Technical specifications (2D detector for the time resolved X-ray diffraction endstation) Table of Content 1. Introduction .............................................................................................................. 3 1.1. 1.2. 1.3. 1.4. 1.5. 1.6. 1.7. Purpose .............................................................................................................. 3 Scope ................................................................................................................. 3 Terms, Definitions and Abbreviations ...................................................................... 3 List of applicable documents .................................................................................. 4 System Configuration ........................................................................................... 4 Input for System Level.......................................................................................... 4 External interfaces ............................................................................................... 4 1.7.1. Diagram of the interfaces of the PXS beamline in E1 (Figure 1). ........................... 5 2. Requirements on System Level .................................................................................... 5 2.1. General System Requirements ............................................................................... 5 2.2. Environmental Conditions ...................................................................................... 6 2.3. System Functional Requirements ........................................................................... 6 2.3.1. Requirements for X-ray detection ..................................................................... 6 2.3.2. Control system, Data Acquisition and Storage .................................................... 7 2.4. System mechanical, vacuum and interface requirements ........................................... 8 2.4.1. System Mechanical Design and stability ............................................................. 8 2.4.2. System Vacuum Pumping Design ...................................................................... 9 2.4.3. Interfaces ...................................................................................................... 9 2.5. System Electrical and Electronics Requirements ..................................................... 10 2.6. System Transportation and Installation Requirements ............................................. 10 2.7. Safety............................................................................................................... 10 2.7.1. General Safety Requirements ......................................................................... 10 2.7.2. Hazardous materials ..................................................................................... 11 3. System Verification Requirements .............................................................................. 12 3.1. Inspection ......................................................................................................... 12 3.2. 3.3. 3.4. 3.5. Review of design ................................................................................................ Analysis ............................................................................................................ Test .................................................................................................................. Functional Demonstration.................................................................................... 12 13 13 14 4. Quality control ......................................................................................................... 15 4.1. 4.2. 4.3. 4.4. Documentation and data control .......................................................................... Formats for data exchange .................................................................................. Warranties ........................................................................................................ Calibration/Verification........................................................................................ 2|16 15 15 16 16 1. Introduction 1.1. Purpose This Requirements Specification Document (RSD) lists the technical requirements and constraints for the selection of a two dimensional detector for the time resolved X-ray diffraction endstation situated at the X-ray plasma beamline (experimental hall E1) at the ELI Beamlines facility. This detector shall have the ability to collect diffraction patterns with sensitivity in the range of X-ray energies 3-20 keV to enable the realisation of various X-ray diffraction and spectroscopy experiments. 1.2. Scope This RSD contains all of the top level functional, performance, safety, operational, design and quality requirements for the RA4 system in experimental area number 1 (E1). 1.3. Terms, Definitions and Abbreviations For the purposes of this document, the terms and definitions from ECSS-S-ST-00-01 apply (AD -001). For the purpose of this document, the following abbreviated terms apply: Abbreviation ELI RA4 E1, 2 PXS beamline trXRD 2D detector L1 RSD NA RoD FD T A I LxWxH SI CCS CVS CDAQS FZU Meaning Extreme Light Infrastructure Research activity 4 Experimental area 1, 2 Plasma X-ray source beamline situated at Experimental area EI Time-resolved X-ray diffraction Two dimensional detector Laser 1 (1 kHz, 100 mJ) Requirement Specification Document Not Applicable Review of design Functional demonstration Test Analysis Inspection Length x width x height International System of Units Central Control System Central vacuum system Central data acquisition system Institute of Physics, Academy of Sciences of the Czech Republic 3|16 1.4. List of applicable documents Applicable documents – ECSS standards (http://www.ecss.nl/) Number of document AD-01 AD-02 Title of document ECSS-S-ST-00-01 Glossary of Terms ECSS-E-ST-10-06C Technical Requirements Specification 1.5. System Configuration The main location of the 2D detector is in E1 at the plasma X-ray source. The 2D detector shall be transferable to enable its use at other experimental areas in the ELI Beamlines facility (for example in E2 or E5). Detailed facility drawings will be provided (on request) during the negotiation phase. 1.6. Input for System Level REQ-005103/A 2D detector shall satisfy all requirements defined in section 2 of this document immediately after its delivery to ELI Beamlines. Verification method: R - review REQ-005105/A The performance of the 2D detector shall be independent on the state and parameters of L1 laser and the PXS. If at the time of delivery the PXS is not available, system verification will be performed using a conventional X-ray tube. Verification method: R - review 1.7. External interfaces External interfaces of the PXS beamline (of which the 2D detector is the main instrument) are schematically shown in Figure 1. Interfaces with the X-ray plasma source in E1 are shown. 4|16 1.7.1. Diagram of the interfaces of the PXS beamline in E1 (Figure 1). Figure 1: Diagram of the interfaces (I1 through I10) of the PXS beamline in E1. E1. I5, I6 and I7 shall serve for input into the experimental system, not for exchange of signals. 2. Requirements on System Level 2.1. General System Requirements REQ-004480/A The 2D detector shall be designed to be installed in the E1 experimental hall. Verification method: R - review REQ-004481/A The 2D detector shall be movable between experimental locations. Verification method: R - review REQ-004482/A The 2D detector shall be compatible with the PXS beamline for X-ray diffraction. Verification method: R - review REQ-004483/A 5|16 The size of the 2D detector housing shall not exceed 400 mm (width) x 500 mm(length) x 400 mm (height). Verification method: T - test, R - review REQ-004484/A The weight of the detector head shall be less than 5 kg. Verification method: T - test, R - review REQ-004485/A The pixel size of the detector shall be smaller than 100 x 100 micrometers 2. Verification method: T - test, R - review REQ-004486/A The number of pixels shall be at least one million (106). Verification method: T - test, R - review REQ-004487/A The 2D detector shall be vacuum compatible. Verification method: T - test, R - review 2.2. Environmental Conditions REQ-004488/A System shall be suitable for operation at humidity level between 40% and 60%. Verification method: FD - functional demonstration REQ-004489/A System shall be suitable for operation at a temperature of (20.0±2.0)°C. Verification method: FD - functional demonstration REQ-004490/A The system shall be compatible with working in a high EMP environment. Further details will be provided on request. Verification method: R - review, FD - functional demonstration 2.3. System Functional Requirements 2.3.1. Requirements for X-ray detection REQ-004491/A The 2D detector shall be able to detect X-ray photons in the energy range 3 – 20 keV with quantum efficiency better than 20 %. Verification method: T - test, R - review 6|16 REQ-004492/A The quantum efficiency of the detector shall be better than 80 % in the main energy interval from 6 to 12 keV . Verification method: T - test, R - review REQ-004493/A The 2D detector shall be able to detect X-ray photons in a single-photoncounting mode. Verification method: R - review, FD - functional demonstration REQ-004494/A The detector shall be able to collect diffraction patterns with the frame rate of >= 1000 Hz. Verification method: T - test, R - review REQ-004495/A The opening time for each exposure (gating) of the detector shall be tuneable with a shortest time < 5 microseconds. Verification method: T - test, R - review 2.3.2. Control system, Data Acquisition and Storage REQ-004496/A The detector shall come equipped with a local control system and local processing unit. Verification method: FD - functional demonstration, R - review REQ-004497/A Experimental data acquisition shall be hardware separated from the central control system network. Verification method: I - inspection, R - review REQ-004498/A The local control system shall be equipped at least with local storage capacity of 1 TB. Verification method: I - inspection, R - review REQ-004499/A The local processing unit shall be equipped with a suitable software suite for data handling and independent data analysis. Verification method: I - inspection, R - review REQ-004500/A The detector shall be capable of synchronization with the 1000 Hz L1 laser system used to drive the PXS or the PXS itself (details of the 7|16 triggering/timing/synchronization system will be provided during the negotiations). Verification method: T - test REQ-004501/A The detector shall be triggered with TTL pulses. Verification method: T - test REQ-004502/A The detector shall be controlled through the Transmission Control Protocol/Internet protocol (TCP/IP) or the User Datagram Protocol/Internet protocol (UDP/IP). Verification method: T - test REQ-004503/A The local control and processing unit shall be compatible with the central control, DAQ, timing, time stamping and interlock systems of the ELIBeamlines facility. Verification method: T - test, R - review REQ-004504/A The detector shall have the ability to collect multiple exposures for each readout depending on the user’s actual need. The number of exposures/frames collected for one readout shall be tuned from 1 to at least 10000. Verification method: T - test, R - review 2.4. System mechanical, vacuum and interface requirements 2.4.1. System Mechanical Design and stability REQ-004505/A System components shall be produced to be operated, used and maintained with standard tools using metric system. Verification method: FD - functional demonstration REQ-004506/A The detector shall be equipped with means for mounting to a standard metric breadboard (M6 thread, 25 mm hole spacing). Verification method: T - test, R - review 8|16 2.4.2. System Vacuum Pumping Design REQ-004507/A The detector shall be vacuum compatible for applications in a medium vacuum, around 10-2 to 10-3 mbar. The detector compatibility for applications under high vacuum (below 10-4 mbar) should be considered an advantage. Verification method: R - review, FD - functional demonstration REQ-004508/A The detector shall come equipped with all items required for vacuum operations: Cabling, feed-throughs, specialized detector head for in-vacuum use (if applicable). Verification method: I - inspection, R - review REQ-004509/A The vacuum components shall be according to ISO-K, ISO-F and ISO-KF standards. (NORMS: ISO 1609:1986 - Vacuum technology - Flange dimension; ISO 2861:2013 - Vacuum technology - Dimensions of clamped type quick-release couplings), or standard ISO/TS 3669-2:2007 - Vacuum technology – Bakeable flanges. Verification method: R - review 2.4.3. Interfaces REQ-004510/A The supplier shall support the interfacing of the detector system with the ELI Beamlines central triggering/synchronization system (details of the central timing system will be provided during the negotiations). Verification method: R - review, FD - functional demonstration REQ-004511/A The supplier shall support the interfacing of the detector system with the ELI Beamlines central control system (details of the central control system will be provided during the negotiations). Verification method: R - review, FD - functional demonstration REQ-004512/A The supplier shall support the interfacing of the detector system with the ELI Beamlines central DAQ system (details of the central DAQ system will be provided during the negotiations). Verification method: R - review, FD - functional demonstration REQ-004513/A 9|16 The supplier shall support the interfacing of the detector system with the ELI Beamlines central interlock system (details of the central interlock system will be provided during the negotiations). Verification method: R - review, FD - functional demonstration 2.5. System Electrical and Electronics Requirements REQ-004514/A System shall be designed according the valid European laws and norms. Verification method: R - review 2.6. System Transportation and Installation Requirements REQ-004516/A All components shall be delivered clean according the ISO 7 standard. Verification method: I - inspection REQ-004517/A Individual components shall be transportable in boxes with dimensions not exceeding (L x W x H) 2m x 1m x 1m. Verification method: I - inspection, R - review REQ-004518/A The system shall be delivered with an installation manual. Verification method: I - inspection, R - review REQ-004519/A The supplier shall provide on-site support at the installation and verification tests performed by ELI staff after delivery either to ELI Beamlines or a testlocation in Prague, Czech Republic, chosen by ELI Beamlines. Verification method: I - inspection, R - review 2.7. Safety 2.7.1. General Safety Requirements REQ-004520/A The supplier shall ensure that system complies with relevant EU and Czech legislation. Verification method: R - review 10|16 REQ-004521/A Supplier shall participate in the ELI Beamlines risk assessment for the normal mode(s) of operation. Verification method: R - review 2.7.2. Hazardous materials REQ-004522/A Supplier shall identify all EU-recognized hazardous materials (if any) present in the system during routine use. Verification method: R - review REQ-004523/A The system shall be designed to prevent routinely used hazardous materials (if any) to contaminate the vacuum system and experimental hall. Verification method: R - review REQ-004524/A For routinely used hazardous materials (if any) the system shall enable safe instrument and sample handling, installation, disposal, cleaning and decontamination. Verification method: R - review, FD - functional demonstration 11|16 3. System Verification Requirements The requirements are presented with the following structure: First the requirement is given. Each requirement definition shall contain a verification method by which requirement will be verified. Verification methods are following: inspection (I), review of design (RoD), analysis (A), test (T) or functional demonstration (FD). 3.1. Inspection REQ-005106/A Verification by inspection shall consist of visual determination of physical characteristics. NOTE Physical characteristics include constructional features, hardware conformance to document drawing or workmanship requirements, physical conditions, software source code conformance with coding standards. Verification method: R – review REQ-005107/A The list of accomplished requirements and their physical location and presence, and the list of unaccomplished and incomplete requirements shall be made. Verification method: R - review REQ-005108/A The results of inspection shall be documented in approved record. Verification method: R - review 3.2. Review of design REQ-005455/A Verification via review shall be the comparison of the relevant documentation which was required with the delivered documentation (e.g. technical, design, safety documentation, operational, maintenance manuals, etc.). Verification method: R - review REQ-005456/A The list of accomplished requirements and the list of unaccomplished and incomplete requirements shall be made. Verification method: R - review REQ-005457/A The results of review shall be documented in approved record. Verification method: R - review 12|16 3.3. Analysis REQ-005458/A Verification via analysis shall be to do a calculation process (calculation, simulation, numerical models, etc.) where the calculation results shall be documented together with further qualified recommendation of the following steps. Verification method: R - review REQ-005459/A The list of accomplished requirements with the calculation results and output parameters and the list of unaccomplished and incomplete requirement with the note of the missing input and reason of calculation failure shall be made. Verification method: R - review REQ-005460/A The results of calculation shall be documented in approved record. Verification method: R - review 3.4. Test REQ-005461/A Verification via test shall be to test a measurable parameter. Verification method: R - review REQ-005462/A The protocol of the measurement shall be made and approved. Verification method: R - review REQ-005463/A The list of accomplished requirements with the note of measured value and the list of unaccomplished and incomplete requirement shall be made. Verification method: R - review REQ-005468/A The test plan shall be defined including all requirements where is applied test as the verification method. Verification method: R - review REQ-005469/A Test plan shall be approved by the Customer. 13|16 Verification method: R - review 3.5. Functional Demonstration REQ-005465/A Verification via functional demonstration shall be to test the system’s response to a subject of requirement and check if its response is within the limits of the requirement. Verification method: R - review REQ-005466/A The protocol of functional demonstration shall be made and approved. Verification method: R - review REQ-005467/A The list of accomplished requirements and the list of unaccomplished and incomplete requirements shall be made. Verification method: R - review 14|16 4. Quality control 4.1. Documentation and data control REQ-005489/A The supplier shall supply the following relevant manufacturing documents (extent as stipulated in contract): Operating manual, maintenance manual, breakdown list as built, Declarations of Conformity and relevant CE markings where required by EU legislation. Verification method: I - inspection REQ-005582/A Certificate of compliance of furnished pieces with design and manufacturing documentation. Verification method: I - inspection REQ-005490/A Documentation shall be supplied in all following formats: hardcopy and PDF/A. Verification method: I - inspection 4.2. Formats for data exchange REQ-005492/A The supplier shall provide following type of documents: 3D model (if available) 2D drawings Printable format for text documents Verification method: I - inspection REQ-005493/A Formal communication between supplier and ELI shall be in the following formats: *.JPG *.PDF/A CAD 2D: *.dwg CAD 3D: STEP type files (*.stp;*.ste;*.step) text processors *.doc, *.docx, OpenDocument Format spreadsheet processors *.xls, *.xlsx, OpenDocument Format presentations *.ppt, *.pptx; OpenDocument Format *.HTML Verification method: I - inspection 15|16 4.3. Warranties REQ-005583/A Supplier shall include applicable warranty and support policies as part of the response to the tender. Verification method: I - inspection 4.4. Calibration/Verification REQ-005494/A The detector shall be delivered with a calibration protocol from successful factory acceptance tests (FATs). This calibration shall be performed using standards which are traceable to relevant national or international standards of measuring. Verification method: I - inspection, R - review REQ-005495/A The supplier shall invite representatives from ELI Beamlines to be present at FATs. Verification method: I - inspection REQ-005496/A The supplier shall supply detailed proposal of the standard calibration procedure for the detector instrument. This procedure shall be approved by the customer. Verification method: R - review, I - inspection 16|16