Supported catalysts Co3O4/α-Al2O3 synthesis using Co3O4
nanoparticles
Mendeleyev University of Chemical Technology of Russia, Moskva, Miysskaya
pl. 9
Yarovaya Oksana Viktorovna. Dotsent kafedri kolloidnoi ximii
Mendeleyev University of Chemical Technology of Russia, Moskva, Miysskaya
pl. 9; e-mail: Y_O_V@yahoo.com
Mostovaya Uliana Leonidovna. Inzheher kafedri kolloidnoi ximii
Mendeleyev University of Chemical Technology of Russia, Moskva, Miysskaya
pl. 9; e-mail: ylyana.m@gmail.ru
Nazarov Viktor Vasilevich
Zavedyyushchii kafedroi kolloidnoi ximii
Mendeleyev University of Chemical Technology of Russia, Moskva, Miysskaya
pl. 9; tel/ +7 (499) 978-60-10; e-mail: nazarov@muctr.ru
Keywords: nanoparticles, Co3O4, DLVO theory, heteroadagulation, catalyst
Abstract: The possibility estimation of synthesized Со3О4 sol particles
heteroadagulation on the surface of support (α-Al2O3) was accomplished via
DLVO theory. The calculation results were verified by experiments. Test samples
were synthesized and investigated, they demonstrated high catalytic activity.
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fabrication of Co3O4 nanorods and application to the degradation of phenol //
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Preparation of sodium fluorosilicate by soda method
T.V. Sharipov, D. I. Shayachmetov, A.G. Mustafin
Bashkir state university
Sharipov Tagir Vildanovich
Bashkir State University. Lead Engineer, Cathedra of Physical Chemistry and
Chemical Ecology. Address: 450076, Ufa, Zaki Validi st. 32. Chemical Faculty.
Tel. (347) 273-66-32. E-mail: tag1957@mail.ru.
Shayakhmetov Dim Idelovich
Bashkir State University. Postgraduate. Cathedra of Physical Chemistry and
Chemical Ecology. Address: 450076, Ufa, Zaki Validi st. 32. Chemical Faculty.
Mustafin Ahat Gazizyanovich
Bashkir State University. Professor, Doctor of chemical Sciences, Head of
Department of Physical Chemistry and Chemical Ecology. Address: 450076, Ufa,
Zaki Validi st. 32. Chemical Faculty. E-mail: mag@anrb.ru
Key words: fluorosilicic acid, fluorosilicate sodium, sodium carbonate, caustic
soda, sodium fluoride.
Abstract. The paper describes a process of production of sodium fluorosilicate
from fluorosilicic acid by soda method in presence of sodium fluoride, obtain the
decomposition estimated amounts of the fluorosilicic acid with an opportunity to
produce easily filtered premium product with a low impurity content of silica.
References
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[Phosphate fertilizer complex technology]. Moscow: Khimiya, 1987, 464 p.
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pererabotke fosfatnogo syrya [Production of fluoride in the processing of
phosphate raw materials]. Moscow: Khimiya, 1982, 244 p.
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its inorganic compounds]. Moscow: GSTCL Publ., 1956, рp 401-403.
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5. Poluchenie neorganicheskikh ftoridov pri pererabotke fosfatnykh rud
[Preparation of inorganic fluorides in the processing of phosphate minerals]. Trudy
NIUIF. Issue 261. Moscow: Lab. STI. 1991, 238 p.
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7. Golyakov L.I., Babkin V.V., Zagudyaev A.M. Patent SU 1659358. Method for
producing sodium fluorosilicate. C01B33/10, 1991.
8. Sharipov T.V., Mustafin A.G. Patent RU 2356835. Method for producing
sodium fluorosilicate. C01B33/10, 2008.
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fluoride containing compounds. C01B33/10, 2000.
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for producing sodium fluorosilicate. C01B33/10, 2000.
11. Sharipov T.V., Mustafin A.G., Shayakhmetov D.I. Patent RU 2492142.
Method for producing sodium fluorosilicate. C01B33/10, 2013.
Synthesis and colloid-chemical properties of hydrosols oxygenated
compounds of aluminum and zinc
Belova I.A., Malova A.V., Marchenko I.N., Kienskaya K.I., Zilina O.V.
D.Mendeleev University of Chemical Technology of Russia
Belova Irina Alexandrovna
MUCTR . D.I. Mendeleev , docent of colloid chemistry
Address: 125047 , Moscow A- 47, Miusskaya, 9 .
Tel. slave. : +7( 499) 978-56-70
e-mail: irinabelova@yandex.ru
Kienskaya Karina Igorevna
MUCTR . D.I. Mendeleev , docent of colloid chemistry
Address: 125047 , Moscow A- 47, Miusskaya, 9 .
Tel.rab . : +7 ( 499) 972-44-38
e-mail: sonoio@mail.ru
Malova Anastasia Valerievna
MUCTR . D.I. Mendeleev, colloid chemistry graduate student
Address: 125047 , Moscow A- 47, Miusskaya, 9.
e-mail: mlvanastasija@yandex.ru
Marchenko Ivan Nikolaevich
MUCTR . D.I. Mendeleev, colloid chemistry graduate student
Address: 125047 , Moscow A- 47, Miusskaya, 9.
Tel.rab.: +7(495) 609-6044
e-mail: i_marchenko@krost.net
Olga Zilina
MUCTR D.I. Mendeleev, docent of colloid chemistry
Address: 125047, Moscow A- 47, Miusskaya, 9.
Tel. slave. : +7 ( 499) 978-56-70
Keywords: hydrosols, aluminum, zinc, mixed systems
Abstract. Two methods of synthesis of aggregative stable hydrosol oxygenates
Al3 + and Zn2 + were developed. Basic colloid-chemical characteristics of the
hydrosols, namely particle size, pH range of aggregate stability, the concentration
of the dispersed phase are studied. The optimum molar ratio of precursor was
selected.
References
1.
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mezhdunarodnoj nauchnoj konferencii «kinetika i mehanizm kristallizacii.
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807.
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pri povyshennoj temperature // kolloidnyj zhurnal. – 2010. – t. 72. – №6. – s. 748 –
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Kuzovkova A.A., Bolshakov A.P., Kalmykov A.G i soavt. Vliyanie uslovij
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The improvement ways of 1,1-diamino-2,2-dinitroethene obtaining
process from 6-hydroxy-2-methylpyrimidine-4(3H)-one and 2methoxy-2-methylimidazolidyne-4,5-dione
Kushtaev A.A.*, Yudin N.V., Zbarsky V.L., Zhilin V.F.
Mendeleev University of Chemical Technology of Russia
Kushtaev Alexander A., D. Mendeleev University of Chemical Technology of
Russia; engineer,+7(495) 496-68-16, e-mail: kushtaev@mail.ru
Yudin Nikolay V., D. Mendeleev University of Chemical Technology of Russia;
candidate of chemical science, docent;+7 (495) 496-68-16, e-mail:
yudinnik@gmail.com
Zbarsky Vitold L., D. Mendeleev University of Chemical Technology of Russia;
candidate of chemical science, docent; +7(495) 496-68-16, e-mail: vlziy@mail.ru
Zhilin Viktor F.; D. Mendeleev University of Chemical Technology of Russia;
doctor of chemical science, professor; +7(499) 978-49-52, (495) 948-54-62, e-mail:
zhilin@muctr.ru.
Keywords: 1,1-diamino-2,2-dinitroethene, kinetics, nitration, hydrolysis.
Abstract. The nitration kinetics of 6-hydroxy-2-methylpyrimidine-4(3H)-one and 2methoxy-2-methylimidazolidyne-4,5-dione has been investigated in sulfuric-nitric
acid mixtures. The hydrolysis kinetics of 2-(dinitromethylene)-5,5-dinitropyrimidine4,6(1H,3H,5H)-dione and 2-(dinitromethylene)-imidazolidyne-4,5-dione has been
studied in a wide interval of medium acidity. The kinetic data have been confirmed
with the series of preparative experiments. The solubility of 2-(dinitromethylene)5,5-dinitropyrimidine-4,6(1H,3H,5H)-dione and 2-(dinitromethylene)-imidazolidyne4,5-dione has been determined in sulfuric acid and sulfuric-nitric acid mixtures. This
results can be used for creating of 1,1-diamino-2,2-dinitroethene technology.
References
1. Ilin V.P., Kolganov Ye.V., Smirnov S.P., Kozhevnikov V.G., Yevstigneev M.Ye.,
Pechenev Yu.G. Analiz sostoyaniya razrabotki malochuvstvitelnykh vzryvchatykh
sostavov v nashey strane i za rubezhom. Sbornik dokladov (soobshcheniy) III-ey
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(soobshcheniy) III-ey Mezhotraslevoy nauchno-tekhnicheskoy konferentsii
«Aktualny problemy i perspektivy razrabotki malochuvstvitelnykh energeticheskikh
materialov i izdeliy ponizhennogo riska», Rossiya, Dzerzhinsk, FGUP «GosNII
Kristall»», 2004. S. 34-38.
3. Bellamy A.J. FOX-7 (1,1-Diamino-2,2-dinitroethene). Struct. Bond – 2007. – 125.
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osnovnye svoystva. Materialy konferentsii «Sovremennye problemy tekhnicheskoy
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organicheskoy khimii, 2001, t. 37, vyp.5. S. 766–770.
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Wellmar U. 2001.
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6-gidroksi-2-metilpirimidin-4(3N)-ona i 2-metoksi-2-metilimidazolidin-4,5-diona.
Zhurnal prikladnoy khimii. 2009, t. 82. vyp. 10. S. 1633 – 1639.
8. Chylek Z., Cudzilo S., Diduszko R.R. Optimitization of 1,1-diamino-2,2dinitroethane. Biul. WAT (Poland). 2004, v. 54, n. 5–6. P.633–634.
9. Bellamy A.J., Latypov N.V., Goede P. Proceedings of the VII Seminar «New
trends in research of energetic materials». Studies on the nitration of new potential
precursors for FOX-7. Czech. Republic, Pardubice, 2004. P. 74-81.
10. Orlova Ye.Yu. Khimiya i tekhnologiya brizantnykh vzryvchatykh veshchestv. //
L.: «Khimiya», 1973. - 688 s.
11. Johansson M., Latypov N.V., Holmgren E., Sizova E.V., Sizov V.V., Bellamy
A.J Proceedings of the X Seminar «New trends in research of energetic materials».
On the synthesis of 1,1-diamino-2,2-dinitroehene (FOX-7) by nitration of 4,6dihydroxy-2-methylpyrimidine. Czech Republic, Pardubice, 2007. P. 183-191.
12. www.sigmaaldrich.com.
Denitration of spent sulphuric acid dicaroxylic acids
Kim P.P., Komarov V.A., Pastukhova G.V., Peretrutov A.A., Chubenko M.N.
Nizhny Novgorod State Technical University n.a. R.E. Alekseev
Kim Pavel, doctor of technical sciences, professor; e-mail: lab202@
dfngtu.nnov.ru
Komarov Vafa, Ph.D, docent; e-mail: lab202@ dfngtu.nnov.ru
Pastukhova Galina, Ph.D, docent; e-mail: lab202@ dfngtu.nnov.ru
Peretrutov Anatoliy, Ph.D, docent; e-mail: lab202@ dfngtu.nnov.ru
Chubenko Mariya, Ph.D, docent; e-mail: lab202@ dfngtu.nnov.ru
Keywords: denitration, spent sulfuric acid, dicaroxylic acids.
Abstract. The process of denitration of spent sulphuric acid dicaroxylic acids. The
possibility of reducing the content of nitrogen compounds in the acid less than 10 -4
%.
References
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gases and liquids], L.: Himija, 1982. 592 р.
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kisloty [The method of purification of spent sulphuric acid] Kim P.P., Peretrutov
A.A., Pastuhova G.V. i dr.// Zajavl. 27.03.91 Zaregistrirovano 23.10.92
Thin-film coatings based on highly filled syntactic foams
with siloxane bonds
Chukhlanov V.Y., Kriushenko S.S.
Vladimir State University named after Alexander and Nikolay Stoletovs
Chukhlanov Vladimir, professor, chair of chemical technology, e-mail:
vladsilan@mail.ru
Kriushenko Sergey, post graduate student; e-mail: sergey.kriushenko@yandex.ru
Keywords: Syntactic foams oligodimetilsiloksan, tetraethoxysilane, binders, thinfilm coating.
Abstract: The article discusses the modes produce thin coatings on the basis of
syntactic foam oligodimetilsiloksanom as a binder. The optimal process parameters
for curing coatings (temperature, concentration, etc.). The physical and mechanical
properties of building materials based on polydimethylsiloxane
References
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Departament prirodopolzovaniya i ohranyi okruzhayuschey sredyi administratsii
Vladimirskoy oblasti, 2013, 106 p.
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Rossiyskoy Federatsii. 2.1. Kommunalnaya gigiena. Metodicheskie ukazaniya.
Sanitarno-gigienicheskaya otsenka stroymaterialov s dobavleniem promothodov. MU
2.1.674 – 97 (State sanitary-epidemiological valuation of the Russian Federation. 2.1.
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Electrodialysis to clean nitrogenous wastewater enterprises
producing mineral fertilizers
Niftaliev S.I.1, Kozaderova O.A.1, Kim K.B.1, Malyavina Yu. M.2
1
Voronezh State University of Engineering Technology
2
Voronezh State Medical Academy N.N. Burdenko
Niftaliev Sabuchi. I. – grand PhD (Chem.), professor, chief of Inorganic
Chemistry and Chemistry Technology chair, VSUIT; tel.: (4732) 553887, e-mail:
sabukhi@gmail.com
Kozaderova O.A. – PhD (Chem.), associate professor of Inorganic Chemistry and
Chemical Technology chair, VSUIT; tel. (905)0518336; e-mail: kozaderovaolga@mail.ru
Kim Kseniya.B. – the post graduate student of Inorganic Chemistry and
Chemistry Technology chair, VSUIT; tel. (952)5470463; e-mail:
kmkseniya@mail.ru
Malyavina Yulia M. –post graduate student of Pharmaceutical Chemistry and
Pharmaceutical Technology Department, VSMA; tel.:(951)5642678, e-mail:
malyavinayulia@yandex.ru
Keywords: electrodialysis, nitrogen-containing wastewater, limiting diffusion
current, irreversible dissociation of water.
Abstract. The results of laboratory investigation of the electrodialysis process of
nitrogen-containing wastewater from JSC "Mineral Fertilizers" (Rossosh) are
given. The fluxes of ammonium and nitrate ions through the ion-exchange
membranes are calculated, and the energy parameters of the process are found. The
optimal conditions of the electrodialysis process are determined.
References
1. Niftaliev S.I., Kuznetsova I.V, Peregoudov Y.S. Prospects of application of
waste water PC "Fertilizers" / / Ecology and Industry of Russia. 2012. №. 3. P. 36 39.
2. Patent RF № 2480440. IPC С05G 1/00.A method for producing liquid fertilizer
on the basis of industrial wastewater from the production of nitrogen-phosphoruspotassium fertilizers. Niftaliev S.I., Kuznetsova I.V., Peregoudov Y.S, Melnik A.V.,
Okshin U.V, Kuznetsov I.A, Bull. № 12, 2013.
3. Shaposhnik V.A, Vasilieva V.I., Grigorchuk O.V. Transport phenomena in ion
exchange membranes. // Moscow, MFTI.-2001. –P.200.
4. Shaposhnik V.A, Kozaderova O.A.Transfer of hydrogen and hydroxide ions
through ion exchange membranes at current densities over limiting //
Electrochemistry. 2012. V. 48. № 8. P. 870 - 875.
5. Volkov A.I, Zharsky I.M. Large chemical directory. / / M: Modern School.2005. – 608 p.
6. Kozaderova O.A, Shaposhnik V.A. Kinetic characteristics of the ion exchange
membrane in solutions of amino acids / / Electrochemistry. 2004. V. 40. № 7. P. 798804.