INSTRUMENTAL ANALYSIS PHARMACY 4TH SEMESTER SPRING 2014/20145 Weeks / Date 1. 2. 3. 4. 5. 6. 7. Lecture On Tuesday 8:00 -9:30 7. Seminar Room Introduction to Instrumental Analysis 27.01 Prof. Ferenc Kilár Introduction Electroanalytical Chemistry: Potentiometric Methods Direct potentiometry: Potentiometric Methods, 03.02. Measurement of solution's pH by direct Conductometric potentiometry Methods Prof. Ferenc Kilár Introduction to Absorption Potentiometric Methods Acid – Base Titration: 10.02. Spectroscopy: Titration of KOH solution using potentiometric Atomic spectroscopy end-point detection Prof. Ferenc Kilár Conductometric Methods: Ultraviolet(UV) – Titration of KOH solution using conductometric Visible(VIS) and end-point detection 17.02. Spectrophotometry Determination of the temporary hardness of tapProf. Ferenc Kilár water by conductometry Electrophoresis / Capillary 24.02. Electrophoresis (CE) Prof. Ferenc Kilár Separation Technique / Gas Chromatography 03.03. Prof. Attila Felinger Ultraviolet(UV) – Visible(VIS) Spectrophotometry: Determination of NiSO4 concentration by spectrophotometry using standard addioton method Methylenblue concentration measurement by spectrophotometry Atomic spectrophotometry (AS) Concentration determination of potassium ion (K+) solution by atomic emission Spectroscopy Concentration determination of copper ion (Cu2+) solution with atomic absorption spectroscopy Liquid Chromatography / High - Performance Liquid Chromatography 10.03. (HPLC) Gas chromatography (GC): Prof. Attila Felinger Gas chromatographic determination of normal alkanes TEST 1. 8. Practice On Friday 8:00 -11.00 17.03. Mass Spectrometry I. High - Performance Liquid Chromatography (HPLC): Quantitative analysis of active substance of Saridon analgetic Instructor Workplace Date Tímea Dergez Laura Nagy SzKK B102 30.01. Laura Nagy SzKK B102 06.02. Laura Nagy SzKK B102 13.02. Laura Nagy SzKK B102 20.02. Tímea Dergez SzKK B102 27.02. Tímea Pernyeszi TTK Dep. of Analytical Chemistry C111 and 06.03 Viktória Poór Anita Bufa Viktor Sándor AOK Institute Of Bioanalysis 13.03. and 20.03. Nuclear Magnetic Resonance 24.03. Spectroscopy (NMR) Dr. Zoltán Berente 9. Mass Spectrometry II. 07.04. (MS) Prof. Ferenc Kilár 10. 11. 14.04 Infrared Spectroscopy (IR) Dr. Tamás Kégl Nuclear Magnetic Resonance Spectroscopy (NMR) Mass Spectrometry (MS): Structural analysis of capsaicin and dihidorcapsaicin by electrospray – ion trap MS and MS/MS methods Capillary Electrophoresis (CE): Determination of preservatives and vitamin C with capillary zone electrophoresis (CZE) 28.04. 14. 05.05. Institute Of Bioanalysis 27.03. and 10.04. Institute of Bioanalysis 17.04. TTK Dep. of Analytical Chemistry 03.04 Capillary Electrophoresis (CE): Determination of preservatives and vitamin C with capillary zone electrophoresis (CZE) TEST 2. Thermal Methods Prof. Ferenc Kilár Lilla Makszin Tamás Kégl Infrared Spectroscopy (IR) 13. Lilla Makszin SZKK “C” building Spring holiday Spectrometry III. 21.04. Prof. Ferenc Kilár 12. Viktor Sándor, Ibolya Prauda Tamás Kégl Infrared Spectroscopy (IR) 30.0306.04 Zoltán Berente Institute of Bioanalysis Holiday Final practice 24.04 TTK Dep. of Analytical Chemistry 01.05. Laura Nagy SzKK B102 08.05. PRACTICE ( EXTRA) TIMETABLE: GROUP A: 1. 2. 3. 4. 5. 6. 7. Ahangar Sina Ashraf Amir Reza Bayat Afsaneh Hamidi Abolghasem Kalali Tahoora Moayedi Hananeh Zarei Hanieh 27.02.2015 06.03.2015 13.03.2015 20.03.2015 27.03.2015 10.04.2015 17.04.2015 24.04.2015 Ultraviolet(UV) – Visible(VIS) Spectrophotometry Atomic spectrophotometry (AS) Gas chromatography (GC) High - Performance Liquid Chromatography (HPLC) Nuclear Magnetic Resonance Spectrometry (NMR) Mass Spectrometry (MS) Capillary Electrophoresis (CE) Infrared Spectroscopy (IR) GROUP B: 1. 2. 3. 4. 5. 6. 7. Mohammadi Fard Shima Momenzadeh Nahid Roodaki Zahra Shanehchiyan Salar Shojaee Rahnama Dorsa Zarei Hoda Efazati Anita 27.02.2015 06.03.2015 13.03.2015 20.03.2015 27.03.2015 10.04.2015 17.04.2015 24.04.2015 Atomic spectrophotometry (AS) Ultraviolet(UV) – Visible(VIS) Spectrophotometry High - Performance Liquid Chromatography (HPLC) Gas chromatography (GC) Mass Spectrometry (MS): Nuclear Magnetic Resonance Spectrometry (NMR) Infrared Spectroscopy (IR) Capillary Electrophoresis (CE)