Effects of Processing Parameters on Constant-Rate Puncture Resistance Behaviors of Compound Fabrics Ching-Wen Lou1, Ting-Ting Li2, b, Jan-Yi Lin3, Mei-Chen Lin3 and Jia-Horng Lin3, 4, 5, a 1 Institute of Biomedical Engineering and Material Science, Central Taiwan University of Science and Technology, Taichung 406, Taiwan. 2 School of Textiles, Tianjin Polytechnic University, Tianjin 300387, China. 3 Laboratory of Fiber Application and Manufacturing, Department of Fiber and Composite Materials, Feng Chia University, Taichung City 407, Taiwan. 4 School of Chinese Medicine, China Medical University, Taichung 40402, Taiwan. 5 Department of Biotechnology, Asia University, Taichung 41354, Taiwan. Corresponding email: ajhlin@fcu.edu.tw, blitingting_85@163.com Keywords: Compound fabric, Kevlar fiber, puncture resistance, thermal bonding. Abstract. The effect of Kevlar fibers amount, number of layers, thermal bonding and fabric type on constant-rate puncture resistance of low-cost compound fabrics are discussed. Therein, compound fabrics were prepared by nonwovens and woven fabric via needle-punching and thermal-bonding processes. The result shows that, Kevlar fibers amount and number of layers are both positive to improvement of puncture resistance. And thermal bonding process increases the wearer safety of puncture-resistance materials. For different kinds of fabrics, compound Kevlar fabric shows the maximum puncture resistance. Introduction As human people become conscious to individual protection, development of puncture-resistance protective materials are aroused much attention. Nowadays, the armor only to resist puncture-resistance is rarely used. And in commercial, current puncture-resistance armor has also bullet resisting function [1]. Thus it is expensive to be used for puncture resistance, and limited in use of police, army fields. Nevertheless, these materials are also necessary to be applied for motorcycle racing driver, taxi driver, and instruments packaging [2]. In view of these, the cost of puncture resistance material needs to be reduced. To reduce cost, some researchers have impregnated thermoplastic films on aramid fabrics [3, 4, 5]. But puncture-resistance materials made by this method are inflexible and uncomfortable to wearers. In this paper, we will only use textile technology to prepare a flexible puncture-resisting material based on nonwoven and needle-punching technique. Meanwhile, different kinds of fabrics after being compounded with nonwovens were discussed comparatively in relation with puncture resistance property. Experimental Compound Fabric Preparation. Recycled Kevlar fibers (50-60 mm length, provided by DuPont Company, America), 6D high-strength Nylon 6 staple fibers (supplied by Taiwan Chemical Fiber Co. Ltd., Taiwan), and 4D low-Tm polyester fibers (supplied by Huvis Corporation, South Korea) were used to make high-modulus nonwovens through opening, blending, carding, lapping and needle-punching (at 100 needles/cm2) processes. The Kevlar fiber was varied from 0 wt%, 10 wt%, 15 wt% and 20 wt%, while the proportion of the low-Tm polyester fibers was constant as 30 wt%. After that, one layer of woven fabric was inserted between double layers of high-modulus nonwovens via needle-punching density, forming compound glass fabrics. Therein, woven fabrics were chosen as glass fabric, Kevlar fabric, and carbon fabric, whose specifications were shown in Table 1. After that, compound fabrics were hot-pressed by Twin-Roller calendaring at 160℃ in velocity of 0.5 m/min, intended to form thermo-bonded fabric. The distance between upper and lower roller was constant as 1.5 mm. Comparatively, the compound fabric before thermal bonding was considered as the control group to discuss thermal-bonding effect influencing on puncture behavior. Constant-rate puncture test. The constant-rate puncture test, also called as static puncture test, was conducted by Instron 5566 (Instron, America) at constant rate of 508 mm/min according to ASTM 1342-05 [6]. The dimensions of testing probe head has chosen Probe A as specified in ASTM standard. During testing, puncture displacement-force curve was displayed, and the maximum puncture force was found. To ignore the thickness and weight on puncture resistance, the puncture resistance was characterized with maximum puncture force divided by volume density, in expression of N/(g/cm3).In this test, six specimens were duplicatedly tested in each group. Table 1. The structural parameters of three fabrics. Area Fabric Fineness Density Thickness Weight Glass fabric 1100 D 328 g/m2 34 × 26/inch 0.31 mm Kevlar Fabric 1500D 227 g/m2 17×17/ inch 0.32 mm Carbon fabric 12 K 390 g/m2 6×6/inch 0.60 mm Results and Discussions Influence of recycled Kevlar fibers on static puncture resistance Figure 1. Static puncture resistance per unit volume density of compound glass fabrics as related to different weight fractions of recycled Kevlar fibers contained in the surface nonwoven. Figure 1 shows the static puncture resistance of compound glass fabrics whose surface nonwovens have different fractions of recycled Kevlar fibers. Apparently, the static puncture resistance per volume density improves from 0 wt% to 20 wt% of Kevlar fibers. This reflects the positive effect of cut-resistance Kevlar fibers. When more Kevlar staple fibers contact with the puncture probe, the more cut-resistance from Kevlar fibers would resist against more puncture energy. Abnormally, the static puncture resistance mains constant between the 10 wt% and 15 wt% Kevlar fibers that contained in nonwovens. This is due to the fact the smaller addition of Kevlar amount compromises to Kevlar fibers non-uniform distribution. Influence of number of layers on static puncture resistance It is displayed in Figure 2 that as the number of compound glass fabrics increases, the static puncture resistance improves steadily. Initially, when adding from one layer to two layers, static puncture resistance is increased by more than two times. This is because the interfacial shear strength and friction strength both provide the additional static puncture resistance. Moreover, while from two layers to five layers, the static puncture resistance per volume density rises proportionally. This increase is due to adding thickness, thus the friction between probe and compound fabric in the process of penetrating through the compound fabrics promotes linearly. Static Puncture Resistamce (N/(g/cm3)) Figure 2. Static puncture resistance of compound glass fabrics comprised of 20 wt% Kevlar fibers on surface as related to number of layers. Influence of heat bonding on static puncture resistance It is shown from Figure 3 that the heat bonding shows negative effect on puncture resistance. Clearly, the hot-pressed compound fabric shows lower puncture resistance regardless of fabric type. We also observed that the compound fabric after being thermo-bonded produce small puncture damage region after puncture test. That means that thermal bonding effect would minish the trauma depth to wearer. Furthermore, the hot-pressed compound fabrics have stable resistance to puncture damage. This results from the smaller interspace contained in compound fabric as compared to un-hot-pressed specimens, and thus bigger pushing forces occur to resist against the puncture. 1400 1200 1000 800 Hot-press 600 non-hot-press 400 200 0 5G 5K 5C Figure 3. Comparative static puncture resistance per volume density of 5-layer compound glass fabric, Kevlar fabric and carbon fabric after being hot-pressed or un-hot-pressed. Comparative fabric pattern change on static puncture resistance In Figure 3, we compare the puncture resistances of different kinds of compound fabrics with five layers. It is clear that the compound Kevlar fabric posses the maximum puncture resistance, reaching 948.439 N/(g/cm3) after being hot-pressed, and compound carbon fabric shows the lowest746.871N/(g/cm3). However, for those un-hot-pressed compound fabrics, the compound fabric consisting of nonwovens and glass fabric owns the optimum puncture resistance, 1159.55 N/(g/cm3), which reflects the fiber density more significantly influence on the static puncture behavior. For being thermal-bonding fabric, fabric type and cut resistance performance determined the puncture performance. Relatively, the high impact-resistance and high cut-resistance fabric compounded with double layers of nonwovens reveals excellent puncture performance after constant-rate puncture impact. Conclusions This paper systematically analyzes the constant-rate puncture resistance of compound fabrics comprised of double layers of nonwovens and a fabric via both needle-punching and heat bonding processes. The Kevlar fiber amount in nonwovens and fabrics type both significantly influence on the puncture resistance of compound fabrics. Puncture resistance improves linearly with Kevlar fiber amount, and multiply and then proportionally increases as the layers of compound fabrics add. Thermal bonding effect would decrease the trauma depth even that negative to the puncture resistance. Finally, comparing with different kinds of fabrics, Kevlar fabric reinforced with nonwovens have the optimum puncture resistance at per volume density. According to this study, we are expected to fabricate low-cost and high-performance puncture-resistance compound fabric for purpose of civil puncture-resistance protection. Acknowledgements This work would especially like to thank National Science Council of the Taiwan, for financially supporting this research under Contract NSC 101-2621-M-166-001. References [1] S. J. Russell, A. Pourmohammadi, I. Ezra and M. Jacobs, Formation and properties of fluid jet entangled HMPE impact resistant fabrics, Composites Science and Technology, 65, (2005): 899-907. [2] L. J. Li, G. M. Jiang and X. H. Miao, Soft stab-resistant materials present situation and new development , Industrial Textiles, 8, (2010), 8-12. [3] Hosur MV, Mayo JB, Wetzel E and Jeelani S. Studies on the fabrication and stab resistance characterization of novel thermoplastic-kevlar composites. Adv Struct Funct Mater Prot 2008; 136: 83–92. [4] Mayo Jr, J. B., Wetzel, E. D., Hosur, M. 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