Crawford University STUDENTS’ HANDBOOK (2011 - 2013) INDUSTRIAL CHEMISTRY i Industrial Chemistry Published by: A Publication of Crawford University P.M.B. 2001 Km 8 Ota – Atan - Agbara Road Faith City, Igbesa, Ogun State Nigeria College Colour: Gold Cover Designed and Printed by: Mustard Communications 10, Adeoye Fafore st. PAB Bus Stop Ikotun, Idimu Rd. Lagos. Nigeria Email: samdaodu@gmail.com. Tel: 08033304269. Copyright ©CRU March 2012 ii Industrial Chemistry TABLE OF CONTENTS Page Title page i Copyright page and Publication History ii Table of Contents iii Addresses iv Objectives of the University v Visitor and Principal Officers of the University vii Foreword viii Officers of the College ix General Information 1 Department 44 iii Industrial Chemistry ADDRESSES Requests for information regarding the University should be sent to: The Registrar: Crawford University Faith City, Igbesa, Ogun State. Postal Address: P.M.B. 2001, Igbesa, Ogun State,Nigeria Website: www.crawforduniversity.edu.ng e-mail: vc@crawforduniversity.edu.ng registrar@crawforduniversity.edu.ng dean-conas@crawforduniversity.edu.ng hod-biosc@crawforduniversity.edu.ng hod-physicalearthsc@crawforduniversity.edu.ng hod-cit@crawforduniversity.edu.ng Telephone: Vice-Chancellor: 08056697800 Registrar: 08056697802 Deputy Vice-Chancellor: 08056697805 Dean’s Office: 08056697803 Academic Planning Unit: 08131183200 Public Relation and Information Unit: 08035456352 University P.R.O. 07054779136 Telephone Room: 08065296600 iv Industrial Chemistry OBJECTIVES OF THE UNIVERSITY Crawford University, was established in 2005. Seven years after, the University is manifesting the dream of its founding father, put together in form of the objectives of the University, to meet the peculiar needs of Ogun State. The objectives of the University are: To give the opportunity of acquiring higher education to qualified candidates without discrimination as to race, nationality, creed, religion, sex or political conviction. To form the apex of the educational system of the State, to provide facilities for learning, and to give instruction and training in such branches of knowledge as the University may desire to foster, and in doing so, to enable students obtain the advantage of liberal education; To promote, by research and other means, the advancement of knowledge and its practical application in social, cultural, economic, scientific and technological problems; To encourage the advancement in general, and to provide the opportunity for acquiring higher and liberal education; To act as a vehicle of development in general, and, in particular, to act as an instrument to effectively stimulate the development of the State through continuing education, applied research, technical assistance, direct consultation, informational services and internship programs; and community service. To provide innovative educational programmes of high standard, regardless of the nature of the degree being pursued, as this has importance and relevance for State and National development; To provide ready access for citizens of the State in particular to higher education, regardless of social origin or income; v Industrial Chemistry To meet the specific manpower needs of the State; To serve as a creative custodian, promoter and propagator of the State’s social and cultural heritage and resources; To undertake undergraduate and postgraduate courses in Arts, and Social Sciences, Education, Science, Engineering, Technology and Environmental Design, Management Sciences and Basic Medical Sciences To enhance educational opportunities for Ogun State indigenes and; to undertake any other activities appropriate for a University of the highest standard. To incorporate Godly virtues into the learning processes in the university. vi Industrial Chemistry VISITOR AND PRINCIPAL OFFICERS OF THE UNIVERSITY VISITOR Rev. Emmanuel Adebayo Adeniran District Superintendent, Apostolic Faith Mission West and Central Africa Headquarters, Lagos. CHANCELLOR Chief Oludolapo Ibukun Akinkugbe CON PRO-CHANCELLOR AND CHAIRMAN, GOVERNING COUNCIL Professor Peter Akinsola Okebukola OFR VICE-CHANCELLOR Professor Samson Adenola Ayanlaja B.Sc. (Hons Ibadan), MBA, Ph.D. (Reading), Cert. Irrig. (Israel) DEPUTY VICE-CHANCELLOR Professor Emmanuel Abiodun Fayose B.Sc,, Ph.D (Wales) REGISTRAR Mr. ‘Tunde Oluite Adekoya B.Sc (Hons), M.I.L.R (Ibadan), M.PP(Ogun), MNIM, AIPM. UNIVERSITY LIBRARIAN Mr. Thomas Akinbayo Adigun B. Sc. (Hons) Ife, MLS. (Ibadan) BURSAR Rev. Elijah O. Ajayi FCA, ACMA. vii Industrial Chemistry FOREWORD This is the second edition of the students’ Handbook of the College of Natural and Applied Sciences, Crawford University, Faith City, Igbesa, Ogun State. Nigeria. The College of Natural and Applied Sciences is one of the two Colleges which was established at the inception of the University in October, 2005. There have been remarkable changes in the staff structure and academic programmes in the College during the past six years of its existence. All these changes have focused on the achievement of the goals and objectives of the University. The first part of the Handbook contains the general information on the organisation/administrative structure of the College, and composition of the Standing Committees, the past and current officers of the College; In addition, there is information on the admission requirements and the regulations governing the award of Bachelor’s Degrees in the College. The second part provides the detailed information on the Department/Teaching Units in the College as regards the course structure (Title/Status/Unit). In addition, the course contents of all courses offered in each degree programmes have been well-documented at each Level as per Semester for each degree programmes. This Handbook covers the period of five years (2011 – 2013). Both the students and teachers will find this Handbook as a reference for consultation periodically. It is hoped that the Handbook shall provide a primary source of information about the University and the degree programmes offered in the College. Prof. Rufus Oladiran Okotore B.Sc, (Ibadan) M.Sc, Ph.D (Dalhousie) MNYAS, FIPAN viii Industrial Chemistry OFFICERS OF THE COLLEGE DEAN Prof. Rufus Oladiran Okotore B.Sc,(Ibadan) M.Sc, Ph.D (Dalhousie) MNYAS, FIPAN COLLEGE OFFICER Mrs. Christianah M. Majasan B.Sc. (Ado-Ekiti) PERSONAL SECRETARY TO THE DEAN Mrs. Felicia Aina NCE, Dip. In Computer Studies ix Industrial Chemistry GENERAL INFORMATION 1. Historical Background The College of Natural and Applied Sciences was established on the inception of the University in October 2005. The decree that established the University academic programmes stipulated the creation of three Departments only; viz. Department of Biological Sciences, Department of Physical and Earth Sciences and Department of Computer Sciences and Information Technology. Within each Department were to be established other teaching units which were to offer B.Sc. degree programmes. Thus, in the Department of Biological Sciences, the B.Sc degree programmes offered were in Microbiology, Biochemistry, Zoology, Botany, Biochemistry whilst the B.Sc. degree programmes in Physics/Electronics, Industrial Chemistry, and Geology/Mineral Sciences were to be offered in Department of Physical and Earth Sciences. The B.Sc. degree programme in Computer Science and Technology, Information and Communication Technology are offered in the Department of Computer Science and Information Technology. Based on the above the students were enrolled into the College in October 2005. Unfortunately, some of the B.Sc. degree programmes failed to start due to insufficient students intake. Those that really got started were seven programmes namely:Microbiology, Biochemistry, Physics/Electronics, Geology, Industrial Chemistry and Computer Science and Technology, Information and Communication Technology. These B.Sc. degree programmes are still in operation till the present day. 1 Industrial Chemistry 2. Organization/Administrative Structure The Dean of the College is the administrative Head of the College that exercises general control over the academic and administrative affairs of the College. The Dean is assisted by the Heads of Department in the College, and the College Secretary. The Heads of Department are responsible through the Dean to the ViceChancellor for the smooth running of their Departments. The College Secretary is the Head of all the non-academic staff of the College. He/She is the Secretary to all the College Boards and Committees. He/She also ensures the implementation of their decisions and directives. Also He/She ensures the proper organization of the student records in the Dean’s Office. Students in the College organize academic and social activities under the aegis of the Students Associations relevant to the academic disciplines in the College. Such association draws its membership from all matriculated students in the particular academic discipline. The Departments also organize career and motivational talks, among other activities, for the students from time to time. 3. College Standing Committees The Board and other Statutory Committees of the College are concerned with the consideration of all academic matters - for example, curriculum development, conduct of examinations and consideration of results, academic staff matters, determination of students’ academic standing and welfare, among other issues that might be brought before them from time to time. The Boards and the Committees are: a. College Board Composition 2 Industrial Chemistry “ “ “ “ “ “ “ “ Vice Chancellor – Chairman Dean, College of Natural and Applied Sciences Sub-Dean, College of Natural and Applied Sciences All Heads of Departments in the College of Natural and Applied Sciences All Professors in the College of Natural and Applied Sciences Dean of College of Business and Social Sciences or his/her Representative The Librarian or his/her Representative College Officer, Natural and Applied Sciences – Secretary b. College Board of Studies Composition “ Vice Chancellor – Chairman “ Dean, College of Natural and Applied Sciences “ Sub-Dean, College of Natural and Applied Sciences “ All Heads of Departments in the College of Natural and Applied Sciences ‘’ All Professors in the College of Natural and Applied Sciences “ All full time members of Academic Staff in the College of Natural and Applied Sciences not below the rank of an Assistant Lecturer “ One (1) Representative of College of Business and Social Sciences “ The Librarian or his/her Representative “ College Officer, Natural and Applied Sciences– Secretary c. College Board or Examiners of Natural and Applied Sciences Composition “ Vice Chancellor – Chairman 3 Industrial Chemistry “ “ “ “ “ “ “ Dean, College of Natural and Applied Sciences Sub-Dean, College of Natural and Applied Sciences All Heads of Departments in the College of Natural and Applied Sciences All full time members of Academic Staff in the College of Natural and Applied Sciences not below the rank of a Lecturer II One (1) Representative of College of Business and Social Sciences The Librarian or his/her Representative College Officer, Natural and Applied Sciences Secretary d. College Postgraduate Committee Composition “ Dean, College of Natural and Applied Sciences – Chairman “ All Heads of Departments in the College “ All Professors in the College “ Coordinators of Postgraduate Programmes in the College “ One Representative of the College on the Postgraduate School Board “ College Officer, Natural and Applied Sciences – Secretary e. College Appointments and Promotions (Academic) Committee Composition “ Dean, College of Natural and Applied Sciences – Chairman “ Sub-Dean, College of Natural and Applied Sciences “ All Heads of Departments in the College “ All Professors in the College “ Dean of College of Business and Social Sciences or his/her Representative 4 Industrial Chemistry “ College Officer, Natural and Applied Sciences – Secretary f. College Finance Committee Composition “ Dean, College of Natural and Applied Sciences “ Sub-Dean, College of Natural and Applied Sciences “ All Heads of Departments in the College “ College Officer, Natural and Applied Sciences “ One (1) Representative from each Department in the College “ College Finance Officer, Natural and Applied Sciences – Secretary g. College Seminars Committee Composition “ Dean, College of Natural and Applied Sciences “ Sub-Dean, College of Natural and Applied Sciences ‘’ One (1) Representative from each Department “ College Officer, Natural and Applied Sciences – Secretary h. College Management Committee Composition “ Dean, College of Natural and Applied Sciences “ Sub-Dean, College of Natural and Applied Sciences “ All Heads of Departments in the College ‘’ Programme Coordinators “ College Officer, Natural and Applied Sciences – Secretary 4. Structure of the College The College has three (3) Departments as listed below: 1. Biological Sciences 2. Computer Science and Information Technology 3. Physical and Earth Sciences 5 Industrial Chemistry The following degrees are awarded: 1. Biological Sciences a. B.Sc. Biochemistry b. B.Sc. Microbiology 2. Computer Science and Information Technology a. B.Sc. Computer Science and Technology b. B.Sc. Information and Communications Technology 3. Physical and Earth Sciences a. B.Sc. Geology and Mineral Sciences b. B.Sc. Physics with Electronics c. B.Sc. Industrial Chemistry 5. 1. 2. 3. 4. 5. 6. PAST AND CURRENT DEANS OF THE COLLEGE 2005 – 2006 Prof. M. B. Asokhia 2006 – 2007 Prof. C. O. Oluwole Alofe 2007 – 2010 April Prof. Rufus Oladiran Okotore 2010-2010 October Prof. Emmanuel A. Fayose 2010-2011 May Dr. Gbolagade. D. Gbolagunte (Ag) 2011 – Till Date Prof. Rufus Oladiran Okotore 6. PAST AND CURRENT VICE-DEANS OF THE COLLEGE 1. 2009 – 2010 Dr. Gbolagade D. Gbolagunte 7. PAST AND CURRENT OFFICERS OF THE COLLEGE 1. 2010 – Till Date Mrs. Christianah M. Majasan 8. S/N OFFICE OF THE DEAN NAME DESIGNATION QUALIFICATION 1. Prof. R. O. Okotore Dean B.Sc., M.Sc., Ph.D. 2. Mrs. Felicia .Y. Aina Personal Secretary NCE, Dip. In Computer Studies, WASC 6 Industrial Chemistry 3. Mrs. Bola Ngburuka Clerical Officer NCE, WASC 4. Miss. Idorenyin Udoh Clerical Officer WASC 5. Mrs. Aina Dosu Cleaner WASC 9. S/N COLLEGE OFFICE NAME DESIGNATION QUALIFICATION 1. Mrs. C. M. Majasan College Officer / Asst. Registrar B.Sc. (Ado – Ekiti) 2. Mr. David Osanyinbi Clerical Officer – Data Processing Cert. in Computer Studies, WASC 3. Mrs. Bukola Ojo Clerical Officer Grade II, WASC 4. Mrs. Bunmi Fariogun Assistant Chief Clerical Officer NCE, WASC, Diploma in Computer 5. Mrs. Dolapo Fakorede Clerical Officer Computer OND, WASC, Dipl. Computer Studies 6. Miss. Tinuke Abagun Clerical Officer – Computer WASC, Diploma in Computer Studies 7. Mr. Anietie Udoaka E. Clerical Officer – Computer WASC, Diploma in Computer Studies 8. Mr. Joseph Fashina Clerical Officer WASC 9. Miss. Omolola Omoniyi N.Y.S.C B.Sc, WASC 10. Mrs. M. O. Ibeh Chief Clerical NCE, WASC 7 Industrial Chemistry Officer 11. Mrs. Christianah Clerical Officer WASC 12. Mrs. Janet Omoniyi Cleaner J.S.S.3 13. Mrs. Sesan Akinpelu Cleaner WASC 10 HEADS OF DEPARTMENTS DEPARTMENTS 1. 2. 3. HEADS BIOLOGICAL SCIENCES Prof. A. W. A. Edwards; B.Sc, M.Sc, Ph.D COMPUTER SCIENCE AND INFORMATION TECHNOLOGY Prof. F. A. Forli; B.Sc, M.Sc, Ph.D PHYSICAL AND EARTH SCIENCES Prof. M. B. Asokhia; B.Sc, Ph.D 8 Industrial Chemistry 11 COLLEGE PHILOSOPHY AND OBJECTIVES Philosophy The philosophy underlying the programmes of the college is to produce graduates who are knowledgeable and competent to meet the demands of the world’s technology-driven economy. Today, the study of science whether Natural or Applied has become almost completely integrated, whilst Computer Science / information technology has become a general language of communication across the globe. The curricula of programmes in this College are designed to ensure that every student is empowered with the minimum skills required in Computer Science and Information technology and basic understanding in adjoining fields disciplines in the Sciences. Objectives 1. To produce graduates who have the ability to understand the basic language of all the disciplines in the sciences and communicate appropriately in the global language of Computer and Information Technology. 2. To produce graduates possessing the intellectual ability to identify and apply the state of art in various scientific disciplines to solve prevailing problems of disease and poverty. 3. To produce graduates who can comprehend, and proffer solutions to the ecological changes in the local environment. 4. To develop in students the potential to apply their knowledge and skills to solve research and theoretical problems in their respective discipline which will ultimately enhance their self-reliance and employment opportunity. 5. To prepare the students for career prospects in agriculture, health care delivery, mineral science, petroleum and oil industry. 9 Industrial Chemistry 12. ADMISSION REQUIREMENTS: COURSES/ REQUIREMENTS UTME SUBJECTS SPECIAL CONSIDERATION PROGRAMME (WAIVER) REMARKS S 1. Biochemistry Direct Entry UTME Two ‘A’ level passes chosen from Chemistry, Mathematics Physics and Biology. NCE/ND/HND in related field plus UTME requirement. Five SSCE credit passes in English Language, Chemistry, Mathematics, Physics and Biology. Biology, Chemistry, Physics or Mathematics. CRAWFORD accepts merit in own Diploma (credit/upper credit), OND (upper credit) or HND in relevant courses is acceptable. O/L credit in either Physics or Mathematics in addition to ‘A’ level passes in Chemistry and Biology is acceptable. 2. Industrial Chemistry (i) Two ‘A’ level passes in Chemistry and Mathematics (ii) OND in Science Technology or ND in relevant field with UTME requirements. Five SSCE credit passes in English Language, Chemistry, Mathematics, Physics and Biology/Agri c Science. Chemistry, Mathematics and any of Physics/Biology /Agric Science. CRAWFORD accepts Holders of OND (ND) certificate with minimum of upper credit pass are eligible for admission into year II (200 Level) provided that their programme cover certain basic courses offered in the school up to the second year. Holder of HND with minimum of lower credit pass are eligible for admission into year II depending on the appropriateness of their requisite academic. 3. Microbiology (i) Two ‘A’ level passes to include one of Botany, Zoology, Biology or Chemistry. (ii) OND/NCE in related fields. 4. Physics with Electronics NCE/Two ‘A’ level passes in Physics and Mathematics or Chemistry Five SSCE credit passes to include English Language, Mathematics, Chemistry, Biology and any other Science subject. NCE/Two ‘A’ level passes in Physics and Biology, Chemistry and Physics or Mathematics. Physics, Mathematics and Chemistry or 10 Industrial Chemistry Mathematics or Chemistry. 5. Geology & Mineral Sciences (i) Two ‘A’ level passes from Geology, Chemistry, Mathematics, Physics, Biology and Geography. 6. Computer Science and Information Technology (i) Two A/L Passes in science subjects including Mathematics (ii) NCE with at least Merit in Mathematics and one other Science or Social Science subject. (iii) Diploma in Data Processing with at least a merit pass from a recognized University or OND/HND in Data Processing, Engineering and Maths with an overall B grade may be considered. (except in Lagos). Biology. Five SSCE Any three of credit passes Chemistry, Physics, in English Mathematics, Language, Biology and Biology, Geography Chemistry, Mathematics and any other subject. Five SSCE credit Mathematics, passes to include Physics and English Language, one of Maths, Physics plus Biology, two other science Chemistry, subjects. Agric Science, Economics and Geography. ELIGIBILITY FOR ADMISSION An applicant must have completed 12 years pre-tertiary education i.e. someone who has finished six years of Primary School, three of Junior Secondary School (JSS) and three in the Senior Secondary School (SSS) in the Nigerian Educational System or to possess equivalent/superior credentials. In addition, applicants must take the mandatory University Matriculations Examination (UME). 13. REGISTRATION PROCEDURE 1. Requirements for Registration a. Original photocopies of credentials b. Birth Certificate 11 Industrial Chemistry c. Eight (8) passport photographs d. JAMB Notification of Results e. University Admission letter 2. Procedure for Course Registration (i) All students should note that Registration of courses commence on resumption for each semester. Students are therefore expected to register twice in a session. i. e. at the beginning of each semester. (ii) After the payment of school fees, students should proceed to the Bursary with proof of bank payment for a pin code for on-line registration. (iii) Students are expected to collect registration forms from Department the and then complete on consultation with the course adviser. Thereafter, the forms are forwarded to the Edu - Portal for proper documentation. (iv) Students are allowed a maximum of seven (7) weeks for registration and an additional two (2) weeks for late registration. (v) Any student that fails to register within this period ceases to be a bonafide student of Crawford University. 3. Add and Delete of Courses Any student wishing to delete course(s) will be allowed to do so within the first nine (9) weeks of registration. Any student wishing to add additional course(s) will be allowed to do so within the first seven (7) weeks of registration for both first and second semester. 14. REGULATIONS GOVERNING THE AWARD OF BACHELOR’S DEGREE (FULL TIME) 12 Industrial Chemistry (A) A programme of study shall be provided leading to a Bachelor’s degree to be denoted by the letters B.Sc (or such other abbreviation as Senate may approve from time to time) which may be awarded with honours or as a pass degree. The programme normally extends over a period of three or four academic years, depending on the student entry qualifications as follows: 1. i. Three years for direct entry candidate with prescribed GCE Advanced Level. Crawford Foundations students or equivalent admitted to the 200 level ii. Four years for students with WASC, GCE, Ordinary or equivalent qualifications, admitted to the 100 level. 2. i. A full-time student is one who carries not less than the minimum load stipulated in the College ii. The minimum duration for graduation for a four-year programme is a period of 8 semesters and 6 semesters for threeyear programme; while the maximum length of time required in the College shall not be more than 12 semesters for the four year programme and 10 semesters for the three-year programme. iii. The maximum load permissible per semester is 27 credit units whilst the minimum load is 18 credit units for full-time studentship. iv. The Dean may on behalf of the College Board permit students in exceptional cases to carry less than the minimum load or more than the maximum load, upon the recommendation by the Head of Department. (B) Graduation Requirements To be eligible for the award of a degree in the B.Sc. degree Programmes, a student must obtain a stipulated minimum total of units for a three-year programme or a maximum total of units for a 4 – year programme as stated in the Table below:13 Industrial Chemistry Minimum Number Units Programme Maximum of Number Units Microbiology 115 160 Biochemistry 124 158 Geology/Mineral Science 132 197 Industrial Chemistry 136 198 Physics with Electronics 127 177 & 114 159 Information & Communications Technology 138 163 Computer Technology Science of Student Academic Status A student’s academic status shall be determined on the basis of his performance in the Harmattan and Rain Semester Examination for each of the 100, 200, 300 and 400 levels of the degree programme. The following categorization of student’s status shall be used. (i) Good standing: To be in good standing, a student must * pass a minimum of 24 units per session and * have a Grade Point Average (GPA) of not less than 1.0 (ii) Probation: i. A student shall be placed on “PROBATION” if; * he/she has not passed a minimum of 24 units for a particular level * his/her GPA is less than 1.0 14 Industrial Chemistry ii. iii. (a) (b) iv. The period of probation shall be a maximum of two semesters A student on probation is allowed to register for courses at the next higher level in addition to his/her probation level courses provided that: The regulations in respect of student workload are compiled with, and The pre-requisite courses of the higher level courses have been passed. A student on probation who fails to improve on his/her cumulative grade point average (CGPA) of 1.0 and 24 units in the subsequent semester, such as to place him/her in good standing shall have another chance, therefore he/she will be asked to withdraw from the University. Transfer Cases 15. i. Students who transfer from other Universities shall be credited with only those courses relevant to the programme of the University, which the candidates have already passed. Such students shall however, be required to pass the minimum number of units provided that these students shall spend less than two (2) year (4 semesters in order to earn a degree of the University. ii. Students who transfer from one College to another within the University for any reason shall be credited with those units passed that are within the curriculum of the receiving College. COURSE ADMINISTRATION AND ASSESSMENT 15 Industrial Chemistry (A) Courses and Units i. A course unit is a series of is one hour lectures or tutorials or an equivalent combination of this type of instruction. No course shall be less than two units and more than six units. ii. There shall be four levels of courses for the 4 -year degree programme and 3 levels for the 3-year 100 – 199 – (100 level courses) 200 – 299 – (200 level courses) 300- 399 – (300 level courses) 400 – 499 – (400 level courses) Course numbers shall be prefixed by a three character course code which designated the academic discipline. (B) Course Status The following standard terminologies are used in all units of the Departments to indicate the status of each course. i. Compulsory: courses specified by a department which students must take and pass. ii. Required course: A course which a student must register for and pass at 40% before a degree can be awarded but which is not counted towards degree classification e.g. General Studies, Library use. iii. Elective: courses specified by a department from which a student must take in order to make up the required additional units for the award of the degree iv. Pre-requisite: A course for which knowledge is essential prior to taking another specified courses. A pre-requisite 16 Industrial Chemistry requirement is fulfilled by completing and passing the prerequisite courses which may also be waived for suitably qualified candidates by the College Board on the recommendation of the Department. v. Audited course: A course which the student attends but in which he/she is not examined. (C) Course Assessment i. All courses shall normally be evaluated by examinations and Continuous Assessment shall be done through essay and tests. ii. Scores from Continuous Assessment shall constitute 30% of the final marks for courses. (D) Examinations i. Each course shall normally be completed and examined at the end of the Semester in which it is offered. ii. A written examination shall last a maximum of three hours for three units of courses and minimum of two hours for two units of course. (E) Conduct during Examination i. Candidates must be seated at least 15 minutes before the commencement of each examination. Thereafter, no candidates will be allowed into the examination room except at the discretion of the Chief Invigilator. Candidates will not normally be allowed to leave the examination room. Outside these periods, candidates may leave the room temporarily only if accompanied by an attendant. 17 Industrial Chemistry ii. Candidates shall not be allowed to take into the examination room or have in their possession during the examination, any book or paper, mobile phone, printed or written document (whether relevant to the examination or not). iii. Any proven attempt made by candidate directly or indirectly to influence the process of examination or any part therefore with a view to obtaining undue advantage shall lead to the candidate’s disqualification from the whole examination. iv. Silence shall be maintained throughout the period of examination and communication among the candidates will not be allowed. v. Candidates shall comply with all instructions set out in the examination answer booklet or other examinations materials. They shall also comply with all instructions given to them by the invigilators. vi. Whenever there is an alleged examination malpractice, the candidates involved shall be required to make a signed statement immediately. Failure to comply shall constitute a serious offence and lead to disqualification from the examination and any other disciplinary action deemed appropriate. A proven case of examination malpractice may lead to dismissal from the University. vii. Candidates must present themselves to all University examinations for which they have been duly registered. Candidates who fail to do so for reasons other than illness or accident attested to by the Chief Medical 18 Industrial Chemistry Officer or the University shall be deemed to have scored Zero in that examination. (F) Pass – Mark The minimum pass-mark in any course shall be 40%, (for Prerequisite purpose, 35% is the specified minimum). (G) Grading System: Grading of courses shall be done by a combination of percentage marks and letter grades translated into graduated system of grade point equivalent. For the purpose of determining a student’s standing. At the end of every session, and for the final degree classification, Grade Point Average (GPA) system shall be calculated, that is: GPA = TCP/TNU Where TCP (GP x Unit) TNU (Total Units of courses taken), TCP (Total Cumulative Point Each course unit shall be graded out of a maximum of 100 marks and assigned appropriate letter grade point equivalent as in the following table: MARKS LETTER GRADE GRADE POINT 70 AND ABOVE A 5 60 – 69 B 4 50 – 59 C 3 19 Industrial Chemistry 45 – 49 D 2 40 – 44 E 1 0 - 39 F 0 (H) Presentation of Results Result from the Department shall be presented to and considered by the College Board of Examiners at the end of each semester. The standard format approved by Senate shall be used. The approved results shall be forwarded through the Head of Department and Dean to the University Exams & Records Division for processing. (I) Classification of Degree The determination of the class of degree shall be based on the Cumulative Grade Point Average at the 100, 200, 300 and 400 levels, the Cumulative Grade Point Average (CGPA) shall be determined at the end of each semester taking into consideration, all the courses so offered, and approximated to 2 decimal places. The Cumulative Grade Point Average (CGPA) shall be used for the determination of the class of degree according to the following ranges: CGPA CLASS OF DEGREE 4.50 – 5.00 First Class Honours 3.50 – 4.49 2.40 – 3.49 Second Class Upper Second Class Lower 1.50 – 2.39 Third Class 20 Industrial Chemistry 1.0 – 1.49 16. Pass COUNSELLING Student’s counseling is an important activity of the Departments, which is aimed at ensuring academic success for all the students. Students are normally attached to a lecturer who is regarded as a senior partner for the success of the students. The lecturer is referred to as the Level Coordinator/Adviser. He/she is responsible to the entire students for that level in each department. 17. INFORMATION MEDIUM (i) Information meant for students are normally pasted on the notice boards. It is the responsibility of students to go to these boards regularly to ensure that they keep abreast of the happenings in the Department and College as regards their programme in the University. The Department and College would therefore not be responsible for negligence on the part of the students for failing to comply with any directives of the departments or its units given through the medium of the notice boards. (ii) Students’ Colloquium and Parents Forum The University Management holds a ‘Students Colloquium’ at least once every semester for both students and lecturers. This is an interactive session that touches on all aspects of student life; that is welfare, student behavior, dressing and attendance at church services and other related activities. In addition, the Parent Forum holds regular meetings at least twice in a session to discuss 21 Industrial Chemistry matters related to the welfare of their wards the good governance, and progress of the University at large. 18. DISCIPLINE The College does not take kindly to acts of indiscipline on the part of students. Degrees are awarded for deserving student by the Departments having been found worthy in character and in learning. Acts such as insubordination acts of violence or any behaviour that borders on disrespect to the constituted authority of the University are treated with utmost seriousness and appropriate punishment given, when guilty. Students are, therefore, advised to take their studies seriously and obey regulations. 19. GENERAL STUDIES PROGRAMME All students of the University are required to pass the General Studies Programme courses (GST) as a condition for graduation. The General Studies Courses are University based. These include: Use of English/Library and Information Sources; Introduction to logic and philosophy, Music Appreciation. These (GST) courses are compulsory for all students irrespective of their level of admission. This also applies to students transferring from other Universities. (i) Entrepreneurial Development Studies (EDS) Based on the Federal Government directives to all Nigerian Universities, the University has introduced two courses on Entrepreneurship. These courses pertain to both theoretical and practical aspects of Entrepreneurship and are taken by students at the 200 Level and 300 Level in the College. 22 Industrial Chemistry 20. CODE OF CONDUCT All students, be they freshmen or returning, are required to sign the CRU code of conduct at the beginning of every session. Without prejudice to existing rules and regulations, this code of conduct shall guide the behavior of students in the university. 1. All secret cults, confraternities and similar organizations in the university are illegal. Any students of the university found to be member, sponsor, or patron of such organization shall be liable to expulsion from the University. 2. The possession, carrying or use of arms and dangerous weapons by the students on campus is illegal and any student found to possess, carry or use such weapon shall be dismissed from the university 3. Any student who threatens or in any way endangers the life of any students or members or staff or engages in physical fight on campus shall be liable to strict disciplinary action, which may lead to expulsion. Students should in addition note and are reminded that causing bodily harm, rape and threat to life are criminal offences and will be reported to the police. 4. Consumption and use of alcoholic beverages and liquor on campus by students are prohibited and any student caught using and consuming such beverages and liquor shall face disciplinary action. 5. All students, organizations, societies, clubs and association are to be registered with the Students’ Affairs division with three copies of their constitution and a list of the names of their executive members, staff advisers, patrons and sponsors. 6. Students are also reminded that suspension from University is suspension from participation in academic activity. Suspended student who continues to attend or attempts to attend academic lectures or course or participate in any other students’ activities on campus while suspension is still in force shall be summarily expelled from the University 23 Industrial Chemistry 7. No mosque, church or any house of prayer or worship on the campus shall be used as residence or for residential purposes by any student. Any such building known or used as a residence or for residential purposes shall be closed forthwith. 8. (a). The use of all Auditoria on campus shall be subject to obtaining a written approval. (b). All forms of students’ social activities that involve drumming and singing should be restricted to the students arcade. 9. Any student found defacing the University walls, posters and other University property, disrupting academic activities for whatever reason and taking over the work of the security officers by locking the gate or hijacking vehicles will be liable for severe disciplinary action, which may lead to suspension or expulsion depending on the severity of such misconduct. 10. All posters and handbills for distribution by students must be cleared and approved by Students’ Affair before distribution; any contravention may lead to suspension . 11. Any student on probation for two consecutive periods shall be asked to withdraw from the University. Students on probation would not be considered for inter-faculty transfer. 12. Any interference on matters of discipline from whatever quarters shall be resisted. 13. There must be strict adherence to a well-defined official line of communication between students and the University authorities. 14. All religious activities including drumming and singing should be restricted to the Chapel or Mosque. 15. Until further notice, no social and religious activities on the University Campus should extend beyond 6.00p.m. 16. As much as the University respects freedom and appreciates the maturity of our students with regards to mode of dressing and comportment on the campus, indecent and sexually provocative dresses are not allowed. Students not properly dressed are normally disallowed access to lecture halls, the library and other 24 Industrial Chemistry official places. Lecturers and the official of the university have the right to deny attention at offices or admission into lecture or examination halls to students not properly or decently dressed. 17. All students are requested to report any infractions or contravention of any of these rules or any other University rules or regulations either to: (i) The Registrar (ii) Dean of students’ Affairs and /or (iii) University Security Agents 21. EXAMINATIONS Examination Malpractices The department frowns seriously at any act of examination malpractice. The penalty for examination malpractice is expulsion. Approved Procedure for the Re-Assessment of Examination Script The complainant will submit in writing an application for re-marking to the Head of Department clearly stating the reasons in writing and copy the Vice-Chancellor and the Dean of the college. Student will then pay a prescribed fee N1, 000 for a re-assessment. The Head of Department conducts a discrete investigation into the request and takes one of the following actions: i) Advises the student to drop the request if he finds no substance in it. ii) Where a complainant is dissatisfied with advice of the head of Department in (i) above, the following procedure will operate iii) The complainant pays the sum of N3,000 to the University iv) Makes the request for remarking to the Dean of the College through the Head of Department clearly stating his/her reasons in writing. v) Depending on the prevailing circumstances, the remarking could be undertaking by the head of Department or any other lecturer who could make professional judgment on the 25 Industrial Chemistry course being remarked and on the lecturer. The Dean, in consultation with the Head of the Department or any other suitably qualified person, sends a sample representing the spread of the grades in the course together with the questions and making scheme to external examiner or any other expert in the subject who is not lower in rank than the internal examiner. The decision to the external examiner shall be final and the Dean shall report the outcome of the exercise to the Vice-Chancellor. Any disciplinary action that might arise from a request for a re-marking shall be treated according to existing regulations governing such matters. Re-sit Examination There shall be NO RESIT EXAMINATION in any course offered. However, students may retake the course after they have attended lectures at the next available opportunity. 22. STUDENTS’ RESPONSIBILITIES It is the responsibility of each student to ensure the following: (a) Prompt registration at the beginning of each semester (b) Regular attendance at lectures (c) Quick response to official calls (d) Completion of all academic assignments (e) Effective use of the library and studying at his/her convenience (f) Close relationship with his or her level adviser (g) Good preparation and success in all examinations (h) Compliance with all rules and regulations of the university (i) Eschew all acts that can lead to suspension or expulsion from the university. Some of such serious acts are joining cult and examination malpractice. To this end, students should know that their success or failure depends on how they are able to manage their resources and comport themselves in the university. 26 Industrial Chemistry 23. STAFF OFFICE HOURS Lecturers in the department keep office hours that are displayed on the door of each academic staff. ACADEMIC REGULATIONS THE COURSE UNIT SYSTEM AND GOVERNING THE AWARD OF A DEGREE REGULATIONS ACADEMIC INFORMATION Crawford University runs the course unit system (cus). This simply means the way courses offered in the University is quantified in units as well as the quantification of an academic session into semesters. each academic session is divided into two semesters. These are: Harmattan semester and Rain semester each semester consists of 15 teaching weeks and 2 weeks of examinations. DESCRIPTION OF THE COURSE UNIT SYSTEM (CUS) The CUS is an operational system in which the entire programme of courses required by a student for a particular Degree is packaged into a number of modules each consisting of a prescribed number of credits. Usually one module is to be offered in one semester. Thus, the student’s workload in a semester is defined in terms of credits where one credit represents one hour of lecture or one hour of tutorials or two to four hours of practical work per week throughout the semester, normally of fifteen weeks’ duration. Depending on the programme, a degree programme is normally packed into eight or ten modules of courses for students coming through the University Matriculation Examination (U.M.E) and less for those coming by direct entry or transfer. 27 Industrial Chemistry MECHANISM OF THE COURSE UNIT SYSTEM (CUS) (i) Registration for courses This is normally at the beginning of each semester. Each department appoints an Adviser for each student whose duty it is to monitor the student’s academic progress and advise him/her appropriately as to how many units he/she should register for in that semester. The University regulations for a semester stipulate a minimum of 15 credits and a maximum of 24 credits for full time studentship. The average number of credits (or workload) is about 20. Other regulations governing registration such as the late registration and penalty may be obtained from the Registry. (ii) Adding and Dropping Courses A student may withdraw from a course for which he/she has registered without running afoul of regulations on registration and examination only with the approval of the Dean of his/her College. Permission to withdraw from the course must be sought by completing a drop form counter-signed by the course instructor or the Head of Department. (iii) Continuous Assessment This is a feature of the CUS, which makes it unique. It provides for a continuous evaluation of the students academic performance in a given course. The evaluation may take the form of take-home assignment, tutorials, class tests and quizzes, reports and any such other means as may be appropriate and consistent with the objective and conduct of the course, as determined by the department offering the Course. Assessment of the performance in tests, tutorials etc. will be used in determining the student’s overall grade in the course and constitute 30% or 40 % of the overall grade. TERMINOLOGY 28 Industrial Chemistry In order to understand the operation of the CUS, the following are hereby explained. (i) Semester: A semester is one half of an academic year as determined by Senate. (ii) Compulsory Course: A compulsory course is a University course which must be registered for and passed by students before obtaining a degree. (iii) Required Course: A required course is a course which the student must register for and pass at 40% before a degree can be awarded but which is not counted towards degree classification e.g. General Studies, Library etc. (iv) Elective Course: an Elective Course is a course which may be taken to make up the minimum required of units to increase the number of units subject to the prescribed maximum allowed by the Regulations. All electives must also be passed at 40 %. (v) Pre-requisite Course: A course, the knowledge of which is essential, prior to taking another specified course. (vi) Concurrent Course: Specified courses, which must be taken within the same semester (vii) Audited Course: An audited course is a course which the student attends but in which he or she is not examined EXAMINATIONS AND GRADING SYSTEM The issue of Examination is a logical follow-up of the discussion of registration. The University has a set of Examination Regulations. a) Pattern of Examinations: Each course shall be examined at the end of the semester in which it is offered. b) Measurement of Performance: A student’s performances in the Course shall be measured in terms of: (a) The scores in the continuous evaluation 29 Industrial Chemistry (b) The results of the prescribed theory and or practical examinations in the course LEVELS OF PERFORMANCE The grades awarded for a course are as follows: Mark Range (%) Letter Grade Interpretation 70 – 100 A Excellent 60 – 69 B Very Good 50 – 59 C Good 45 – 49 D Satisfactory 40 - 44 E Fair only 0 – 39 F Failure Semester Performance A student’s performance in a semester is computed to obtain the Grade Point Average (GPA). This involves the awarding of credit points in respect of each course taken during the semester. To this end, numerical values are attached to the letter grades earlier mentioned as follows: A - 5 Credit points per unit of course B - 4 Credit points per unit of course C - 3 Credit points per unit of course D - 2 Credit points per unit of course E - 1 Credit point per unit of course F - 0 Credit point per unit of course 30 Industrial Chemistry The GPA is obtained as the ratio of the Total Weighted Grade points (TWGP) to the Total Credit Offered (TCO) during the semester. Thus GPA = TWGP ÷ TCO Cumulative Performance While the GPA specified above is used to measure the performance of a student in a given semester, the Cumulative Grade Point Average (CGPA) is the one that really determines the student’s overall academic standing and therefore, his continued stay or otherwise in the University. It is also the CGPA that is used to classify the Degrees awarded Students in their final year. The CGPA is obtained as the ratio of all the weighted points accumulated since entering the University to the total number of credits units registered for since coming into the University. In other words, CGPA is equal to the Total Credit Point (TCP) divided by the Total Number of Units (TNU) offered thus TCP ÷TNU All CGPA calculations are to two places of decimal. Incomplete Grade When for valid reasons, a student is unable to complete all the prescribed requirements for a course in which he/she is formally enrolled, he/she may, on the recommendation of the department concerned, be awarded an incomplete grade. Such a grade shall be removed when the department certifies that all prescribed requirements have been met. But in any case, not later than one semester after the course. Academic Probation A Student who’s CGPA at the end of semester is less than 1.00 shall be placed on Academic Probation during the subsequent semester. 31 Industrial Chemistry Withdrawal from the University A Student who is on academic probation in a semester and fails to achieve a CGPA of at least 1.00 at the end of the session may be advised to withdraw from the University. Release of Examination Results At the end of each semester, a provisional result of course Examinations shall be published by the College Secretary soon after the ratification of the recommendation of the College Board of Examiners. The Registrar shall publish the final results of the semester Examinations as soon as the Senate has approved them. Repetition of Courses Any compulsory, elective or required course failed by a student must be repeated until it is passed, or otherwise stated by the regulations. A student may repeat only those courses in which he has obtained a grade of F. The grade earned in a repeated course shall be recorded and used in the computation of the GPA, CGPA in the usual way. Requirements for the Award of a Degree To be eligible for the award of a Degree, a candidate must satisfactorily complete the minimum number of credits prescribed for the Degree. He/she must, in addition, complete successfully all compulsory courses as well as the special and free electives for the degree as prescribed. A repeated course cannot be counted twice in fulfilling the requirement for minimum number of units. Residency Requirements To qualify for a Degree in the University, each candidate shall normally be required to spend a minimum period of three, four or five academic years at Crawford University depending on the programme and mode of entry. RULES AND REGULATIONS GOVERNING THE CONDUCT 32 Industrial Chemistry OF EXAMINATIONS ELIGIBILITY All students who are registered for courses in a given semester are eligible to sit for examinations in those courses except students in the following categories: (i) a student who is absent from the University for upwards of three weeks without official permission. Such student shall normally be deemed by Senate to have withdrawn from the Course and its examination for that semester, (ii) a student who fails to attend up to 70 percent of lectures or practical in any course. INSTRUCTIONS TO CANDIDATES Candidates shall: (i) Be admitted into the examination hall only on the production of the University identity card, (ii) Ensure that he/she acquaints himself/herself with and adheres strictly to the instruction governing examinations in the University, including those printed on the front cover of the examination answer booklets, (iii) have the full responsibility of ensuring, before the commencement of any examination or test, that nothing incriminating is found on his/her person or on materials he/she legitimately brought into examination hall ,e.g. rulers, four figure tables, etc., (iv) Conduct him/herself in an orderly manner and obey all the instructions of the invigilator/examiner, 33 Industrial Chemistry (v) Not be engaged in, or attempt any manner of examination malpractice, (vi) Not go into the examination hall before they are allowed in by the invigilators. They are also advised to keep strictly to the seating arrangement to avoid confusion. No candidate should, under any circumstances, remove chairs arranged in halls used for examination purposes, (vii) Report at the examination venues punctually at the time scheduled for their papers. Candidates arriving later than half an hour for an examination may be refused entry into the examination hall, (viii) bring with them to the examination hall their own ink, pen, ruler, eraser and pencil and any material which may be permitted by this regulation (as stated hereunder).They are however, not allowed to bring any books or papers, except those that may be permitted or provided by the Department responsible for the examination being held. Candidates are warned in their own interest to ensure that lecture notes, textbooks, jotters, bags or any other unauthorized materials or aids etc are not brought into the examination hall, (ix) Not be allowed to be in possession of Mobile Phones or equivalent handsets in the examination hall. While any examination is in progress, no handset should, therefore, be found on any candidate, (x) Not engage in communication of any kind with one another during the examination. Any candidate found to be giving or receiving irregular assistance shall face disciplinary action, 34 Industrial Chemistry (xi) Observe silence in the examination hall. The only permitted way of attracting the attention of the invigilator is for the candidate to raise his/her hand, (xii) Not use scrap paper. Rough work must be done in the answer booklet, crossed neatly through and submitted along with the answer booklet/script, (xiii) Bring their own mathematical or drawing instruments. Personal copies of Mathematical Table will not be allowed in the examination hall (see Regulation 2.18 on the use of calculator), (xiv) Use their Matriculation number for the examination and not names, (xv) Before handing in their answer scripts at the end of the examination, satisfy themselves that they have inserted, at the appropriate place, their Matriculation numbers and the numbers of the questions answered, except for the question paper and any other materials they may have legitimately brought with them. Candidates are not allowed to remove or mutilate any paper or materials supplied by the University, (xvi) Not normally be permitted to leave the examination hall during the first and last 30 minutes of any examination, (xvii) At the end of an examination remain seated while invigilators go from row to row to collect answer scripts, and (xviii) Be required to sign against their Matriculation Number on the Attendance Register at the beginning of the examination and when submitting the answer booklet/script. 35 Industrial Chemistry (i) (ii) (iii) (iv) (v) (vi) (vii) (i) (ii) USE OF CALCULATORS For examinations in certain courses, the use of electronic calculators is permitted, but the calculators must be nonprogrammable. Only one calculator shall be allowed per candidate. Organizers are not permitted. The calculator must be small (hand-held) and battery operated. A candidate must not borrow another candidate’s calculator during an examination. The responsibility for correct operation of the calculator rests with the candidate alone. Instruction manuals, organizers, calculator packets and containers are forbidden in the examination halls. Invigilators and Examinations Assistants shall confiscate them whenever and wherever they are discovered in the examination halls. Calculators must be switched off on entry into the examination room and can only be turned on when ready to be used. Candidates shall declare their calculators and make them available for inspection by invigilators on entry into the examination hall. Contravention of any of these regulations shall constitute examination malpractice or misconduct. INSTRUCTIONS TO INVIGILATORS Invigilators shall normally allow candidates into the Hall ten (10) minutes before the commencement of the examination and ensure that they sit in an orderly manner in spaces marked according to their Matriculation Numbers. Blank answer booklets and graph papers, where required, shall then be distributed. About five (5) minutes before the commencement of the examination, the envelopes containing the question papers shall be opened and the papers distributed face 36 Industrial Chemistry down, while the candidates are warned not to start until they are told to do so. (iii) At the scheduled time for the commencement of the examination and after the distribution of papers has ended, the Invigilators shall ask the candidates to start, and note the exact time of commencement and the exact time to end the examinations, depending on the amount of time allowed for the various examinations holding in the hall. (iv) Invigilators shall pass round the candidates the Attendance Registers corresponding to their courses for the candidates to fill and sign at the beginning and end of the examination. (v) Invigilators shall familiarize themselves with instructions to candidates and enforce the rules and regulations contained in these instructions. (vi) Invigilators shall exercise constant and vigilant supervision over the candidates. (vii) In any case of examination misconduct by candidates, the Chief Invigilator shall require the candidate(s) concerned to write and sign a statement on the incident, and allow the candidate(s) to proceed with the examination. The Chief Invigilator shall report such cases to the Dean, the Chief Examiner and Head of Department concerned within 24 hours. (viii) Invigilators shall ensure that candidates bring only authorized materials into the examination hall. Bags, books and other candidates' properties must be left outside the Examination Hall. For this purpose, Invigilators shall inspect the hall after candidates have been seated before the commencement of each examination. (ix) No candidate may leave the examination hall during the first half-hour of an examination except to go to the rest 37 Industrial Chemistry room or the first-aid room, accompanied by an attendant or Invigilator. (x) Normally, no candidate shall be admitted after the first half hour of the examination, and no question paper shall be removed from the hall before the first-hour of the examination has elapsed. (xi) If any candidate finishes his/her paper before the time required, the Chief Invigilator may at his/her discretion allow the candidate to submit his/her answer booklet and depart, (xii) Invigilators should ensure that silence is maintained in the examination hall. The only way of attracting the attention of the invigilator is the candidate to raising his/her hand. (xiii) Invigilators must warn candidates of the time, 30 minutes and 5 minutes before the close of an examination. (xiv) At the close of each examination, invigilators should go round to collect from candidates their answer booklets/scripts and check them against the Attendance Register. The candidates should sign the Attendance Register and be allowed to leave. (xv) The invigilators should enclose the collected answer booklets/ scripts and the corresponding Attendance Registers in the special envelopes provided by the Chief Examiner. (xvi) The Chief Invigilator should sign and seal the envelopes and submit them to the Chief Examiners concerned. ABSENCE FROM EXAMINATION Candidates must present themselves at such University Examinations for which they have registered under these regulations. Candidates who fail to do so for reasons other than ill-health, accident or other exceptional causes shall be deemed to have failed that examination. . 38 Industrial Chemistry Mis-reading of the time-table and such lapses on the part of the candidates shall not be accepted as a satisfactory explanation for absence. A student who falls ill during an examination should report in writing to the Dean of his/her College through his/her Head of Department with a report from the University's Director of the Health Care Unit. A student who is absent from an examination on account of illness confirmed by Medical evidence from the University Health Care may obtain the permission of Senate to make up the examination on another occasion. Otherwise, he/she shall take the regular examination on the following occasion. Approval for a make-up examination shall be by Senate on the recommendation of College Board. EXAMINATION MISCONDUCT Examination Malpractices include: a) Possession of question papers before examination/test or an attempt to do so, b) Swapping examination/test, of answer before, during or after a) bringing into the examination hall any unauthorized piece(s) of paper whatsoever, b) tattooing: inscription of answers, hints or codes thereof on any part of the candidate's body/dress, or in any other manner whatsoever, c) passing information from one candidate to another in the examination hall, d) seeking or soliciting any assistance whatsoever from any other student or any other unauthorized person in the examination hall, 39 Industrial Chemistry e) any disorderly conduct before, during or after any examination or test, f) pre-arranged sitting pattern by any student or group of students in the examination hall with a view to facilitating unauthorized exchange of information, g) a candidate arranging with another person to write an examination on his/her behalf, h) unauthorized possession of the University answer Booklets or attempts thereof, i) assaulting/manhandling Invigilator and/or attendant, j) any action or inaction of any student in and around the examination hall, which is inimical to or subversive of the integrity of the university examination process, such as the offences listed above, shall constitute examination misconduct and k) Offering information/assistance and accepting information/assistance from another student during examination is a breach of examination regulations and both carry equal punishments. HANDLING OF CASES OF EXAMINATION MALPRACTICE (i) Examination misconduct shall be processed through the Students’ Disciplinary Committee. (ii) The Chief Invigilator shall require the candidates concerned to write and sign a statement on the incident and allow the candidates to proceed with the examination. (iii) The Chief Invigilator shall write forward the case to the Chief Seurity Officer who will investigate the case and after investigation, shall forward his recommendation to the Head of Department concerned who will report to the Dean. 40 Industrial Chemistry (iv) On receiving the report, the Dean shall after writing his own comment shall forward the case to the Vice Chancellor. (v) At his discretion, the Vice Chancellor may act on the report submitted by the Dean or forward it to the Student Disciplinary Committee for advice. At the discretion of the Chief Invigilator, a candidate may be required to leave the examination room when his/her conduct is judged to be disturbing or likely to disturb the examination. The Chief Invigilator shall submit a written report on any such action to the Head of Department and the Dean of his/her College immediately after the end of the examination. (vi) 41 Industrial Chemistry EXAMINATION OFFENCES AND SANCTIONS Examination offences and sanctions to be imposed are as follows: S/N Punishment (maximum) Offence Unless otherwise stated (i) Non-display of ID card Rustication (ii) Noise making during an examination Rustication (iii) Refusal to submit oneself for search by Rustication for an Invigilator one semester (iv) Use of scrap papers with written notes in Expulsion Examination hall (v) Irregular possession of the University Expulsion Answer sheets (Whether used or unused) (vi) Mutilation or removal of any paper or Expulsion answer script supplied (vii) Failure to submit answer script to Expulsion invigilator after an examination (viii) Oral communication between candidates Expulsion during an examination (ix) Communication involving passing of Expulsion notes or other accessories to aid performance in an examination 42 Industrial Chemistry S/N Punishment (maximum) Offence Unless otherwise stated (x) Possession or use of any material such as Expulsion notes, scraps, etc, to aid performance in an examination (xi) Refusal to sit for and/or preventing other Expulsion students from sitting for an examination (xii) Smuggling of prepared answer scripts into an examination hall or submission of same under false pretence that they were Expulsion prepared in the examination hall. (xiii) Smuggling of cell phones or Expulsion unauthorized books into the Examination (xiv) Possession and/or acquisition of live Expulsion Question paper (xv) Arrangement with another person to Expulsion write Examination (xvi) Assault on Invigilator Examination Attendant and /or Expulsion (xvii) Absence from examination without due Appropriate Authority Sanction Any other misconduct concerning examination (not being one of those listed above), which is inimical to or subversive to the integrity of the University examination process, shall be an offence, which could attract appropriate sanction. 43 Industrial Chemistry INDUSTRIAL CHEMISTRY 44 Industrial Chemistry ACADEMIC STAFF Name Qualification Designation E. K. OKOH B.Sc, Ph.D O.A. BAMGBOYE U.U. EGEREONU O.O. AYEJUYO G.O. OLUWADARE K. A. YUSUF B.Sc, Ph.D A. N. MADU B.Sc; M.Sc. Ph.D Reader (Associate) Professor (Associate) Professor (Associate) Reader (Sabbatical) Reader (Associate) Senior Lecturer (Associate) Lecturer 11 A.D. FOLAWEWO R.O. OGBODU B.Sc, M.Sc. A.T. ODULARU B.Sc. , M.Sc R. A. ALANI B.Sc, M.Sc, Ph.D B.Sc, Ph.D B. Sc, Ph. D B.ScM .Sc B.Met, M.Met Ph.D. B. Sc. Ph. D. B.Sc., M. Sc Assistant Lecturer Assistant Lecturer Assistant Lecturer (Study Leave) Lecturer 11 (Associate) Area Of Specialization Organic Synthesis Environmental Chemistry/Inorganic Analytical Chemistry Environmental Chemistry -Extractive metallurgy Environmental Chemistry Solid-State Inorganic Chemistry Pharmaceutical Chemistry -Physical Chemistry -Food Chemistry Analytical Chemistry S.K.OGUNBOWALE NON-ACADEMIC STAFF AIST, PGD, Asst. Chief M.Sc.(LASU) Technologist K. OSUNLEYE G. C. E. O/L Lab. Assistant Abagun Atinuke Clerical Officer – Computer Ojo Christianah Clerical Officer 45 Industrial Chemistry PHILOSOPHY OF THE DEPARTMENT Industrial Chemistry is the index of industrial development everywhere in the world. The frontiers of Chemistry are very large, ranging from one extreme of natural products to those of synthesized by man. The enormous strides made by man in the understanding, exploration of nature and synthesis of new products all have their roots in Chemistry and Industrial Chemistry/ Chemical Technology. The degree programme is designed in such a way as to provide the students with a sound, broad, relevant and balanced theoretical and practical foundation in modern aspects of Chemistry and Industrial Chemistry to pursue a career in production, management, research and development in the chemical and allied industries of Nigeria. They are also provided with broad mental skills for a cutting-edge competence in design of process methodology and analysis of products, raw materials, as well as, intermediates. The training will enable the students to discharge their initiatives in tasking industrial processes/chemical processes, especially the unfamiliar ones. The intellectually equipped students will be able to proffer meaningful solutions to any environmental and industrial problem to enhance remarkable economic sustenance and development in Nigeria as well as other African nations and beyond. The students’ knowledge will however, not be limited to chemical/industrial processes alone, but will ramify with environmental, biochemical applied science and technology. OBJECTIVES The objectives of the bachelor degree in Chemistry/Industrial Chemistry include the following: 1. (a) To develop the students’ interest in Chemistry and Industrial Chemistry and their applications in the areas of industrial chemical process of raw materials and finish products, as well as, synthesis of new materials and products. 46 Industrial Chemistry (b) To acquaint the students with classical and instrumental methods of analysis, as well as, modern and current analytical techniques. (c) To expose the students to various quality control analysis in industrial, food, Pharmaceutical, metallurgical and petrochemical industries. (d) To develop the students to appreciate the importance of research and development, capital and labour requirements, technical and scale services. (e) To enhance the students’ knowledge of physical and chemical instrument in environmental sciences as well as impact assessment in environmental studies. (f) To develop the students knowledge of clinical aspect of chemistry, and its application to routine analysis. 2.(a) To develop in students the potentials to apply their knowledge and skills in revolving and solving research and theoretic problems in Chemistry which ultimately will enhance the self reliance and employment opportunities. (b) To create in the students the potentials to manage industrial production as entrepreneur, as well as, to develop industrial process techniques for sustainability. 3. To assist the students in unlocking natural resources for the benefits of humanities 4. To prepare students for graduate studies in specialized areas of Chemistry/Industrial Chemistry and multidisciplinary areas. 47 Industrial Chemistry ADMISSION REQUIREMENT a) UME ENTRY REQUIREMENT The minimum entry requirement for admission into either Chemistry or Industrial Chemistry in the department of Chemistry sciences is five O’level (SSCE/NECO/GCE or Equivalent). Credit level passes in English Language, Mathematics, Chemistry, Biology and Physics obtained in not more than two sittings. However, it is not allowed to present passes obtained in a combination of different examination bodies. The UME subjects required include English Language, Chemistry, Physics and Mathematics. b) DIRECT ENTRY REQUIREMENTS Holders of OND (ND) certificate with minimum of upper credit pass are eligible for admission into year II (200 Level) provided that their programme cover certain basic courses offered in the school up to the second year. Holders of HND with minimum of lower credit pass are eligible for admission into year II, depending on the appropriateness of their requisite academic preparation. Holders of two A ‘level subjects passes including Chemistry and one of Physics, Mathematics are also eligible for admission into year II (200 Level) programme in any of the Chemistry courses. In addition to fulfilling the requirements stated in (b) above, a holder of OND (ND), HND or A’ level must also have five O’level credit passes as in (a) above. GRADUATING REQUIREMENTS The minimum number of units a student must obtain to qualify for the award of a bachelor’s degree in either option shall be 160 units with the 48 Industrial Chemistry exception of direct entry students which must be 115 units. The Cumulative Grade Point Average (CGPA) regulation shall be applied to determine the class of a degree. 49 Industrial Chemistry COURSE STRUCTURE FIRST YEAR (100-LEVEL COURSES) HARMATTAN COURSE CODE COURSE TITLE STATUS L P T UNITS HARMATTAN SEMESTER CHM 101 GENERAL CHEMISTRY I (PHY. & INORG.) C 30 00 10 3 MTH 101 ELEMENTARY MATHEMATICS I C 30 00 10 3 INTRODUCTORY BIOLOGY C 30 00 10 3 C 30 00 10 3 BIO 101 PHY 101 GENERAL (MECHANICS) PHYSICS I PHY 103 ELECTRICITY & MAGNETISM C 30 00 10 3 CHM 107 GENERALCHEMISTRY PRACTICAL C 00 10 00 1 GST 101 USE OF ENGLISH / LIBRARY & INFO. SOURCES C 20 00 10 2 GST 103 MUSIC APPRECIATION I R 10 15 00 0 PHL 101 INTRODUCTION TO LOGIC & PHILOSOPHY I C 20 00 10 2 CSC 101 INTRODUCTION TO GENERAL COMPUTING C 30 00 10 3 CHM 107 C 00 10 00 00 1 TOTAL UNITS 23 COMPULSORY: 23 REQUIRED: 0 COURSE CODE FIRST YEAR (100-LEVEL COURSES) RAIN COURSE TITLE STATUS L P T UNITS 50 Industrial Chemistry RAIN SEMESTER CHM 102 GENERAL (ORGANIC ) CHEMISTRY II C 30 00 10 3 CHEMISTRY C 00 30 00 2 C 30 00 10 3 C 30 00 10 3 CHM 108 GENERAL LABORATORY MTH 112 ELEMENTARY MATHS II PHY 112 GENERAL PHYSICS SOUND AND OPTICS) STA 122 INTRODUCTION TOPROBABILITY THEORY I C 30 00 10 3 GST 102 USE OF ENGLISH/LIBRARY & INFO.SOURCES II C 20 00 10 2 GST 104 MUSIC APPRECIATION II R 10 15 00 0 PHL 102 HISTORY AND PHILOSOPHY OF SCIENCE C 20 00 10 2 *PHY 106 GENERAL PHYSICS LAB. C 00 30 00 2 CSC 102 INTRODUCTION APPLICATION R 30 00 1 3 II(HEAT, COMPUTER TOTAL UNITS 23 COMPULSORY: 20 REQUIRED: 3 NB:* To be done through both semesters REQUIRED: 3 51 Industrial Chemistry SECOND YEAR (200-LEVEL COURSES) RAIN COURSE COURSE TITLE CODE STATUS L P T UNITS RAIN SEMESTER CHM 202 INTRODUCTORY ANALYTICAL CHEMISTRY C 30 00 10 3 CHM 206 INDUSTRIAL CHEMISTRY C 30 00 10 3 CHM 208 EXPERIMENTAL CHEMISTRY II C 00 15 00 1 BCH 201 INTRODUCTION TO BIOCHEMISTRY I INTRODUCTION TO NUMERICAL ANALYSIS R 20 00 10 2 C 30 00 10 3 ELECTRICAL CIRCUITS ELECTRONIC I INTRODUCTORY GENETIC EVOLUTION C 30 00 10 3 R 30 00 10 3 GST 208 MUSIC APPRECIATION IV R 10 15 00 0 BTH 202 INTRODUCTION TO BIOTECHNOLOGY TOTAL UNITS R 30 00 10 3 MTH 242 PHY 202 BIO 208 21 COMPULSORY: 12 REQUIRED: 9 52 Industrial Chemistry SECOND YEAR (200 -LEVEL COURSES) RAIN COURSE COURSE TITLE STATUS CODE L P T UNITS RAIN SEMESTER CHM 202 INTRODUCTORY ANALYTICAL CHEMISTRY C 3 0 00 10 3 CHM 206 INDUSTRIAL CHEMISTRY C 3 0 00 10 3 CHM 208 EXPERIMENTAL CHEMISTRY II C 0 0 15 00 1 BCH 201 R 2 0 3 0 00 10 2 MTH 242 INTRODUCTION TO BIOCHEMISTRY I INTRODUCTION TO NUMERICAL ANALYSIS 00 10 3 PHY 202 ELECTRIC CIRCUITS AND ELECTRONIC I C 3 0 00 10 3 BIO 208 INTRODUCTORY GENETIC AND EVOLUTION R 3 0 00 10 3 GST 208 MUSIC APPRECIATION IV R 1 0 15 00 0 BTH 202 INTRODUCTION TO BIOTECHNOLOGY R 3 0 00 10 3 C TOTAL UNITS 19 COMPULSORY: 12 REQUIRED: 9 53 Industrial Chemistry THIRD YEAR (300-LEVEL COURSES) HARMATTAN COURSE COURSE TITLE STATUS L CODE HARMATTAN SEMESTER APPLIED CHEMICAL THERMODYNAMICS AND C 3 ICH 321 KINETICS 0 ICH 323 HEAT TRANSFER R 2 0 ICH 327 SPECIAL TOPICS IN C 3 INORGANIC CHEMISTRY 0 ICH 335 ELEMENT OF FOOD R 2 SCIENCE AND 0 TECHNOLOGY CHM 337 SPECTROSCOPY C 3 0 ICH 341 METALLURGY AND R 3 METAL FABRICATION 0 ICH 345 EXPERIMENTAL R 0 ORGANIC CHEMISTRY 0 ICH 347 INTRODUCTION TO C 2 CATALYSIS 0 TOTAL UNITS COMPULSORY: 12 REQUIRED: 8 THIRD YEAR (300-LEVEL COURSES) RAIN COURSE COURSE TITLE STATUS CODE CHM 306 COORDINATION C CHEMISTRY ICH 322 UNIT OPERATION R ICH 336 ICH 352 ICH 348 ICH 342 ENVIRONMENTAL CHEM/AIR POLLUTION PHYSICAL ORGANIC CHEMISTRY MANAGEMENT AND CHEMICAL INDUSTRY ELECTROCHEMISTRY C C C C P T UNITS 00 10 3 00 10 2 00 10 3 00 10 2 00 10 3 00 10 3 15 00 1 00 10 2 19 L P T UNITS 2 0 2 0 3 0 3 0 2 0 1 0 0 10 2 0 10 2 0 10 3 0 10 3 0 00 2 1 5 00 2 54 Industrial Chemistry INDUSTRIAL TRAINING C 0 0 ICH 325/326 1 2 0 00 TOTAL UNITS 6 20 COMPULSORY: 18 NB: Students will go for ICH 325/326 for six months during the long vacation. REQUIRED: 2 FOURTH YEAR (400-LEVEL COURSES) HARMATTAN COURSE COURSE TITLE STATUS L P CODE HARMATTAN SEMESTER ICH 425 ICH 427 CHM 429 QUALITY CONTROL SEMINAR NON-AQUEOUS SOLVENTS ICH 431 BASIC CONCEPTS IN DRUG DESIGN CHM 433 ORGANIC SYNTHESIS CHM 435 REACTION KINETICS CHM 439 MEDICINAL PLANT CHEMISTRY ICH 443 SURFACE CHEMISTRY ICH 445 SUGAR TECHNOLOGY ICH 447 PETROLEUM CHEMISTRY CHM 449 INSTRUMENTAL ANALYTICAL METHODS TOTAL UNITS COMPULSORY: 16 REQUIRED: 7 T UNITS C 20 00 10 2 C R 10 10 00 00 00 00 1 1 R 20 00 10 2 C C R 30 30 20 00 00 00 10 10 10 3 3 2 C R C 20 20 20 00 00 00 10 10 10 2 2 2 C 30 00 10 3 23 55 Industrial Chemistry FOURTH YEAR (400-LEVEL COURSES) RAIN COURSE CODE COURSE TITLE CHM 420 ORGANOMETALLIC CHEMISTRY ICH 424 L P T UNITS R 10 0 10 20 INDUSTRIAL METHODOLOGY C 20 00 10 30 BREWING SCIENCE TECHNOLOGY C 10 00 10 20 ICH 426 DETERGENT AND COSMETIC CHEMISTRY R 10 00 10 20 ICH 428 FERTILIZERS AND AGROCHEMICAL R 10 00 10 20 ICH 436 ENVIRONMENTAL CHEMISTRY - AIR PURIFICATION C 10 00 10 20 TEXTILE AND DYESTUFF CHEMISTRY R 10 00 10 20 POLYMER TECHNOLOGY C 10 00 10 20 SPECIAL PROJECT C 00 60 00 60 ICH 440 ICH 444 STATUS ICH 446 ICH 499 TOTAL UNITS 23 COMPULSORY: 17 REQUIRED: 8 56 Industrial Chemistry COURSE CONTENT Note: C: COMPULSORY, R: REQUIRED, E: ELECTIVE CHM 101 - GENERAL CHEMISTRY I (PHYSICAL & INORGANIC) Chemical reactions, equations and stoichiometry. Atoms, molecules and structures. Periodic classification of elements in the periodic table. Electronic theory of atoms. Radioactivity. Chemical Bonding: Ionic and covalent bonds. Solids and their structures. Dipole-dipole interactions and its effect on physical properties. Redox reactions, oxidation number and nomenclature. Chemical equilibrium. Elementary electrochemistry. Electrolysis and Faraday's laws of electrolysis. Introduction to gas kinetics. Properties of gases. Basic chemical kinetics, thermochemistry and chemical thermodynamics. Principles of acid and base reactions. pH, solubility product. 30h (T), 45h(P), PR: Credit at SSCE, GCE O' Level Chemistry or equivalent. CHM 102 – GENERAL CHEMISTRY II (ORGANIC) 3 Credits Organic formulae and structures. Functional group classes of carbon compounds. Homology and isomerism. Concept of hybridization. Introduction to the chemistry of alkanes and petroleum, alkenes including ozonolysis, alkynes, benzene, haloalkanes, alkanols including phenols, ethers amines, aldehydes, carboxylic acids and their derivatives. Structure of simple sugars, starch and cellulose, peptides and proteins. Note: Mechanism of reactions discussed in all cases and uses of compounds. 30h(T), 45h(P), PR: Credit at SSCE, GCE O' Level Chemistry or equivalent CHM 108 – GENERAL CHEMISTRY LABORATORY Same course content as CHM 101 and CHM 102 but half the amount of work required. 45h(P), CR: CHM 101 and CHM 102. 57 Industrial Chemistry CHM 201- PHYSICAL CHEMISTRY Ideal and real gases. Boyles and Charles laws. Equation of state for real gases. Thermodynamic concepts and parameters. Thermodynamic process e.g. isobar, isotherm, adiabatic, reversible and irreversible processes. State functions and differentials. First law of thermodynamics, thermochemistry, lattice enthalpy. Second law of thermodynamics. Chemical equilibrium, mixture and solutions. colligative properties. Electrochemistry. Chemical kinetics – rate of reactions. 30h (T), 45h (P), PR: CHM 101. CHM 202 - INTRODUCTORY ANALYTICAL CHEMISTRY Introduction to analytical chemistry. Types of sampling methods. Theory of sampling methods. Titrimetric analysis: acid/base, redox, complexometric and precipitation, Gravimetric analysis. Colorimetry. Introductory spectroscopy. 30h(T), 45h(P): CHM 203 - ORGANIC CHEMISTRY Aromatic chemistry with mechanism of reaction (aromaticity). Functional group chemistry in aromatic and aliphatic compounds. Simple alicyclic compounds and their synthesis. Conformational and isomerism. Stereochemistry and stereoisomerism. Modes of bond formation and fission in organic compound. Electronic and steric effects. Substitution, addition and free radical reaction. Energetic, kinetics and the investigation of reaction mechanisms. Nucleophilic and electrophilic substitution reactions. Functional group analysis. 30h(T), 45h(P), PR: CHM 102 CHM 206 - INDUSTRIAL CHEMISTRY Survey of chemical and related industries and sources of raw material for the chemical industries in Nigeria: Inventory, state and 58 Industrial Chemistry convertability of Nigeria's natural resources. Environmental effects of Nigeria's chemical industries. The economic importance and general characteristics of the chemical industry. Introduction to chemical technology processes, mineral processes and chemical plant operations. Ore processing for selected metals. Industrial gases, purification and uses. Importance of research and development, capital, labour requirements, technical and scale services. Basic requirements for setting up a chemical factory. 30h (T), 45h (P) CHM 207 – EXPERIMENTAL CHEMISTRY I Same course content as CHM 201, 202, & 211 but half the amount of work required. 45h(P), CR: CHM 201, 202 & 211 CHM 208 - EXPERIMENTAL CHEMISTRY II Same course content as CHM 203 & 206 but half the amount of work required. 45h(P), CR: CHM 203 & 206 CHM 211 - INORGANIC CHEMISTRY Comparative group relations of the elements in the Periodic Table. Chemistry of group IlIA (boron group), VA (nitrogen group), noble gases and 1st row of transition metals. Polymorphism. Theory and principles of qualitative and quantitative inorganic analysis. Separation of elements into analytical groups by the solubility of their compounds in quantitative inorganic analysis. Concepts of hard and soft acids and bases. Oxidation and reduction reactions. 30h(T), 45h(P), PR: CHM 101 CHM 306: COORDINATION CHEMISTRY: 2 Credits Definition, history development, types of Ligands, coordination number, and structural aspects. Nomenclature, isomerism, preparation, thermodynamic stability.Structure and bonding ,structural investigation 59 Industrial Chemistry by physical methods.Magnetometry and spectroscopic techniques. Reaction of metal complexes .Application of coordination compounds. 30h(T), PR.CHM 211 ICH 321 - APPLIED CHEMICAL THERMODYNAMICS AND KINETICS 3 Credits Principles of thermodynamics, phase equilibria chemical kinetics of complex reactions. Theory of reaction rates. Reactions in solution and catalysis. 45h(T), CHM 201. ICH 322 - UNIT OPERATIONS 3 Credits Introductory fluid mechanics and fluid handling processes. Physiochemical industrial processes: grinding, size-reduction, filtration, distillation and solvent extraction processes. 30h(T), PR:CHM 201 ICH 323 - HEAT TRANSFER 2 Credits Introductory heat transfer principles and applications in chemical industries, forced and natural convections, steady-state conduction, radiation, boiling and condensation, boilers and heat exchangers. 30h(T), PR: CHM 201 ICH 325 INDUSTRIAL TRAINING m6 Credits Students will do their final year industrial training attachment for 1012 weeks during long vacation. 270h(P) ICH 327 - TOPICS IN INORGANIC CHEMISTRY Chemistry of metals, occurrence, extraction, and general properties. Structure of metals, ionic and covalent compounds. Eutectic diagrams. Chemistry of inorganic compounds and complexes of industrial interest. 30h(T), 45h(P), PR: CHM 211 60 Industrial Chemistry ICH 335 – ELEMENTS OF FOOD SCIENCE AND TECHNOLOGY 2 Credits Analysis of food samples for trace elements, vitamins, proteins contents, etc. methods of food preservation. Studies of food poisoning and problems of nutrient deficiencies. 30h(T) ICH 336 - ENVIRONMENTAL CHEMISTRY - AIR POLLUTION 3 Credits The atmosphere structure, properties and photo-chemistry. Airpollutants, natural and man-made. Chemical interactions between the atmosphere and the hydrosphere. Effect on living things. Smogs. Emissions, emissions control analysis. 45h(T) CHM 337 – SPECTROSCOPY 3 Credits Existence of characteristic energy levels; Bohr-Einstein frequency relationship selection rules; characteristics spectra ;factors determining relative intensities; Boltzmann distribution effects of temperatures; characteristics line width ; absorption and emission spectra and their determination;absolute intensity ;Beer-Lambert Law. Survey: Spectral transaction and their uses. Vibrational Spectroscopy: Harmonic oscillators and the effects of anharmonicity; normal modes of vibrational criteria for infra-red activity ;Raman activity ;group frequencies. 61 Industrial Chemistry Ultra-violet and Visible Spectroscopy: Types of transitions; consideration of intensities d/d transitions; aromatic systems; Woodward rules. Resonance Spectroscopy: Resonance condition, chemical shifts; intensities; coupling constants. Mass Spectroscopy: Generation of positive ions; characteristic fragmentations patterns; isotope effects. Practical Work: Examples are as follows: determination of meaningful spectra (sample preparation and instrumental parameters); determination of simple n.m.r and mass spectra; investigation of carbonyl stretching frequencies ; study of the effects of conjugation in the ultra-violet region ; Lambert’s Law as applied to mixture; determination of pKa of methyl red; the investigation of an unknown compound using the integrated approach.30h(T), 45h(P)PR: CHM 101,CHM102. ICH 341- METALLURGY AND METAL FABRICATION 3 Credits Production of metals and alloys. Metal cutting, hot forming and cold forming metals. Casting and sintering . Oxidation and corrosion of metals. 30h(T), 45h(P) CHM 342- ELECTROCHEMISTRY 2 Credits Chemical Equilibria: Ionic equilibria, Conductance, theory and measurement, interpretation of data for strong and weak electrolytes, Conductance and transport processes. Thermodynamics and galvanic cells. 62 Industrial Chemistry Standard electrode potentials. Practical electrode. Molecular forces in solids and liquids: Dipole moments. Interaction potential and forces. Reversible galvanic cells, measurement of e.m.f. Electrode and the electrochemical series. Standard state and the Nernst equation. Application of e.m.f. measurements (excluding thermodynamic relationships).Potentiometric titration including measurement of pH. Redox reactions. The electrical double layer and its application. 30h(T),PR: CHM 201 ICH 344 - INDUSTRIAL CHEMISTRY LABORATORY 2 Credits An integrated laboratory course covering all the 300 level optional ICH Courses. 90h(P) ICH 345 - EXPERIMENTAL ORGANIC CHEMISTRY 1 Credit Same course content as CHM 308 but half the amount of work required. 45h(P), CR:CHM 328; PR: CHM 208 ICH 346 - EXPERIMENTAL PHYSICAL CHEMISTR Y 1 Credit Same course content as CHM 305 but half the amount of work required. 45h(P); CR:ICH 321; PR: CHM 207 ICH 347 INTRODUCTION TO CATALYSIS 2 Credits Principles of catalytic processes. Factors to be considered in choosing catalysts for industrial reactions. Types of catalysts: Homogeneous and heterogeneous with examples. Forms and preparation of heterogeneous catalysts. Homogeneous and heterogeneous catalysis with examples. Mechanism and steps involved in catalysis(Thermodynamics and 63 Industrial Chemistry kinetics of catalysis).Industrial applications of catalysis. Chemistry and structures of catalysts. 30h(T) ,PR:CHM 211,CHM 201 CHM 352- PHYSICAL ORGANIC CHEMISTRY 3 Credits Stepwise and concerted reaction mechanism. Kinetics studies, nonkinetics studies, Nucleophilic displacement reactions. The mechanism of SN1, SN2 processes. The effects of structure, environment, nature of the nucleophile ,salvation factors ,added salts etc on the course and rate of reactions, stereo-chemical concepts. Ester hydrolysis – unimolecular and bimolecular processes. Linear free energy relationships. The Hammet equation; determination of constituent and reaction constants; significance and use of the signs and symbols to +6m/P+0+6+m/o application to evaluation of mechanistic ways. Review of reaction intermediates viz.benzene,carbenes,nitrenes,carbonium ions. Orbital symmetry in Pericyclic reactions. Electrocyclic reactions. Sigmatropic rearrangements. Woodward Hoffman Rule. Huckel Rule and aromaticity. 30h(T), 45(P)PR:CHM203 CHM 420 – ORGANOMETALLIC CHEMISTRY: 2 Credits Introduction to Organometallic compounds of the transition elements. Classification of ligand electron rule, bonding, preparation of organic transition metal compounds. Reaction and structures of organometallic compounds of transition elements. The organic chemistry of Ferrocene and related compounds. The role of organometallic compounds in some catalytic reaction. 30h(T), 45h(P) PR:CHM 302 and 306. 64 Industrial Chemistry ICH 424 INDUSTRIAL METHODOLOGY 3 Credits Measurement and evaluation of work. Time, motion and method of studies. Reliability theory and quality control. Production and inventory control. Resources allocation. CPA principles of economics and accounting. Ergonomic design of machine systems. 45h(T) ICH425 QUALITY CONTROL 2 Credits Chemical and technical quality of textiles, plastics, dye, detergents, foods and cosmetics. 15h(T), 45h(P), PR:CHM 328 & 335 ICH 426 - BREWING SCIEENCE AND TECHNOLOGY 2 Credits History of brewing, fermentation, Alcohol Politics (social effects and legal aspects), Brewing of beer, wine, hot alcoholic beverages and quality control in brewing. Wine types, wine making, wine analysis and wine instability. 30h(T) ICH 427 – SEMINAR 1 Credit Literature search, presentation of seminars on comprehensive literature reviews of selected topics of research interest especially related to the research project. 45h(P)ICH 428 - DETERGENT AND COSMETICS CHEMISTRY 2 Credits Survey of classes of detergents. Surfactants: preparations, properties and industrial applications. Definition and classification of cosmetics. Preparations, properties and application of frequently used cosmetic products: e.g. face powder, creams., lotions, hair care products. Lipsticks. Legal consideration and regulatory governing cosmetics. 30h(T) 65 Industrial Chemistry CHM 429: NON-AQUEOUS SOLVENTS: (L 15: PO: TO) Pre-requisite-CHM 211 Classification and General Characteristics, solute-solvent interaction. Protonic solvents. Oxyhalide solvents. Liquid halides.Dinitrogen tetroxide, sulphur dioxide. Leveling effects, non-aqueous titrations. ICH 431 - BASIC CONCEPTS IN DRUG DESIGN 2 Credits Classifications of the various types of drugs. The chemistry and properties of each class of drugs. The metabolism of drugs in the body. 30h(T), CR: CHM 204 CHM 433 – ORGANIC SYSTHESIS Reaction methods. Catalytic hydrogenation. Reduction reaction with boron and aluminum hydrides and their analogues and derivatives. Metal reductions. Selective reduction in polyfunctionalcompounds. Oxidation methods.Epoxidation ,hydration and hydroxylation of alkanes,oxidative cleavage of glycol.Peroxyacids and coupling and relevance to biosynthesis survey of synthetic applications of Organometallic organoboranes.Hydroboration oxidation to ketones.Carboxylation reactions and protonolysis phosphorus halides and their applications .Enamines: synthesis and applications. Formation of polycyclic compounds.Aldol type reactivity and reaction of minimum salts with nucleophile.Synthesis of complex molecules .Pericyclic reactions. Methodology for the construction synthesis routes. 45h(T),PR: CHM 203. CHM 435- REACTION KINETICS 3 Credits Second and third orders rate equations- review. Rate constant and equilibrium constants- derivation state theory ,reaction coordinates, unimolecular reactions theory , bimolecular reaction mechanism; chain reaction mechanisms. Photochemical and electrochemical reactions; 66 Industrial Chemistry complex reaction systems; concurrent, consecutive and chain reactions. Catalysis and heterogeneous reactions.45h(T),PR:CHM 201, ICH 247. ICH 436 - FERTILIZERS AND AGROCHEMICAL 2 Credits Advanced chemistry of fertilizers, insecticides, and growth regulators. Recent trends in the synthesis and structural elucidation of commercial fertilizers and pesticides. 30h(T) PR:CHM 204. ICH 438 – MANAGEMENT AND CHEMICAL INDUSTRY 2 credits An introduction to the anatomy of management; Industrial Relation; PUBLIC Relations; Industrial Psychology; Organizational Design: Management of Personnel; An introduction to the production functions; planning for productivity. Corporate policy and organizational constraints on management process. 30h (T). CHM 439 - MEDICINAL PLANT CHEMISTRY 2 Credits Chemistry, synthesis, structural-activity relationships, synthetic analogues and medicinal use of alkaloids, glycoside lipids and volatile oils. 30h(T). ICH 440 -ENVIRONMENTAL CHEMISTRY: AIR PURIFICATION 3 Credits Spreading of air pollution in the atmosphere. Alternative to the Ottocycle engine. Purification of waste gases, oxides of sulphur, nitrogen and other gaseous pollutants. Methods of purification of waste gases. Effectiveness of purification installations. 30h(T), PR: ICH 228 67 Industrial Chemistry ICH 443 - SURFACE CHEMISTRY 2 Credits Thermodynamics and electrical surface phenomena. Adsorption at the gas-solid, liquid-gas, and solid-liquid interfaces. The Gibbs adsorption isotherm, Kelvin equation, Langmuir isotherm. Wetting and flotation. The colloidal state. 45h(T); PR:ICH 321 ICH 444 - TEXTILE AND DYESTUFF CHEMISTRY 2 Credits Basic chemistry of natural and synthetic fibres, chemistry of dyes and bleaching. Synthesis of dyes and intermediates. Apysico-chemical methods of dye analysis. Application of dyes in food and drug. ICH 445 - SUGAR TECHNOLOGY 2 Credits Introduction. Crushing, shredding, inhibition, extraction, diffusion, clarification, evaporation, crystallization and drying. 30h(T) ICH 446 - POLYMER TECHNOLOGY 2 Credits Large scale industrial polymerisation processes mechanical properties of polymers. Introduction of polymer rheology, polymer processing; injection extrusion, calendaring, compression and transfer moulding of thermoplastics. Important. Methods of processing thermosets. Polymer morphology. ICH 447 - PETROLEUM CHEMISTRY 2 Credits Composition, classification and properties of petroleum and petroleum gases. Processing of petroleum and hydrocarbons. Preparation and chemical transformation of primary petrochemicals. 30h(T) 68 Industrial Chemistry CHM 449 - INSTRUMENTAL ANALYTICAL METHODS 3 Credits Radiochemical methods; fluorescence and phosphorescence; Electroanalytical methods; voltametry; spectroscopy; Theory and practices of gas chromatography; Thermal methods of analysis; High performance liquid chromatography; Automated analytical methods; Enzymatic methods.30h(T),45h(P),PR:CHM 202, ICH 322, 1CH 323. ICH 499 - SPECIAL PROJECT 6 Credits Experimental investigation into an applied chemistry problem carried out independently by the student under the guidance of an academic member of staff. 225h(P). PR: Four hundred level registration. 69 Industrial Chemistry