-1IRON AGE SMELTING AT MELVILLE Koppies Contents 1) Discovery 2) Origin of iron making 3) Types of furnaces 4) Bellows 5) Firing 6) Chemical process 7) Forging 8) Recent records of iron firings 8.1) Klaas’ firing 8.2) 1936 Empire celebration firings 8.3) Tshovote brothers 8.4) Wits experiments 1977 9) Black art 1) Discovery. Prof Revil Mason of the University of the Witwatersrand Archaeological Research Unit anticipated that there would be furnaces in the area because the ridges, from Linksfield to Northcliff, are rich in iron ore. This can be seen fromthe reddish colour of the shale, into which ferruginous fluids (iron rich) have seeped and coloured it red. Many of the furnaces have been built over, but the ones at Melville koppies had been saved because the Council bought the land in 1940s. The lecture hut was supposed to be built where the protected furnace and shed are now. A sharp eyed builder noticed a funny circular rim on the ground and contacted Wits. There were also slag pellets on the surface, which were a good indicator of a possible furnace A more recent furnace which had been at ground level had been swept away by erosion. Pottery sherds and slag were found banked up against the rim of the retaining rocks of the ridge Revil Mason began to dig there in 1963 (site 7/63) and found the furnace, dated 1050 AD. The furnace that was excavated probably had a dome-shaped roof with a chimney. The openings for the tuyeres may have been closed except for a circular opening for the tuyeres. Erosion may have washed away the dome and opened the sides openings more. The present shape is round with two openings for the tuyeres (blow pipes) Mason was also helped by the SA Defence Force, which was stationed at Auckland Park. They used mine sweepers to look for further sites but were unsuccessful. Aerial photos of the area were also not successful in revealing any more sites. -2Mason excavated two levels further down and found late Stone Age and Middle Stone Age artefacts. These are all kept in a providenced collection at Wits because MK cannot guarantee their security at the Koppies. However, donations of similar artefacts are in display on the furnace. The vandalized furnace on the lower northern slope was site 28/64. This is a much more recent one, probably 1860’s. Bone fragments, teeth, pottery sherds, slag, charcoal were found here. The remains of kraals to the north west of this furnace are still there but they are well concealed by the bushes in the area. This furnace was totally vandalized in 2000. The MKMC decided not to restore this one because of the expense. The upper furnace was also vandalized at the same time, but not so badly. The South African Ceramic Restorers repaired the upper furnace. The bill was R20 000 but they only charged the MKMC R2000 because it is a non-profit organisation. The cave, site 9/65 was excavated by J.D. Seddon in 1971. This was a shelter used by traders who brought grain and cattle from the south, Klipriviersberg, and traded with the metal makers of Melville koppies, Lone Hill and Panorama. They used the natural fault between the koppies, which Beyers Naude runs through, as a route. The cave area was declared a National monument because of the remains found there, viz. bone fragments of sheep, domestic fowls, birds, ostrich eggs, mice, hares. jackals, mongooses, dassies, Burchell’s zebra, buffalo, eland, kudu, steenbuck, blesbok, hartebeest, . 2) Origin of iron making. It probably started by accident in the Tigris-Euphrates area, the Fertile Crescent. A fire that was very hot may have had some iron ore in it. The molten lump could have been idly toyed with, beaten into a shape, and it’s properties discovered. The knowledge and skill was a closely guarded secret, but nevertheless it got passed on. It seems to have reached North Africa, and then traveled down south along routes to the west and east of the Rift valley. As the iron makers came, they brought with them their culture of crops and husbandry. Crops were millet, sorghum. Maize, or corn, was only introduced in the 1760’s, and the better nutrition it gave caused a population explosion, the same as happened in Europe during the agrarian revolution which preceded the industrial revolution. The iron makers seem to have traveled down the East Coast and fanned into the Transvaal as well. A site at Amamzimtoti is dated to 850A .D. and a site at Broederstroom in Gauteng is also dated to 850A.D. These earlier iron makers moved away, climatic change perhaps? And then another wave swept into the Transvaal later. In the northern Transvaal, Mapungubwe is dated to 1060 AD, and thereafter the iron sites in the Transvaal are all in the 1500s AD -33) Types of furnace. 1) Round furnace, domed with a chimney, with two openings for tuyeres. Melville Koppies 2) Oval domed furnace with chimney and two openings. Buispoort NW of Zeerust 3) Loole type. Round, domed, chimney with one opening from Loole in Phalaborwa. 4) Venda type. A cylindrical-shaped furnace with a wide chimney and three openings for tuyeres at equidistant intervals, i.e. 120* intervals Most of the furnaces are sunk into the ground, from 15cm deep to the equivalent of half of the furnace height. This was to prevent the walls from cracking during firing. Cracks would let in oxygen which would stop the smelting process. The furnace was prepared from anthills and clay. It was fired to dry it out before use. Some furnaces were lined with clay at the bottom, others were not. 4) Bellows. At Melville Koppies, smelters used bellows made of goatskin. The goat was skinned alive because it was believed that this helped the iron-making process. The skin was loosed at the hind quarters then dragged to the neck. The cut ends were neatly sewn together. A thin awn-like needle made tiny holes, just enough to pull the sinew thread through, so that no air could escape. The skin was bent and rubbed to make it flexible. Tannin bearing leaves or cattle dung were also rubbed into the skin to preserve it. The one end of the bag was firmly attached to a straight horn, eg cow horn, and this was inserted into the tuyere. The other end was attached by lashing with thongs to two sticks, which the smelter would open and close as a valve. The capacity of the bags was about 5l of water. A bundle of grass was put in the bellows to plump it out. The art of leather making of these bags is also lost. Further north, people used drum bellows. These are made from a hollowed out log and skin is attached over the rim. The skin is lifted up and down with a stick inserted through the skin and air is forced out of a hole in the drum. The availability of large trees favoured drum bellows. The goatskin bellows seem to have been superior even though they were more fragile. Women used drum bellows to make copper (a women’s’ metal). They stood in a circle and carried out a rhythmic dance while blowing. Women used straws to blow gold in a crucible over a fire. Gold was also a female metal but was only used for ornaments by royalty. The tuyeres were made out of clay by women -45) Firing. This is what probably happened. Charcoal was used to smelt the ore. The ratio of charcoal to ore was 1:10. At Melville Koppies they probably used the Acacia caffra and A. robusta. To make charcoal, cut down the tree and wait for it to dry. Then set the wood alight and when it forms coals, rake the coals out and bury them in sand to exclude the oxygen and so make charcoal. A slow burning charcoal is best. (Nowadays, exotic invaders are used to make charcoal) If no charcoal was available, it could be obtained by trading. One bag charcoal for one bag sorghum or, millet, grain, and after 1760, maize. A flux was also used to get the fire going. It was probably crushed quartz, regarded as ‘medicine’ to improve the extraction. Fat was also used. The iron ore was probably found in a few localities close to Melville Koppies i.e. the contorted banded iron stone beds along Jan Smuts Ave near Wits, and the squashed quartzite formation along the arboretum. The iron ore was broken into pigeon egg sized nuggets. The iron ore was probably haematite, which has a high ration of iron, or geetite or magnetite. There were other impurities in the iron ore as well! The fire was lit at about 4pm on a full moon night. Perhaps for visibility, or for omens. First a fire was made at the bottom of the furnace with some charcoal. When this was red-hot, alternate layers of iron ore nuggets and charcoal were dropped on top through the chimney, keeping the ratio of 1 part ore to 10 parts charcoal. Tuyeres were placed in the openings at an angle so the wind did not blow directly into the centre of the furnace, but was directed at the side so that the cold air swirled around the inside perimeter first and got warm. A team of smelters would work through the night. Each smelter had two bellows, which he would pump at up to 120 beats per minute. The smelters were kept hydrated with water and beer, brought by old women. Menstruating women were not allowed near the furnace as it was believed that it would jinx the process. The extraction of iron was seen as a birthing process, hence the womb-like shape of the furnace and the phallic shape of the tuyeres. A woman of child bearing age or a man whose wife was pregnant could not come near the furnace. The furnace could not give birth to iron at the same time as another human birth It took the charcoal from about two trees to do one firing, which might produce iron for a hoe head, spearhead, and a chisel or two. -56) Chemical process. The first chemical reaction to take place is the removal of one atom of oxygen from each oxygen molecule in the furnace and the bonding of C (Carbon) from the charcoal with one molecule of oxygen to form carbon monoxide. Heat + C + O2 = CO (+O which disappears) Then the carbon monoxide combines with the haematite to form iron crystals and carbon dioxide. CO + Fe2O3 = Fe2 + 3CO2 Sponge iron or bloom is iron crystals, slag, bits of unburnt charcoal and bits of iron ore. Slag is iron with lots of impurities. In modern blast furnace, slag is the scum which rises to the top of the molten iron. Tempering is heating and then fast cooling with water, oil or fat, to make the iron hard. Tempering with blood, urine, breast milk were believed to impart human qualities to the iron Annealing is heating and then slow cooling Melting is turning a solid to a liquid state. Smelting is a chemical process of extracting iron Forging is beating the iron into shape. Too much oxygen and the process stops. Too little oxygen and the process doesn’t start. The carbon content was difficult to control. Too much carbon and the result was cast iron which is brittle and not pliable enough for tools. Too little and wrought iron was produced. The right mix and the beating afterwards resulted in a type of steel, so the quality of some tools was very good. 7) Forging. Nuggets of iron from several smeltings were placed in a clay envelope to reduce the oxidation in the next firing. The clay envelope was then broken and the nuggets beaten and forged into the required shapes, e.g. hoe, chisel, pin, scraper spear head, arrow head. Microphotography of Iron Age tools shows that nuggets of varying carbon content were successfully laminated together -68) Recent records of Iron Age firings. There are very few written records of actual firings. 8.1) KLAAS ‘S FIRING (This account appears to be a myth. The temperatures reached in the furnaces were not likely to be high enough to melt the iron to a runny state) “ The Afrikaans naturalist, poet and author, Eugene Marais, had the privilege to have seen an expert iron smelter at his craft. This was sometime during the period 1907 to 1917 when Marais was stationed in the Waterberg district as Justice of the Peace. He was introduced to ‘old Klaas’, as he was known, by a farmer, Jan Nel. Klaas was also one of the last Vaal pense, the now extinct Transvaal Bushmen. Klaas lived in the Waterberg Middleveld on the watershed between the Magalakwena and the Palala rivers. His kraal was hidden away between huge boulders and thorn trees. His garden was about three hectares in extent. Crystal clear and ice-cold water emerged from a fountain between the rocks. Klaas was about 135cm (4.5ft) tall. He must have been very, very old, judging from the condition of his skin, which was 100% wrinkled. He had the widest and flattest nose Marais had ever seen, with a gigantic mouth, and monstrous lips. His head was abnormally big. He had broad shoulders, but poorly developed legs, which accentuated his outward-pointing feet. He wore a necklace from which were suspended various small tools – a strange pair of pliers, knife, snuff spoon, tweezers and a porridge spoon. On his back he carried a small bag containing a pipe and tinderbox, as well as a few extra tools. All these tools were hand-made, as could be seen from the marks of a stone hammer. He pointed out that the blade of his spear was fastened to the haft with wire, which he had made himself. As a youth, Klaas was a slave of a Mapela tribesman, from whom he learnt the art of iron smelting. It is interesting to compare Klaas’ technique with that of the Tshvote brothers. Klaas’s furnace was built against a huge rock. It was of the Loole type and consisted of a clay chimney about one metre tall. The ore consisted of reddish pebbles mixed with earth of the same colour. This was mixed in a carefully measured ratio with powdered glassy quartz, which was the flux. The fuel was charcoal made from a specific tree. Thick branches were ignited in a sandpit and then quenched with sand after one hour. The ore was mixed with the charcoal in a specific ratio, and packed in the furnace on a layer of dry dung. Through a 10cm diameter hole at the base, the charge was lit. The hole was then closed with wet clay. Klaas’ twelve-year-old son operated the bellows, which consisted of two goatskins stitched together with sinew. A clay pipe connected the bellows to the furnace. -7The smelting was a tedious process. Every now and then charcoal or ore-flux mixture had to be added through the chimney. In the meantime, Klaas showed his visitors his tools. The anvil was a smooth black rock. The hammers were fashioned from stones made of a white sandstone which “came from very far”, and which Klaas considered as treasures. But the greatest treasure of all was the wire making tool, which consisted of an iron plate 18cm by 10cm by 2.5cm in dimensions with holes of various diameters. Klaas inherited this tool from hid Mapela master. It was passed down from one generation to the next, and must have been hundreds of years old, judging from its degree of wear. How the holes were made through such thick metal was a mystery, which even Klaas could not guess at. Unfortunately Klaas did not give a demonstration of wire-making, but he told his visitors that the red hot wire, as it is drawn through the hole and wound round a stick, must be tempered in a grass fire and then coated with lizard fat, which was the only compound capable of preventing brittleness. (Perhaps copper wire for ornaments and fastenings??) Klaas then produced a bag containing magic powder. This was made from a very special type of stone, and was essential to lower the viscosity of the molten iron to nearly that of water. In front of the clay-covered hole, Klaas made a mould of a pickaxe in moist sand. Everything was carefully measured off using a long stick with notches. The boy was then instructed to renew his efforts with the bellows. The sweat poured down his naked body and he panted for breath. As Klaas added the magic flux, an unbearable stench of hydrogen sulphide emerged from the chimney. Klaas said this was a good sign. He then took a sharpened stick, and with one deft movement, pierced the clay hole. The boy jumped out of the way, dragging the valuable bellows with him. Witha dull rumble, a pure stream of white-hot iron emerged from the furnace and flowed into the mould, sparks flying. Klaas’ measurements were exact. Not a drop of metal was wasted. A thin layer of moist sand was spread over the red-hot pickaxe, and then water blown over it by mouth. This was to temper the metal. After cooling, the pickaxe was finished off using hammer and anvil. Klaas admitted that the “white man’s pick-axe” which had a hole for the haft was superior to his product, which had a peg which must pass through the haft. Klaas was famous throughout the north, and he must have been a true metallurgical genius to have been able to produce molten iron with apparently little effort. Sometime later, Klaas spent two weeks with Marais, who recorded that Klaas was an absolute treasure house of knowledge. POSTSCRIPT. In our old uncle Pierneef’s collection on the farm Rietvlei, district Lydenburg, there is a hand made axe as described above, which was unearthed during ploughing operations. What a treasure that is! (Unfortunately the article I have has no author) 8.2) 1936 firing demonstration for the Empire Celebrations. Unfortunate, no record was kept of this firing! -8- 8.3) Tshovhote Bothers Two half brothers, Piet and Andries Tshovhote, who still practiced as blacksmiths and whose father was an iron smelter, were prepared to demonstrate the whole process as far as they remembered it. The demonstration included the mining of ore, the building of the furnace, the making of the bellows and tuyeres, the burning of the charcoal, the smelting process itself and the erection of a typical Venda smithy. They used cape beech (Rapanea melanophloeos), water berry (Syzigium garrardii) and wild syringa (Burkea africana) to obtain charcoal. The highest temperature reached was only 1140 degrees C. No sponge iron was present. This demonstration showed that the art of iron making has been lost. It was not a primitive art at all, but a highly specialized technique which is far more complicated than most authors make it out to be. 8.4) Wit’s experiments 1977 A study of prehistoric metal technology was part of the experimental research programme of the Archaeological Research Unit at the University of the Witwatersrand. Revil mason, Dr Heinrich Friede, Robbie Steel were some of the researchers involved. In their conclusions, they found that the raw materials, airflow system, temperatures, gas composition varied very much from batch to batch of sponge iron. Success or failure depended largely on the aptitude, training and experience of the operators. The researchers were only able to forge small pieces. The more complicated forge-welding techniques that the African smiths used when making large implements could not be reproduced. The researchers found that they could not get the layers to forge together. (Photomicrographs were taken of original Iron Age implements. These photographs revealed the lamination process of making implements. It also revealed the different chemical composition of the layers. Nuggets of iron from several firings in the smelting furnaces were heated in a forge and then laminated together by beating) “The smelting and forging of iron were complicated processes, and it is much to the credit of the smelters of that time that they could turn out, with the simple means available to them, relatively uniform, high-grade products in quantities sufficient for their needs.” (Acknowledgements to Mason who initiated the project, the Human Sciences research Council who subvented it, the Research laboratories of the SA Iron and Steel Corp, Steele and H.Toch of the National Institute for Metallurgy and others. Journal of the South African Institute of Mining and Metallurgy June 1977) 9) Black art In the early days of iron making in Europe it was called the ‘Black art”. There were two possible reasons; the smiths got very dirty from the charcoal. Secondly, the art was so secret and the firings so attuned to a specialist ‘feel’ that only experts could produce iron. -9Because there were so many factors that could influence the outcome, the smelters tried to eliminate known problems. According to Credo Mutwa, menstruating women were not allowed near the firing because the iron had to be pure and they could contaminate it. Only old women who were not menstruating could attend the smelters during the smelt. Men who had had sex the night before and men whose wives were pregnant could not attend the smelting either because a person could only give birth to one offspring. The production of iron was a birthing process. Once the iron bloom had been obtained, the next process of forging could take place in the kraal where women were, because this was not a magical process. He said that body fluids, eg urine, breast milk, were sometimes also used to anneal the iron tools and to give them strength. Iron was considered a ‘male’ metal. In modern day iron making, computers are used to regularly test the chemical composition of the iron and to test the tensile strength etc. It is still an art, but technology is there to assist. The so-called very complicated ‘primitive’ art of iron making has been lost. The demand for this iron fell after iron goods from Europe flooded South Africa in the 19th Century. Gradually the art died out, as there was less and less demand. Compiled by Wendy Carstens from various sources 2003 (Papers by H.M Friede, R. Mason, U.S Kusel, R.H. Steele and other papers without authors)