99 March 2099 From: Midn Alpha Beta To: Professor Roy McClean Subj: Identification of Metal Ions in Unknown X1234 Ref: Experiment 25 - (Type name of experiment here, without the parenthesis) Encl: (1) Flow Chart for Determining Metal Ions in a Solution 1. The purpose of this experiment was to determine what metal ions were present in unknown solution X1234. We found that this solution contained Hg2+, Na+, Zn2+, and Ca2+ ions. 2. Experimental Method. We used qualitative analysis to analyze our solution. In brief, the experimental method we used is based on …………. See the attached flowchart and the lab handout for exact procedural steps. (use words such as separation, confirmation test, precipitation, supernatant, centrifuge, etc.) 3. Results. Mercury (II), sodium, zinc (II), calcium, aluminum, cadmium (II), and cobalt (II) ions were the possible species in our unknown solution. After careful testing, our solution was found to contain Hg2+, Na+, Zn2+, and Ca2+ ions. The presence of Hg2+ was confirmed by the formation of a bright purple precipitate when it reacted with plebeium. Na+ …. 4. Discussion and Conclusion. ….. We conducted the experiment twice in order to confirm the presence of Hg2+. Another metal ion, Cd2+, also reacts with plebeium and forms a dark blue precipitate which could be mistaken for Hg2+ or vice versa. ……….. (You must discuss every possible ion, even if it/they were not present in your unknown sample. Discuss possible sources of error. ) /S/ Midn Alpha Beta Instructions 1. Delete these instructions before printing. 2. Use this document for your memo. It is correctly formatted with 1” margins, single-spaced, times new roman font, 11 pt, left justified, numbered paragraphs, spaces between paragraphs, etc. Do not change the formatting. 3. Use 8 ½” x 11” white copier paper, with black ink (the ink should not be faded). 4. Check your grammar, spelling, and chemical formulas. 5. The memo must be between 1.5 to 2 pages, portrait format, and stapled (2-sided printing is acceptable and is encouraged). Do not exceed 2 pages. 6. Remember to change the date, name, etc. 7. Sign your memo (replace /S/ with your signature). Your signature indicates that this is your own work. You may ask anyone to proof-read your memo, if you feel the need to. Lab Report Due Tuesday, 3 November 2015, before class is called to attention. Submit only the type-written memo, not the lab handout. Grading Rubric The report (memo) is out of 100 points Section Header information Para 1: Purpose & identification of metal ions found Para 2: Experimental method Para 3: Results Para 4: Discussion and conclusions Correct identification of metal ions Signature block Miscellaneous (Format, organization, clarity, readability, etc.) Points 5 5 20 10 20 25 5 10