UNIVERSITY COLLEGE LONDON Job Description Job Title: Research Associate Department: Chemistry Reports to Professor P F McMillan Grade: 7 The Project The overall project is supported by an award to Professor PF McMillan for synthesis and study of new materials via chemical routes under high pressure-high temperature conditions. This project will develop studies of metal nitrides and oxynitrides using large volume press and diamond anvil cell techniques combined with metal-organic chemistry syntheses. Characterisation of the new compounds will be carried out using optical spectroscopy and X-ray or neutron diffraction. The project will particularly develop the materials as new semiconductors for photocatalysis applications. Main Purpose The postholder will carry out research into (a) developing new chemical precursors and routes to new nitride materials using metal-organic chemistry techniques; (b) high pressure-high temperature treatment of the precursors to obtain new nitride and oxynitride compounds; (c) structural characterization of the new compounds using X-ray and neutron diffraction, including experiments at national and international synchrotron and neutron facilities; (d) characterization of the optical properties using spectroscopy techniques; (e) characterization of the chemical and photocatalytic properties of the new materials using standard tests for various aspects of photocatalysis; (f) development of technological properties of the new materials produced. Duties and Responsibilities To contribute to the development, design and application of organometallic chemistry routes to synthesize new nitride and oxynitride materials To design, develop and implement high pressure-high temperature synthesis routes to achieve new nitride/oxynitride materials and solid state compounds To characterize the new materials using optical spectroscopy and Xray or neutron diffraction, including in situ experiments under high pressure and high temperature conditions at national and international synchrotron and neutron sources To evaluate the chemical and photocatalytic properties of the new nitride and oxynitride materials To record, analyse and write up the results of these experiments, predictions and procedures on a regular basis for periodic inspection by the funding agency and for future reference. To contribute to the drafting and submitting of papers to peer reviewed journals. To prepare progress reports on research for funding bodies as required. To contribute to the preparation and drafting of research bids and proposals. To contribute to the overall activities of the research team and department as required. To undertake a limited amount of teaching in relation to subject area. To contribute to the induction and direction of other research staff and students as requested. Responsible for ensuring that equipment is safe and maintained in working order. As duties and responsibilities change, the job description will be reviewed and amended in consultation with the postholder. The postholder will carry out any other duties as are within the scope, spirit and purpose of the job as requested by Professor P F McMillan or the Head of Department. The postholder will actively follow UCL policies including Equal Opportunities and Race Equality policies The postholder will maintain an awareness and observation of Fire and Health & Safety Regulations. UNIVERSITY COLLEGE LONDON Department of Chemistry Person Specification for the Post of Research Associate Knowledge – including Qualifications Post Graduate Degree in chemistry, physics or materials science with an emphasis on experimental metal-organic and solid state synthesis as well as high pressure studies, combined with structure-properties characterisation of functional materials. (Essential) Applicant must demonstrate detailed knowledge of chemical synthesis especially applied to nitride and oxynitride materials, including organometallic precursor chemistry, sol-gel synthesis, nitridation methods, nanomaterials preparation, handling air- and moisturesensitive materials, and vacuum line techniques. (Essential) Skills Must have demonstrated ability to recognise and develop technologically relevant materials and processes through publication of patents etc as well as academic publications. (Essential) Basic research skills. (Essential) Ability to analyse and write up data. (Essential) Ability to present complex information effectively to a range of audiences. (Desirable) Effective written and verbal communication skills. (Essential) Experience Experience with high pressure-high temperature synthesis methods, and characterisation of structure and optical properties of materials using X-ray diffraction, Raman spectroscopy and other techniques. Characterisation of materials for photocatalysis applications. (Essential) Experience of working in a research environment. (Essential) Experience of multi-disciplinary working. (Desirable) Experience with all of the following: synthesis of solid state materials and chemical precursors using metal-organic chemistry routes, including sol-gel synthesis, nitridation, glove box and vacuum line techniques for handling air-/moisture-sensitive samples, characterisation of structure and optical properties of materials using spectroscopy and diffraction techniques. (Essential) Experience of working on technologically relevant materials and problems including developing patentable results as well as academic publications. (Essential) Personal Qualities Commitment to high quality research (Essential) Ability to work collaboratively and as part of a team (Desirable) TERMS AND CONDITIONS SALARY The post is graded as Grade 7, the salary for which ranges from £28,983 to £35,646 p.a. (excluding London Allowance of £2,795 p.a.) .Starting salary is usually £28,983. Please note, appointment at Grade 7 is dependent upon having been awarded a PhD; if this is not the case, initial appointment will be at postgraduate research assistant Grade 6 with payment at Grade 7 being backdated to the date of submission of the PhD. Progression through the salary scale is incremental. Cost of living pay awards are negotiated nationally and are normally effective from 1 st August each year. PROBATION Appointments are subject to receipt of satisfactory references and a probationary period of 9 months. HOURS OF WORK Full time hours for Research staff average 36.5 hours per week and times of work are as determined by the Head of Department. HOLIDAYS Annual leave is 27 working days for a full time member of staff. UCL also closes for a period at Christmas and Easter, at which times staff benefit from a total of 6 ´closure days´ in addition to Bank Holidays. PENSION The postholder will be eligible to join the Universities Superannuation Scheme, which is a final salary scheme with a current employee contribution rate of 6.35% and an employer contribution rate of 14% of salary. SEASON TICKET LOANS A season ticket loan is available to staff who have successfully completed their probationary period with the facility to repay through a monthly deduction from salary. OTHER BENEFITS Other benefits of joining UCL as a staff member are many and include: Access to an extensive range of in-house staff development opportunities. Staff have full use of the UCL libraries and UCL operates a Study Assistance Scheme for those undertaking part-time workrelated study. An excellent location for transport networks being near Euston, Kings Cross and St. Pancras stations and a choice of underground stations connected to London 's other mainline stations. A wide range of bus routes serves the area. UCL lies in Bloomsbury , just north of Oxford Street , Covent Garden and the heart of the West End with access to shops, theatres, cinemas, bars and restaurants. UCL also has its own 550 seat West End arts venue (Bloomsbury Theatre) which hosts drama, dance, music, debates and lectures during the year The main campus has subsidised cafeterias/bars and shops, gym and a travel agent. UCL staff can also benefit from corporate membership at a Tottenham Court Road gym. TO APPLY Apply online at: https://atsv7.wcn.co.uk/search_engine/jobs.cgi?owner=5041178&ownertype=f air&jcode=1179081 You will need to register to use the system if you have not used it before. and are able to do this after you have clicked on the 'Apply now' button at the bottom of the page. Please upload a full curriculum vitae, including research experience and scientific publication list when you apply. The closing date for receipt of applications is 11 March 2011 Thank you for your interest in this post and the Department of Chemistry at UCL