Gradient-Index Research Group Metrology Instruments Instrument Wavelength (μm) 0.4 – 1.1 Index Range Any Absolute /Relative Relative Material Type GRIN Schmidt Immersion 0.4 – 1.1 < 1.7 Absolute GRIN MWIR MachZehnder Interferometer 3.0 – 5.0 Any Relative GRIN *LWIR MachZehnder Interferometer 8.0 – 12.0 Any Relative GRIN Abbe and Pulfrich Refractometers 0.4 – 1.7 < 1.7 Absolute Homogeneous Metricon Refractometer 0.4 – 1.7 < 2.0 Absolute Homogeneous Visible Sagnac Interferometer 0.4 – 1.1 Any Absolute Homogeneous Instrument Wavelength (μm) 3.0 – 5.0 Index Range Any Absolute or Relative Absolute Material Type Visible MachZehnder Interferometer MWIR Sagnac Interferometer Homogeneous Comments Sample Geometry Gives two-dimensional relative index. Accuracy limited by sample preparation and mechanical properties. Same as Mach-Zehnder but uses index fluid that matches the sample at some point. Limited by available fluids. Gives two-dimensional relative index. Accuracy limited by sample preparation and mechanical properties. Cannot use index fluid. Gives two-dimensional relative index. Accuracy limited by sample preparation and mechanical properties. Cannot use index fluid. Requires index fluid and wellcharacterized reference prism. Sample must have lower index than prism and fluid. Critical angle measurement with reference prism. Thin (~1mm), plane, parallel slice. Index is constant through sample thickness (exposed gradient). Thin (~1mm), plane, parallel slice. Index is constant through sample thickness (exposed gradient). Thin (~2mm), plane, parallel slice. Index is constant through sample thickness (exposed gradient). Figure error < 1λ. Wedge error < 5μm over region of interest. Thin (~3mm), plane, parallel slice. Index is constant through sample thickness (exposed gradient). Figure error < 1λ. Wedge error < 5μm over region of interest. Figure error < 3λ Accuracy limited by sample thickness measurement and sample preparation. Comments Small sample blank (5x5x5 mm3, up to (20x10xN mm3). One polished surface and one edge that is at least ground Small sample blank (5x5x5 mm3, up to (20x10xN mm3). One polished surface required Plane parallel window. Diameter > 15mm Thickness > 5mm Sample Geometry Accuracy limited by sample thickness measurement and sample preparation. Plane parallel window. Diameter > 15mm Thickness > 5mm Wedge < 5 arcmin Thicker samples reduce measurement uncertainty *Instrument under construction or upgrade, expected completion by spring of 2015 www.optics.rochester.edu/workgroups/moore/downloads Sample Prep Requirements Figure error < 1λ. Wedge error < 5μm over region of interest. Figure error < 1λ. Wedge error < 5μm over region of interest. Figure error < 3λ Wedge < 5 arcmin Thicker samples reduce measurement uncertainty Sample Prep Requirements 7/14/2014 Gradient-Index Research Group Metrology Instruments *LWIR Sagnac Interferometer 8.0 – 12.0 Any Absolute Homogeneous *Low Coherence Distance Measuring Interferometer 0.650 N/A Absolute Thickness GRIN or Homogeneous 0.4 – 0.7 Any Relative GRIN *Thermal Interferometer 0.6328 Any dn/dT and CTE GRIN or Homogeneous *Mini MachZehnder Interferometer 0.6328 Any Relative GRIN Beam Deflection Accuracy limited by sample thickness measurement and sample preparation. Measures thickness of plane parallel samples. Expected accuracy around 100nm. Plane parallel window. Diameter > 15mm Thickness > 5mm Nominally plane parallel sample with polished surfaces Wedge < 5 arcmin Thicker samples reduce measurement uncertainty TBD Calculate relative GRIN profile by measuring laser deflection through GRIN material. Gives two-dimensional measurement of index and thickness change as a function of temperature. Limited by phase measurement error and environmental stability and monitoring. Microscope configuration for small samples or large fringe densities. One-dimensional gradient. Plane parallel window or cylinder geometry Thin (~1mm), plane, parallel slice. Index is constant through sample thickness (exposed gradient). Thin (~1mm), plane, parallel slice. Index is constant through sample thickness (exposed gradient). Advantages Figure error < 1λ. Wedge error < 3μm over region of interest. Reflective coating on one half of one surface Figure error < 1λ. Wedge error < 3μm over region of interest. Instrument Best Case Error Bar Mach-Zehnder Interferometer 2x10-5 - Very versatile and robust measurement method - Schmidt immersion method provides absolute index - Sample prep problems can limit measurement accuracy - Sample prep is typically destructive Abbe and Pulfrich Refractometers Sagnac Interferometer 1x10-5 - Robust measurement method 1x10-4 Limited by reference prism and available index fluids Surface measurement only Limited by sample thickness measurement Sensitive to scatter and surface shape Beam Deflection 1x10-3 Thermal Interferometer CTE and dn/dT to 2 or 3 digits - - Limited accuracy Requires constant index in propagation direction Double pass (reduces effective fringe resolution) Requires environmentally controlled chamber Average index measurement Used for any index or wavelength range Uses plane parallel sample rather than prism Nondestructive test for certain geometries Can be implemented in-process Gives CTE and dn/dT as a function of (x,y) Useful for GRIN and homogeneous materials Disadvantages *Instrument under construction or upgrade, expected completion by spring of 2015 www.optics.rochester.edu/workgroups/moore/downloads 7/14/2014 Gradient-Index Research Group Metrology Instruments *Instrument under construction or upgrade, expected completion by spring of 2015 www.optics.rochester.edu/workgroups/moore/downloads 7/14/2014