day May 9 Comprehensive Final Exam, 10:15 am