m Internal Charges Policy Schedule O: Analytical Laboratory Approving authority Executive Group Approval date 3 December 2014 Advisor Associate Director, Corporate/Divisional Resource Management | Planning and Financial Services | S.Carroll@griffith.edu.au | (07) 373 55467 Next scheduled review 2015 Document URL http://policies.griffith.edu.au/pdf/Internal Charges Policy Schedule O.pdf TRIM document 2014/0003572 Description This schedule provides internal charge costs pertaining to the Analytical Laboratory located on Nathan campus. This document is a supplement to the Internal Charges Policy and subsequent Approved Internal Charges List. Related documents Internal Charges Policy Approved Internal Charges List Finance Management Practice Manual Information Services - Service Catalogue DISCRETE CHEMICAL ANALYSER (DCA) $25 for setup plus: Analysis Charge (per sample): NH4 $1.50 NOx $1.50 PO4 $1.50 Chloride $1.50 Total Nitrogen (DCA) $1.50 Persulfate digestion $1.50 Persulfate digestion + DCA $3.00 Total Phosphorus (DCA) $1.50 Persulfate digestion $1.50 Persulfate digestion + DCA $3.00 Total Nitrogen & Phosphorus (DCA) $3.00 Persulfate digestion $1.50 Persulfate digestion + DCA $4.50 Standards preparation 1 Internal Charges Policy 2014 - Schedule O: Analytical Laboratory included in setup GC-ECD-MS Description: Charge: $25 for setup plus $2.35 for 2 mins and 10c for each additional minute examples: $2.95 ( 8 min) $3.65 (15 min) Gas Chromatograph fitted with an in-line electron capture detector and mass spectrometer GC-ECD-FID Description: Charge: Gas Chromatograph fitted with an in-line electron capture and flame ionisation detectors $25 for setup plus $1.60 for 2mins and 10c for each additional minute examples: $2.20 ( 8 min) $2.90 (15 min) GC-TCD-FID Description: Charge: $25 for setup plus: $1.60 for 2 mins and 10c for each additional minute examples: $2.20 ( 8 min) $2.90 (15 min) Gas Chromatograph fitted with in-line thermal conductivity and flame ionisation detectors FDRY Description: Small and Large Freezer Dryers Charge: $10.00 per day ASE Description: Accelerated Solvent Extraction Client pays for solvents Charge: $10.00 per sample OR $15.00 per hour (including set-up) Description: Charge: $5.00 per run (A run can include up to 10 standard samples OR up to 30 samples if inserts used) MWD Microwave Digestor AAS Description: Atomic Absorption Spectrometer Charge: $5.00 for each element for setup plus: $1.50 each for first 100 $1.00 each for second 100 $0.50 each for any additional HPLC-PDA Description: High Pressure Liquid Chromatography Equipped with Photo Diode Array Detectors Client pays for own solvents / column Charge: $25.00 for setup plus: $2.00 per injection AGILENT UV-VIS Description: UV-Vis Spectrophotometer purchased from Agilent Charge: $0.50 per sample OR $5.00 per hour SHIMADZU UV-VIS Description: UV-Vis Spectrophotometer purchased from Shimadzu 2 Internal Charges Policy 2014 - Schedule O: Analytical Laboratory Charge: $0.50 per sample OR $7.50 per hour School of Natural Sciences Schedule of Fees and Charges for Common and General Use Instrumentation. Submitted Samples Spectrometry GU & Ass. Academics Low Resolution Mass ESI - LCMS Direct Injection 4000da limit. Single mode.(II) $25.00/sample APCI - LCMS Direct Injection 4000da limit. Single mode. (II) $25.00/sample ESI/APCI - multimode Direct Injection $35.00/sample 4000da limit. Single mode. (II) Proteomic Mass Spectroscopy ESI - LCMS Raw Data $50.00/sample +ve or -ve mode, raw unprocessed data. (V) (VIII) ESI - LCMS Deconvolution. $150.00/sample +ve or -ve mode, processed MAXENT data. (V) (VIII) Chromatography GU & Ass. Academics GC-FID Method supplied $30/hr min $15(total run time for batch) Gas Chromatography. Results include peak table. (V) GC-MS Method supplied $30/hr min $15(total run time for batch) Gas Chromatography. EI MS mass range 1200da. (V) HPLC Method supplied $30/hr min $15(total run time for batch) Liquid Chromatography, single wavelength. (V) UPC^2 Method supplied Convergence Chromatography (CO2) $50/hr min $15(total run time for batch) HPLC-MS Method supplied $50/hr min $15(total run time for batch) Liquid Chromatography. ESI or APCI, 4000da limit single mode. (V) UPLC-MS/MS Method supplied $150/hr min $75(total run time for batch) Liquid Chromatography. ESI, 3000da MS/MS-MRM Method Development 3 Ω $50/hr + total run time for all meth dev runs Internal Charges Policy 2014 - Schedule O: Analytical Laboratory Optical Spectroscopy ICP-OES negotiable FTIR $20.00 Fourier transform inferred. UV/Vis $20.00 LC-MS (+ $5 session fee) $30/hr UPLC-MS/MS GC-FID (+ $5 session fee) $100/hr (+ $5 session fee) $20.00/hr GC-MS (+ $5 session fee) $20.00/hr GC-MS/MS (+ $5 session fee) $30/hr (+ $5 session fee) $50/hr (+ $5 session fee) $20.00/hr GC-MS/MS HPLC SPME Optical Spectroscopy RU RU FTIR UV/Vis User-operator Charges (IX) GU & Ass. Academics Low Res Mass Spectrometry Instrument Training Optical Instrumentation – FTIR, UV/VIS BPS users will attract no charge for training. ENV, Eskitis, Glycomics and other research institutions $50/hr General Equipment – GC, GC-MS, HPLC HPLC-MS, AA GU and associated users will be charged at a nominal rate of $50/hr per person. II Direct injections and infusions are run in 80:20 MeCN:Water, use of other solvents must be specified. Use of other modes and other dopants (i.e. NH4+, Li+, Ag+, etc.) attracts an additional ‘unique’ sample charge. IV By Direct Injections or Infusion. Samples are run in 60:40 MeCN:0.1% Formic acid, use of other solvents must be specified. V VI VIII Quantitative analysis data interpretation will incur additional hourly rate charges, $200/hr (min $100). Method Development will incur additional charges as shown. EI Peak identification attracts a $2 per peak charge for 3 peaks and more. Bulk samples are eligible for a discount after discussion with operator. Per sample charges apply for lamp changes. Sample should be desalted and ready for instrument use. Please include low res MS Data. If a low res MS spectra is not submitted one will be charged. Reasonable use policy. Discuss with operator RU 4 Internal Charges Policy 2014 - Schedule O: Analytical Laboratory