Maris Stella High School Measurements and Experimental Techniques Name: _________________________( ) Class: 3______ Date: ___________ Topic 1: Measurement and Experimental Techniques Syllabus Objectives: (a) Name appropriate apparatus for the measurements of time, temperature, mass and volume, including burettes, pipettes, measuring cylinders and gas syringes; (b) Suggest suitable apparatus, given relevant information, for a variety of simple experiments, including collection of gases and measurement of rates of reaction. 1.1 Measurement of Time, Temperature and Mass Time Temperature Mass Apparatus used Units 1.2 Measurements of Volumes of Liquids Apparatus Accuracy For measuring accurately the volume of a liquid. (0 to 50.0cm3) For measuring accurately a fixed volume of liquids, e.g. (20.0 cm3 or 25.0 cm3) For measuring up to the nearest cm3, e.g. (24 cm3 or 99 cm3) (least accurate) For estimating the volume of a liquid, e.g. (50 cm3 or 100 cm3) *Note: different decimal places used for different apparatus 1 Maris Stella High School Measurements and Experimental Techniques Example of Burette readings : Burette readings: Final: Initial: Volume of liquid used = Initial reading 1.3 Measurements of Volumes of Gases Apparatus Gas Syringe Hydrochloric acid+ lumps of calcium carbonate Final reading Accuracy For measuring accurate volume of gases up to a maximum of 100 cm3. Accurate volume of gases can be manually read on the graduated scale, or automatically recorded using data logging. 2 Maris Stella High School 1.4 Measurements and Experimental Techniques Preparing a Dry Sample of Gas We can collect dry samples of gases by passing it through drying agent. Some commonly used drying agents are concentrated sulfuric acid, quicklime (calcium oxide) and fused calcium chloride. 1.5 Collecting Gases in the Laboratory Method of collecting a gas depends on the physical properties of the gas: - The _______________ of the gas in water - The ______________________ of the gas compared to the density of air Method Displacement of water Downward deliverydisplacement of air Upward deliverydisplacement of air Used on gases that are insoluble or slightly soluble in water. For fairy soluble or very soluble gases in water that are heavier or denser than air. For fairly soluble or very soluble gases in water that are lighter or less dense than air. Example of gases 3 Maris Stella High School Measurements and Experimental Techniques Method: ________________________________ Method: ________________________________ Method: __________________________________ 4