Contamination Guide Type: Effect: Type: Effect: Mainly rust; white particles: additives Rapid oil ageing Breakdowns in pumps & valves Wear and tear. Oil ageing products Blocking of filters Silting-up of system Metal swarf Breakdowns in pumps & valves Wearing of seals Leakage Oil ageing Particles and swarf in bronze, brass and copper Breakdowns in pumps & valves Oil ageing Leakage Wearing of seals Gel-type residue from filter element Blocking of filter Silting-up Silicates due to lack of, or inadequate, air breather filter Heavy wear on components Breakdowns in pumps, valves Wearing of seals Coloured particles (red/brown) Synthetic particles (blue) Breakdowns in pumps & valves Wearing of seals Fibres due to initial contamination, open tank, cleaning cloths etc. Blocking of nozzles Leaking from seat valves The patch shows debris deposited onto a 3 µm patch. The sample was a 320 cSt gear oil from a reduction gearbox. The bronze particles shown are typical of this type of application. The particle size, shape, morphology and number are indicative of the severity of wear Typical SEM image of the severe visible contamination US Navy Codes Severe Severe Advantages of the Patch Test In a high-pressure hydraulic system, the operator suspected that the axial flow piston pump had suffered damage and was operating with reduced efficiency. The laboratory analysis suggested that the system was satisfactory with no evidence of iron, copper, zinc or tin, and its 16/13 ISO code was within the target cleanliness level for that system. A routine patch test (1 µm) showed the presence of numerous brass/bronze cutting wear particles (Figure 1). Subsequent examination of the piston pump revealed serious wear at the slipper pad/swash plate surfaces. Figure 1 high-pressure hydraulic system The spectrographic analysis failed to detect any abnormal wear or contamination. However, in this case, the PQ index and particle counts showed an abnormal contamination level. Spectrometry failed to detect iron due to the analysis limitation of particle size (less than 5 µm). The patch test, however, showed a high concentration of spherical particles ranging in size from 20 µm to 75 µm - typical of welding debris Figure 2. A sample of hydraulic oil from a pre-feeder The sample of hydraulic oil from a pre-feeder similar to the unit detailed in Example No. 2. The spectrographic analysis, particle counting and PQ index failed to detect any abnormal wear or contamination. Although the viscosity of the hydraulic fluid was lower than the specification, there was no obvious problem. The patch test, however, revealed possible filter element deterioration Fibers were prevalent over the whole patch surface. A faulty element that had collapsed was subsequently changed Figure 3. A sample of hydraulic oil from a pre-feeder The large bronze-type particles greater than 100 µm (Figure 4) were not detected by the emission spectrometer or the PQ instrument which measures the ferromagnetic debris in the sample. It is important to note that the bronze forces a negative PQ measurement in relation to the positive ferrous reading. Reference: Mervin H. Jones, Swansea Tribology Services Ltd. U.K., "Effective Use of the Patch Test for Simple On-site Analysis". Practicing Oil Analysis Magazine. September 2004