Shaquaria Wallace 11/29/12 Copper Cycle Lab Report (Your lab report will be due by email to tbamannion@gmail.com or on paper by next Friday 12/7) Abstract: In this lab my group and I experienced in copper. We started off with copper and during this process we added many chemicals to see how copper will react and at the end with ended up back with copper. But just remember copper never disappeared it just simply was going with different partners (chemicals) to see how it will react. We used copper power, breaker, water etc.. Materials: Copper power Sulfuric acid (1m) Nitric acid (8m) Zinc filings Sodium hydroxide (8m) Water Beaker Metal spatula Glass rod Grautuated cylinder Filter paper Funnel Tongs Hot plate Goggles Erlenmeyer flask Pipette Fume hood Procedures: 1. 2. 3. 4. Measure out 0.10 g of copper powder Place the copper in a 250 mL beaker Slowly add 2 ml of concentrated nitric acid (8m) to the copper When the brown gas is no longer being produced, remove the beaker from the fume hood 5. Add approximately 25 ml of water 6. Slowly add 2 ml of sodium hydroxide (8m) to the beaker. Be sure to look for any solid that begins to appear scattered throughout the liquid 7. Heat the beaker on the hot plate set it medium. Stir with the glass stirring rod while heating. 8. Use tongs to move the beaker from the hot plate to the lab bench. 9. Filter the solution with a funnel and a piece of filter paper. 10. Gently scrape the solid from the paper using a small spatula into a 100 ml beaker 11. Add 15 ml of sulfuric acid (1m) slowly while stirring. As you add the acid observe any changes in the liquid and solid. 12. Measure approximately 0.1 g of zinc filings to within 0.098 g to 0.102 g. add the zinc to the beaker. 13. Pour off most of the liquid. Clean up your area Data : What you did Chemical added What you saw (observations) Got copper from the teacher Added nitric acid Cu (s) Added sodim hydroxide NaOH(aq) Reddish brown powder A brown gas bubbled out and then there was a blue solution A dark blue cloud formed in the solution Black solid formed in the liquid Black solution Added heat HNO3(aq) ---- Added sulfuric acid H2SO4 (aq) Added zinc Zn (s) Bubbled and then a reddish brown Chemical Formula and Name of copper compound Cu (s) Solid copper CU(NO3)2 (aq) Copper nitrate solution Where is the copper? Cu(OH)2 (aq) Copper hydroxide solution CuO4 (aq) Copper sulfate CuSO4 (aq) Copper sulfate Cu(s) In the copper hydroxide solution In the copper powder In the copper nitrate solution In the copper oxide solid In the copper sulfate solution In the beaker as a solid again powder appeared Analysis: My group and I started with copper powder and added nitric acid. A brown gas (nitrogen dioxide) escaped and the blue solution that was left was copper nitrate. Then we added sodium hydroxide which created a dark blue cloud (copper hydroxide). Then my group mate added heat to the solution, which we put the beaker on top of the heat plate, which then formed a black liquid (copper oxide). Afterwards my next group mate added sulfuric acid, and then it turned into a blue liquid (copper sulfate). At the end we then added zinc which bubbled and a reddish brown powder appeared. Discussion: 1. 2. 3. 4. 5. 6. 7. 8. What happened to the copper in this lab? It is changing partners. Did it disappear or was it destroyed? No it just kept changing after its being bond with different elements. Did the copper always look the same? No, every time we added a different chemical the color which then changed. Why do you think that was? Because each chemicals has different types of reacting in it. What types of compounds are Cu(NO3)2 , Cu(OH)2 , CuO , CuSO4 ? Ionic compounds. What element is the cation for each of these compounds? Copper Honors/Extra Credit: What charge does the cation have? Positive. /How do you know? Because it’s on the right side of the periodic table. What happens to the anion? It gets electrons added to them because they don’t have enough electrons. Is it always the same? No depending on the element. Honors/Extra Credit: What type of chemical reaction is it when the ions switch places? It’s called double replacement. Honors/Extra Credit: Why are the formulas for copper nitrate and copper hydroxide written with parentheses and a 2 like this: Cu(NO3)2 , Cu(OH)2 ? So it can show how many it has and what’s added. Conclusion: In this experiment the copper was combing with different elements which cause it to react differently with the color and how it forms and smells. This laboratory experiment is called the copper cycle because during this experiment it kept switching to different forms. It also went through many changes with its color and how it looks. Like for example when we added nitric acid it started to bubble and had a blue color solution to it, then when we added sulfuric acid it clumped into a reddish brown clumps of what it looked like dirt. When atoms was added it was never destroyed it just turn into a different solution. It tells me that depending on the chemical that is added it changes it form like it’s always there it just looks different until it goes back to its original form. Copper Cycle Lab Report Category Advanced 8 Proficient 6 Abstract Abstract is a thorough summary Abstract covers all aspects of the Abstract covers only some of the lab report. lab report but is not thorough. aspects of the lab report. Abstract does not cover that many aspects of the lab report. Materials All materials are listed, both chemicals and non-chemicals. Most materials are listed. Some materials are listed. Little or no materials are listed. Procedure All procedures are written. Most procedures are listed. Some procedures are listed. Little or no procedures are listed. Data Data table is filled in completely. Data table does not have subscripts written properly. Analysis The analysis summarizes the data The analysis summarizes most of The analysis summarizes in paragraph form. the data. some of the data. Discussion The discussion questions are answered thoroughly and correctly. Conclusion The conclusion section includes a The conclusion section includes conclusion about the lab and conclusions just about the lab. elements in general. Spelling, Punctuation, Grammar There are no spelling, punctuation, or grammar mistakes. There are few spelling, punctuation, or grammar mistakes. On Time The lab report is turned in on time The lab report is 1 day late. The discussion questions are mostly answered correctly. Developing 4 Data table is missing some information. Beginning 2 Data table is mostly incomplete. The analysis summarizes little or none of the data. The discussion questions are The discussion questions are somewhat answered mostly answered correctly. incorrectly. The conclusion section does not make real conclusions about the lab. There are some spelling, punctuation, and grammar mistakes. Grade _______ / 72 There are many spelling, punctuation, and grammar mistakes. The lab report is more than 1 day late.