Chemistry Lab Conservation of Mass The law of conservation of mass states that in a chemical reaction, matter is neither created nor destroyed. Stating the law another way, the total mass of the reactants is the same as the total mass of the products. In this laboratory investigation, you will perform three reactions and observe how this law is valid under ordinary laboratory conditions. You will do this by comparing the masses present before the reaction with the masses present after the reaction. Objectives 1. Measure the mass of reactants before a reaction and the mass of the products after the reaction. 2. Calculate the percent difference of mass before and after the reaction 3. Evaluate the validity of the law of conservation of mass under the ordinary laboratory conditions. Materials Apparatus Reagents Balance 0.1 M sodium sulfate solution Na2SO4(aq) Beakers 0.1 M strontium chloride solution SrCl2(aq) Test tubes Potassium iodide solution KI(aq) Rack Lead (II) nitrate solution Pb(NO3)2(aq) 10 ml graduated cylinder Sodium nitrate NaNO3 (s) Procedure Part 1. 1. 2. 3. 4. Put on safety goggles and laboratory apron. Place about 2.0 mL of 0.1M sodium sulfate solution Na2SO4 (aq) in a test tube. Clean the graduated cylinder thoroughly and rinse it well with distilled water. Place about 2.0 mL of 0.1M strontium chloride solution, SrCl2 (aq), in another test tube. 5. Place the test tubes with their contents in a small beaker. Determine the total mass of the solutions, test tubes, and beaker. Record the total mass in Table 1. 6. Pour the strontium chloride solution into the test tube containing the sodium sulfate solution. Record observations for the chemical reaction. 7. Place the product test tube and the empty test tube in the small beaker. Mass the two test tubes, the beaker, and the reacted solution. Record this combined product mass in Table 1. Part 2. 1. Place 10.0 mL of water in a test tube. 2. Obtain a capped test tube containing a sample of sodium nitrate solid, NaNO3(s), from your teacher. 3. Place the test tubes with their contents in a small beaker. Determine the total mass of the solutions, test tubes, and beaker. Record the total mass in Table 1. 4. Add the water to the sodium nitrate, recap the test tube firmly, and shake the mixture until the sodium nitrate dissolves. Feel the test tube and record observations. 5. Place the product test tube and the empty test tube in the small beaker. Mass the two test tubes, the beaker, and the reacted solution. Record this combined product mass in Table 1. Part 3 1. 2. 3. 4. Place about 2.0 mL of potassium iodide KI (aq), in a test tube. Clean the graduated cylinder thoroughly and rinse it well with distilled water. Place about 2.0 mL of lead nitrate, Pb(NO3)2 (aq), in another test tube. Place the test tubes with their contents in a small beaker. Determine the total mass of the solutions, test tubes, and beaker. Record the total mass in Table 1. 5. To minimize contamination, pour the potassium iodide solution into the flask containing the lead nitrate solution. Record observations for the chemical reaction. 6. Place the product test tube and the empty test tube in the small beaker. Mass the two test tubes, the beaker, and the reacted solution. Record this combined product mass in Table 1. Cleaning Up 1. Lead compounds are toxic. Place the lead product solution from Part 3 in the receptacle located on the front desk. DO NOT POUR DOWN THE DRAIN. 2. Wash all other glassware in the sink and return it to its proper place. 3. Wash your hands thoroughly before leaving the laboratory. Data Presentation TABLE 1. Mass Recordings Experiment Total Mass Before Rx (g) Part 1 Part 2 Part 3 Total Mass After Rx (g) Data Analysis 1. Calculate the change in mass (mass after Rx - mass before Rx) for each part of the experiment. Record the results in Table 2, below. 2. Calculate the percentage change in mass and record your results in Table 2 below. [(change in mass) / mass before RX] x 100 = % change. 3. Be sure to include the calculations in the report. TABLE 2. Percent Change in Mass Experiment Change in Mass (g) Part 1 Part 2 Part 3 Percent Change in Mass (%) Conclusions 1) Write the balanced chemical reaction showing reactants and products for Parts 1 and 3. Be sure to predict solubility of the products. 2) Based on the data and calculations, was the law of conservation of mass found to be valid in all three parts? 3) Suggest reasons why the data may not have confirmed the law in every part. 4) What observations were made for each of the three chemical reactions? 5) Give an example of a chemical reaction in which it would be essential to stopper (seal) the reaction vessel in order to show conservation of mass?