Measurement in the Laboratory Name Abby Hanson, Deidre Hooley, Taylor Woodhouse Chemistry Lab #1 Date 9/29/2010 Purpose: to practice making accurate quantitative measurements in the laboratory. Procedure: We will conduct six experiments to practice the measurement of length, temperature, mass, volume, density, and concentration. We will use a variety of objects to measure, including rulers, graduated cylinders, and scales. We will strive to accurately measure the substances we are given. We will wear goggles. In part one, we shall measure a textbook using a standard metric ruler. In part two we will measure the volume of a test tube filled with water by pouring the water into a graduated cylinder. Also we will find the volume of a metal screw by finding how much water it displaces. In part three will find the mass of 100ml of water by weighing it in a plastic cup then subtracting the mass of the cup. Using the same method we’ll find the mass of the screw. Prelab Questions: 1. What instruments may be used to measure each of the following quantities? a. Length: rules b. Mass: scale c. Volume: graduated cylinder d. Temperature: thermometer 2. What is density? -mass divided by volume, or the amount of matter in an object 3. Does color affect heat absorption? -Yes. Some colors, i.e., black, absorb and hold heat better than others, rather than colors like white that reflect heat instead of holding it. 4. How might the concentration of a substance affect its ability to harm an organism? -The more of a harmful substance you ingest/are exposed to the more likely you are to be harmed/affected by it. Results: Observations: (General descriptions of visible appearances or changes that occur during the experiment, such as “table salt is a white, cube-shaped crystal which dissolves in water. (Qualitative)) Data: Part 1: Measuring Length 1 Textbook Measurement Dimension Millimeters (mm) Centimeters (cm) Length 220.1 22.01 Width 35.9 3.59 Height 276.8 27.68 Part 2: Measuring Volume Test Tube Measurement Milliliters (ml) Microliters (l) 29.0 29,000 Substance Water Meters (m) .2201 .0359 .2768 Liters (l) .029 Pipet Measurement Number of Drops in 1 ml 22 Substance Water Screw Measurement Final Water Volume Water Displaced (ml) (Volume of screw) (ml) 50.19 .19 Initial Water Volume (ml) 50.00 Part 3: Measuring Mass Mass of Cup (g) 9.41 Water Measurement Mass of Cup and Water (g) Mass of 100 ml of Water 108.36 98.95 Mass of Screw (g) 7.52 Part 4: Measuring Density Substance Water Salt Water Isopropyl Alcohol Density Measurement Mass Mass of Mass of of Cup Cup and Liquid (g) Liquid (g) (g) 9.39 58.94 49.55 9.39 64.86 55.47 9.39 51.49 42.1 Volume of Liquid (ml) 50.0 50.0 50.0 Density of Substance (g/cm3) .991 1.11 .842 Part 5: Measuring Temperature Temperature Measurement 2 Time (minutes) Initial 2 minutes 4 minutes 6 minutes 8 minutes 10 minutes ___15__ minute (cooldown) Black Sand Temperature (C) 22.5 23.0 23.5 24.1 24.5 24.9 23.9 White Sand Temperature (C) 21.7 21.5 21.7 22.0 22.2 22.5 21.5 Part 6: Measuring Low Concentrations of Water Pollutants Solution Blue food dye (10%) Cup 1 Cup 2 Cup 3 Cup 4 Cup 5 Concentration (ppm) 10 1 .1 .01 .001 .0001 Calculations: Screw Measurement: 50.19ml-50.00ml= .19ml Water and Cup: 188.30g-9.41g= 98.95g Density: D=m/v=49.55g/50.0ml=.991g/ml Conclusion: We measured a textbook, found the volume of water and a screw using a pipet and a test tube, the mass of a screw, the density of water, salt water, and isopropyl alcohol, the temperature of sand over a period of time, and the concentration of food dye in water. Skills were learned that we will use in every other lab throughout the rest of the year. A better understanding of how to work through a lab and make accurate measurements was achieved. Discussion of Theory: See Turnitin.com Experimental Sources of Error: There could be many things involved for experimental sources of error. The numbers could have been rounded wrong, causing them to be bigger or smaller then they actually were. The tools could have been used improperly, and therefore caused a different amount. Also reading the scale, the ruler, and the graduated cylinder improperly could have caused error. The part if the lab that gave us the most experimental error was the concentration. The pipet was difficult to get the correct amount of water in, which caused the amount of water in the cups to be off. 3 Post Lab Questions: 1. Convert the length measurements of the textbook in Part 1 to volume by multiplying the length, width, and height. Record the answer in cubic centimeters. - V=lwh 22.01 cm 3.59cm 27.68cm 2187cubic centimeters 2. In part 3 the mass of 100 ml of water was determined. Using this information calculate the density of 100 ml of water. - D= m/v D= 98.95g/ 100mL D= 1 g/mL 3. How does this density compare to the density of 50 ml of water calculated in Part 4? - They are closely related, because .991 can be rounded to 1, which is the approximate density of rounded. 4. Which liquid in Part 4 had a density greater than water? Less than water? - Salt water has a greater density than water. Isopropyl alcohol has a density less than water. 5. In Part 5, the temperature of two different colors of sand, black and white, were compared under a lamp. Using the data table/worksheet, graph the temperature values for the 10-minute exposure of each color of sand. (Note: Graph both sand colors on the same graph using a different color pencil for each.) 6. Did one color of sand lose heat faster than the other color after being allowed to cool for 15 to 20 minutes? Explain. 7. Would it make sense to wear lighter colored clothing in the winter or in the summer based on this data? Explain. 8. What happens to the color of the dye in Part 6 in each successive medicine cup? - The color got lighter as the concentration level became lower. 9. Convert the final concentration of cup 5 in Part 6 into parts per billion (ppb) and parts per trillion (ppt). 10. What other quantitative measurements may be taken? 4