APPENDIX 2.2 SPECIFICATION OF REQUIREMENTS Open procedure for the Purchase of one research grade Inductively Coupled Plasma Mass Spectrometer (High-end) Aarhus University Procurement Fuglesangs Allé 26 DK-8210 Aarhus V Case-no. 100627 September 2015 1. Description of minimum requirements and wishes This section holds the Contracting Authority’s specification of minimum requirements and wishes relation to the sub criteria. In the table below the Tenderer must do the following with regard to minimum requirements (MR) and wishes (W): – Fill in either “Yes” or “No” in the column asking ‘fulfilled? (Yes or No) – Fill in a complete description of whether the” MR”, “W high priority” or “W” is satisfied/not satisfied where requested. – Provide a full description of why the tendered product satisfies or does not satisfy the requirements. The statements in the description in this Appendix 2 will be assessed in conjunction with the tender evaluation of the sub-criteria. The assessment will focus on the degree to which the requirements are satisfied. Tenderers are therefore urged to provide as detailed an account of each requirement as possible - simple Yes/No answers may result in a low score. Please note that a minimum requirement (MR) is a requirement that the Tenderer MUST satisfy in order for the tender to be taken into consideration (need to have), whereas a “W high priority or “W” does not need to be satisfied in order for a tender to be taken into consideration (nice to have). The tender evaluation will take into account the extent to which preferences are satisfied. It should be stressed that failure to satisfy a “W high priority” will be given great importance in the tender evaluation and thus considerably lower the score. Case-no: 100627 1 2. Minimum Requirements (MR) and Wishes (W) No. Description of the Minimum Requirement or Wish (Orderer) Minimum Requirement/ Wish MR Additional explanation W Fulfilled? (Yes/No) Tick off Yes 1. GC-ICP-MS coupling and chromatographic software MR Description of how the Minimum Requirement/wish is met or reference to the part of the offer where the description of the fulfillment or the non-fulfillment is to find (Tenderer) The ICP-MS must be easily coupled to a GC unit in a standard ICP-MS setup i.e. for routine analyses of solution chemistry. The provided software must provide full control over the GC autosampler. and ICPMS. No The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; Fill in description Include price on GC if system is not compatible with our current Agilent 6890N modified for GC-ICPMS coupling. 2. Multiple nebulizer systems including: -Babington or a similar type of nebulizer for robust sample introduction (e.g. for samples with high total suspended Case-no: 100627 MR We expect to change nebulizers and sampling systems between departments due to The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; 2 solids). -self-aspirating nebulizer for high sensitivity sample introduction i.e. for optimal detection limits when analyzing low-concentration samples. different sample types and sample preparation methods. Ease of change is an important factor. Also, see pt. 4 and 5 below. Fill in description Instrumental detection limits in the sample solutions must be in the sub ng/l range to meet our needs for accurate trace element determination in low-concentration samples. The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; Also, the instrument must be adaptive to different auto sampling systems for introduction of samples with different volumes e.g. 6 and 15 ml sample vials. 3. Detection limits in the sub ng/l range for trace elements in 18 Mohm (MilliQ) waters MR Fill in description Expected real sample detection limits using 0.4 g sample to 100 ml digest of sediment/biota after DS 259 (7M nitric acid digest diluted to 100 ml): <0.1 mg/kg for Pb, Cu, Ni, Cr, As, Zn and <0.02 mg/kg for Cd. 4. Batch autosampler with room for at least 200 samples/standards. Case-no: 100627 MR For use with robust sample introduction system (e.g. Babington-type nebulizer). The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; 3 Fill in description 5. 6. 7. 8. High sensitivity autosampler with room for at least 80 samples/standards MR Gas reaction/collision cell for minimizing interferences (<2% oxides and double charged ions), with multiple gasses (hydrogen/helium). MR Education of at least 4 technicians and 3 academic staffs, consisting of on-site training following installation and a course after at least 1 month of practice on our instrument (follow up preferably at delivers site). MR LC-ICP-MS coupling and chromatographic software Case-no: 100627 W For use with high sensitivity sample introduction system (self-aspirating-type nebulizer). The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; A gas cell for minimizing inferences is required as part of the ICP-MS unless other devices or techniques to reduce interference on especially As, Se and Ni is included and proven. The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; Course should include both software and routine maintenance of the chosen instrument, including trouble shooting The tenderer must confirm the fulfilment of the minimum requirement and describe the fulfilment; The ICP-MS must be easily coupled to a LC unit in a standard ICP-MS setup i.e. for routine analyses of solution chemistry. The provided software must provide full control over the LC autosampler. and ICPMS. The tenderer should confirm the fulfilment of the wish and describe the level of fulfilment. Fill in description Fill in description Fill in description Fill in description 4 If system is not compatible with our current Agilent 1100 HPLC system, include compatible HPLC system in option 1 below 9. Long term stability of <5 % for 200 samples or 72 hours of operation W Stability after internal standard correction based on standard solutions. The tenderer should confirm the fulfilment of the wish and describe the level of fulfilment. Fill in description 10. 11. 12. 13. At least 9 decades of linear concentration range. W Guaranteed performance and spare parts availability for 10 years from purchase W (HP) Direct measurement of seawater (3.5% NaCl) with detection limit of <100 ng/l for Cr, Ni, Cu, Zn, As, Se, Pb and <50 ng/l for Cd, Mo, Mn. Recovery of 85-115% of samples spiked in the µg/l range High Resolution (R>1000, eg. Sector field or TOF) or triple-quad capability Case-no: 100627 W (HP) MR In some sample types e.g. samples from mining areas, we expect concentrations levels ranging from µg/kg to % depending on element based on previous results. The tenderer should confirm the fulfilment of the wish and describe the level of fulfilment. With proper maintenance, as set forth by the tenderer, e.g. by option 4 below The tenderer should confirm the fulfilment of the wish and describe the level of fulfilment. If extra equipment is needed (i.e. high suspended solid sampler/nebulizer or autodilutor system), what is the extra cost is for this The tenderer should confirm the fulfilment of the wish and describe the level of fulfilment. For use in mining The tenderer should confirm the fulfilment Fill in description Fill in description Fill in description 5 for removing and/or verifying potential mass overlaps (Isobaric or polyatomic) 14. 15. Capability to measure 80Se, 75As in fresh water, seawater and biota at very low concentrations (<=1, <=5 ng/l detection limit respectively in water) Capability for removing isobaric overlap of 55Mn ,58Ni in samples from Iron Ore, i.e. %-levels iron and sub µg/l Ni, Mn Case-no: 100627 W W application and research looking at low target mass concentrations where ordinary quadrupoleresolution and removal by reaction/collision cell is not sufficient due to high concentrations of interfering elements. of the wish and describe the level of fulfilment. This is for total concentrations, to establish capabilities for research on Se and As cycling, including speciation (using HPLC), and (total) measurement of all Se isotopes should be demonstrated. The tenderer should confirm the fulfilment of the wish and describe the level of fulfilment. Fill in description Fill in description Expected detection limits for individual isotopes of Mn, Ni in fresh and 3.5% saltwater containing 5% Fe at best performance 6 3. Options The Tenderer has to offer a LC-ICP-MS coupling and associated chromatographic software ( LC or HPLC) Please fill in description. The Tenderer must state the price for the Option separately in Appendix 1 – Bid schedule The Tenderer has to offer a compatible Laser-ablation-ICP-MS coupling with associated software for handling transient signals Please fill in description. The Tenderer must state the price for the Option separately in Appendix 1 – Bid schedule The Tenderer has to offer a compatible Flow-injection or similar coupling with associated software for handling transient signals Please fill in description. The Tenderer must state the price for the Option separately in Appendix 1 – Bid schedule The Tenderer has to offer a 10 years maintenance contract of the instrument from installation date, with only minor degradation of specification if maintained properly. It should also include priority repair service within 7 days or better from breakdown are reportedto the Tenderer Please fill in description. The Tenderer must state the price for the Option separately in Appendix 1 – Bid schedule Case-no: 100627 7 4. Signature Place: ____________ Signature: ___________________________________ Case-no: 100627 Date:________ 8