Instructions Save this template and print it out so you have a hard copy of the instructions. Then save it again with a different name like Spec report. You can then go through and delete each of these instruction text boxes by clicking on the border and then hitting the delete key. After you complete the report you may go through and delete any unneeded blank lines. The Results and Discussion section must start on page 2. Delete this text box of instructions from your report. Put the following items in the table above: First Line – a title for the report. Come up with a unique title of your own that is descriptive of what you did but is not overly long. Think about what the experiment was trying to accomplish and how it was being accomplished. Second line – Your name Third line – Type Lab Partner: and your partner’s name Fourth Line – The date of submission of the report Fifth Line – Type Instructor: your instructor’s name Delete this text box of instructions from your report. Experimental Procedures for this investigation have been previously described. 1,2 Preparation of Stock Solutions Table 1 provides the data for the preparation of stock solutions of the copper(II) ion, Cu2+, and the tetraamminecopper(II) ion, [Cu(NH 3)4]2+ from copper(II) sulfate pentahydrate, CuSO 4·5H2O. Table 1 Formula of absorbing species Mass of CuSO4·5H2O used to prepare stock solution Volume of stock solution Concentration of absorbing species in stock solution Complete the table above. First give it a descriptive title after Table 1. The descriptive title should allow a reader to know what the table is about independent of the text preceding it. Add the units of measurement to any of the descriptions as necessary. After the table, write a 3 to 4 sentence paragraph indicating how to make your stock [Cu(NH3)4]+ solution and its concentration (it would be the same as if you were making copper(II) sulfate solution of the same molarity…the only difference is using 1M ammonia instead of distilled water as the solvent). End the paragraph with the statement “The calculation for the molarity of this solution is shown below.” and then show in detail the dimensional analysis calculation starting with the mass of the copper(II) sulfate pentahydrate and ending with the concentration of the tetraamminecopper(II) ion. You may insert the calculation by hand if you wish. Delete this text box of instructions from your report. 1 Schultz, Emeric, “Determining the Concentrations of Dissolved Matter by Spectrometry”, in Laboratory Exercises for Chemistry for the Sciences 1, Spring 2007, Bloomsburg University, pp. 41-43. 1 Results and Discussion Standard Curve for [Cu(NH3)4]2+ Insert here the appropriate lead in sentence and then a five-column table containing the information about your standard curve. (Don’t forget the label and title). Essentially, you will reproduce the Table you made in your lab notebook. (To insert a table, click Table, Insert, Table and then complete the information. Make the table 1 more row bigger than you need. Then, to make the top row available for the title, highlight the cells in the top row, click Table, Split Cells, and then make the number of rows and columns 1 each.) Then, insert the plot of your standard curve from Excel. Of course, there must be an appropriate lead in sentence. This plot must have a descriptive title and the axes must be appropriately labeled (description and units) and must have the equation from the trend line displayed. This plot must be computer generated from a spreadsheet program such as Excel. It must be imbedded in your text and, therefore, NOT be attached as a taped or glued object. Delete this text box of instructions from your report. Analysis of Unknown Solution Write a paragraph describing what you did to analyze your unknown and how you determined the concentration. Show any calculations you performed. Conclude with a statement that indicates the unknown original concentration. Delete this text box of instructions from your report. 2 How to do superscripts and subscripts: In Font Box, click on arrow in lower right hand corner, and click the appropriate box, OK, type the character(s), In Font Box, click on arrow in lower right hand corner, and unclick the appropriate box, OK. 3