Sensitivity of V-shaped atomic force microscope cantilevers based on a modified couple stress theory Haw-Long Lee and Win-Jin Chang * Department of Mechanical Engineering Kun Shan University, Tainan 71003, Taiwan * Corresponding author: e-mail: changwj@mail.ksu.edu.tw Tel: +886(6)2050883; Fax: +886(6)2050509 1 Abstract A relationship based on a modified couple stress theory is developed to investigate the flexural sensitivity of a V-shaped cantilever of an atomic force microscope (AFM) taking into account the normal interaction force between the cantilever tip and the sample surface. An approximate solution to the flexural vibration problem is obtained using the Rayleigh Ritz method. The results show that the sensitivity of the V-shaped AFM cantilever using the modified couple stress theory is smaller than that using the classical beam theory for the lower contact stiffness. However, when the contact stiffness becomes higher, the situation is reversed. Furthermore, as the ratio of cantilever thickness to internal material length scale parameter decreases, the sensitivity of the cantilever decreases. Keywords: Atomic force microscope; V-shaped cantilever; Flexural sensitivity; A modified couple stress theory. PACS: 07.79.Lh; 62.25.Jk; 68.37.Ps 2 1. Introduction The atomic force microscope (AFM) has been widely used as a tool for imaging the surface topographies of conductors and insulators on an atomic scale [1 4]. It is well known that a cantilever with a sharp tip at the free end plays an important role in AFM measurements. AFM cantilever induces a dynamic interaction force between the tip and the surface when a tip scans across a sample surface. The dynamic behavior is complicated and precise analysis is difficult, but it is related with the resolution of the surface image. Therefore, the dynamic vibration analysis is significant enough to warrant further investigation. Rectangular and V-shaped cantilevers are commercial available and are most commonly used in AFM. A Rectangular cantilever can easily reflect the optical signal in measurements. However, it is also prone to lateral twisting once the cantilever jumps into and out of contact with the specimen. On the other hand, a V-shaped cantilever can reduce lateral twisting, but its vibration response is difficult to analyze due to the complicated geometries [5]. In the last few years, there is a growing interest in studying the vibration frequency and sensitivity of AFM cantilever for both configurations using different methods, including analytical and numerical methods [6-12]. Recently, Kahrobaiyan et al. [13] studied the resonant frequency and sensitivity of AFM rectangular cantilevers using a modified couple stress theory. The theory introduces additional material parameters used to modify the classical continuum model applying to micro-scale structures [14-16]. In order to compare the vibration response of an AFM cantilever obtaining using 3 the two theories, in this article we analyze the sensitivity of a V-shaped cantilever. In addition, the sensitivities of the V-shaped and rectangular cantilevers are compared based on the modified couple stress theory. 2. Analysis A schematic diagram of a V-shaped AFM probe cantilevered at one end as shown in Fig. 1. The cantilever has a length L, thickness h, width B and legs width b with length L1 . A tip with mass M is attached at the free end of the cantilever. The tip interacts with the sample that is modeled by a spring constant k. X is the coordinate along the center of the cantilever; Y(X,t) is the vertical deflection in x-direction at time t. The linear differential equation of motion for free vibration of the V- shaped cantilever is [13,17] 2 2 2Y ( X , t ) 2 Y ( X , t) [( EI ( X ) GA ( X ) l ) ] A ( X ) 0, X 2 X 2 t 2 (1) where E and G are the elastic modulus and the shear modulus, respectively; l is the material length scale parameter which indicates the size-dependent behavior of the microcantilever based on the modified coupled stress theory; ρis the volume density; A(X) and I(X) are the cross-sectional area and the area moment of inertia of the cantilever, respectively, and they are a function of X. The corresponding boundary conditions are Y (0, t ) 0 (2) Y (0, t ) 0, X (3) 4 2Y ( L, t ) 0, X 2 (4) 2Y ( L, t ) 2Y ( L, t ) , [( EI GAl 2 ) ] kY ( L , t ) m X X 2 t 2 (5) The cantilever is assumed to be fixed at X = 0. The boundary conditions given by Eqs. (2) and (3) correspond to the conditions of zero displacement and zero slope at X = 0. In addition, Eq. (4) represents zero moment at X = L . Eq. (5) is the combination of the normal tip-sample interaction force and the inertia force of tip mass. Since a linear model is used to describe the tip-sample interaction force, the cantilever is restricted to small displacements. Eqs. (1)-(5) define the flexural vibration problem. The harmonic solution to the problem can be expressed as Y ( X , t ) W ( X )eit (6) where is the angular frequency. The dimensionless variables are defined as x EI A X W , y , ( x) , ( x) , L L EI 0 A0 m , A0 L 2 2 A0 L4 EI 0 , A0l 2 EI 0 kL3 , EI 0 12 E h / l 2 (7) where EI 0 and A0 are the bending stiffness and mass density at X = 0, respectively; , , , and denote the dimensionless contact stiffness, tip mass, natural frequency, and the effective flexural rigidity based on the modified coupled stress theory, respectively. Meanwhile, h/l is the ratio of cantilever thickness to internal material length scale parameter. Applying the above harmonic solution and dimensionless parameters, we can obtain a 5 dimensionless fourth-order ordinary differential equation and four corresponding boundary conditions. Since the parameters ( x ) and ( x) are dependent on the position x along the cantilever, a numerical method for solving the boundary value problem is proposed. In this article, the Rayleigh-Ritz method is used to calculate the natural frequencies. we set r y ( x ) ai ui ( x). (8) i 1 where ai are constants, and ui ( x) is the admissible function which requires to satisfy the geometric boundary conditions, but need not satisfy the natural boundary conditions. In this study, ui ( x) x i 1 , i 1, 2,3,...,10 is chosen, then applying the Rayleigh quotient, the following eigenvalue problem can be obtained: Ka 2 Ma (9) where a is the eigenvector of expansion coefficients and 1 d 2ui ( x) d 2u j ( x) K i j ( ( x) ( x)) dx ui (1)u j (1), 2 2 0 dx dx 1 M i j ( x)ui ( x)u j ( x)dx ui (1)u j (1), (10) (11) 0 Due to the fact that the mass matrix M does not depend explicitly on , and assuming the eigenvector to changes in stiffness is negligible. After the derivative of the eigenvalue problem, Eq. (9), is taken with respect to , then we can get the following equation K a 2 Ma Finally, the normalization condition (12) aT Ma 1 is introduced, the dimensionless flexural 6 sensitivity, S n , can then be expressed as Sn 1 T K a a 2 (13) When the contact stiffness is given, the natural frequencies and corresponding mode shapes can be calculated from Eq. (9) and then the flexural sensitivity for each vibrational mode can be obtained from Eq.(13). While the parameter ( x ) 1 and ( x) 1 , it imply the probe is a rectangle shape which flexural frequency and sensitivity are also analytical. From Eqs.(1) to (7), the dimensionless fourth-order ordinary differential equation and boundary conditions were simplified as d 4 y ( x) 2 y ( x) 0 dx 4 (1 ) (14) and y (0) 0 , dy (0) d 2 y (1) d 3 y(1) 2 0, 0 , y(1) dx dx 2 dx3 1 (15) The dimensionless flexural frequency equation and sensitivity can be analytical derived as C ( , ) 3 (1 cosh cos ) ( 4 )(cosh sin sinh cos ) 1 (16) and 2 S na 3 (sinh cos cosh sin ) (1 cosh cos ) (1 4 )(sinh cos cosh sin ) 2( (1 ) 3 ) sinh sin (18) where 4 2 1 (19) 7 3. Results and discussion In order to calculate the flexural sensitivity of a V-shaped AFM cantilever, a ten-term polynomial expansion is used. The geometric and material parameters of the V-shaped cantilever are as listed in Table 1, which are chosen to be similar to typical AFM cantilevers.[17] In addition, the tip mass used in the analysis is 2 1013 kg [18]. The ratio of cantilever thickness to internal material length scale parameter, h/l, is assumed to be 4. The dimensionless flexural sensitivities of a V-shaped AFM cantilever based on modified couple stress theory and classical beam theory are depicts in Fig. 2. Unlike the classical beam theory, the modified couple stress theory includes the effect of small-scale structure and that leads to a stiffer cantilever. Therefore, when the contact stiffness is small, it can be seen that the sensitivity of the V-shaped cantilever using the modified couple stress theory is smaller than that using the classical beam theory. When the contact stiffness becomes large, the situation is reversed. This indicates that a stiffer cantilever is better for scanning a harder surface. In addition, a softer cantilever is easier to bent and more sensitive for imaging of soft biological samples. The dimensionless flexural sensitivities of the cantilever for the V-shaped and the rectangular cross section with h / l 4 based on modified couple stress theory are illustrated in Fig. 3. When the contact stiffness is low, the sensitivity of the V-shaped cantilever is larger than that of the rectangular cross section cantilever. However, the situation is reversed when the contact stiffness becomes large. It implies that a V-shaped cantilever is suitable for scanning a softer surface, while a 8 rectangular cross section cantilever is better for scanning a stiffer surface. The effect of the ratio of microcantilever thickness to internal material length scale parameter h/l on the sensitivity is shown in Fig.4. The material length scale parameter h/l represents the size effect based on modified couple stress theory. It is noted that for the case of h / l , this implies that the classical beam theory is used in the analysis. Hence, it can be seen that the effect of h/l on the sensitivity becomes significant as the thickness of cantilever is close to the internal material length scale parameter for the lower contact stiffness. In addition, the sensitivity decreases as the value of h/l decrease. This indicates the thickness-dependent behavior of an AFM cantilever. 4. Conclusions The sensitivity of the flexural vibration modes for a V-shaped atomic force microscope cantilever has been analyzed using the Rayleigh-Ritz method. According to the analysis, the sensitivity of the V-shaped cantilever using the modified couple stress theory was smaller than that using the classical beam theory. The V-shaped cantilever was suitable for scanning a softer surface, while it was a better choice for scanning a stiffer surface using a rectangular cross-section cantilever. In addition, the sensitivity of a V-shaped cantilever decreased as the ratio of cantilever thickness to internal material length scale parameter decreased. Acknowledgment 9 The authors wish to thank the National Science Council of the Republic of China in Taiwan for providing financial support for this study under Projects NSC 99-2221-E-168-019 and NSC 99-2221-E-168-031. References [1]K. Holmberg and A. Matthews, Coatings Tribology: Properties, Techniques and Applications in Surface Engineering, Elsevier, New York, 1994. [2]B. Bhushan, Handbook of Micro/Nanotribology, 2nd edn., CRC, Boca Raton, FL, 1999. [3]Trends in Nanotechnology Research, edited by Eugene V. Dirote, Nova Science Publishers, New York, 2004. [4]Nanophysics, Nanoclusters and Nanodevices, edited by Kimberly S. Gehar, Nova Science Publishers, New York, 2006. [5]S. K. Jericho, and M. H. Jericho, Rev. Sci. Instrum. 73 (2002) 2483. [6]W.J. Chang, Nanotechnology 13 (2002) 510. [7]W. J. Chang and S. S. Chu, Phys. Lett. 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Table 1 11 The geometric and material parameters of a V-shaped AFM cantilever. Figure captions Fig. 1. Schematic diagram of a V-shaped AFM cantilever in contact with a sample. The interaction with the sample surface is modeled by a normal spring. Fig. 2. Dimensionless flexural sensitivities of a V-shaped AFM cantilever based on modified couple stress theory and classical beam theory. Fig. 3. Dimensionless flexural sensitivities of V-shaped and rectangular AFM cantilevers 12 with h / l 4 based on modified couple stress theory. 13 Fig. 1. Schematic diagram of a V-shaped AFM cantilever in contact with a sample. The interaction with the sample surface is modeled by a normal spring. 14 100 mode 1 mode 2 Dimensionless sensitivity, Sn 10-1 mode 3 mode 4 mode 5 10-2 Classical beam theory Modified couple stress theory -3 10 -4 10 -2 10 10 -1 10 0 1 10 10 Dimensionless contact stiffness, 2 3 10 Fig. 2. Dimensionless flexural sensitivities of a V-shaped AFM cantilever based on modified couple stress theory and classical beam theory. 15 100 mode 1 mode 2 Dimensionless sensitivity, Sn mode 3 -1 10 mode 4 mode 5 10-2 V- shape Rectangular -3 10 -4 10 10-2 10-1 100 101 102 Dimensionless contact stiffness, 103 Fig. 3. Dimensionless flexural sensitivities of V-shaped and rectangular AFM cantilevers with h / l 4 based on modified couple stress theory. 16 Dimensionless sensitivity of mode 1, Sn 0.7 0.6 h/l=4 h/l=8 h/l= 0.5 0.4 0.3 0.2 0.1 0 10-2 10-1 100 101 102 Dimensionless contact stiffness, 103 Fig. 4. Dimensionless flexural sensitivity of mode 1 for an AFM V-shaped cantilever at various ratios of microcantilever thickness to internal material length scale parameter h/l. 17 Dimensionless sensitivity of mode 2, Sn 0.2 0.15 0.1 h/l=4 h/l=8 h/l= 0.05 0 10-2 10-1 100 101 102 Dimensionless contact stiffness, Fig 5 18 103 Dimensionless sensitivity of mode 3, Sn 0.1 0.08 0.06 h/l=4 h/l=8 h/l= 0.04 0.02 0 10-2 10-1 100 101 102 Dimensionless contact stiffness, Fig 6 19 103 0.6 n Dimensio less s 1, f mode o y it iv it s en Sn 0.6 0.5 0.5 0.4 0.4 0.3 7 0.3 10 8 6 6 L1 / b 5 4 4 Fig 7 2 β=1 20 h/l 0.2 2, f mode o y it iv it s n nless se io s n e im D Sn 0.2 0.18 0.18 0.16 0.16 0.14 0.14 0.12 0.12 0.1 7 0.1 10 8 6 6 L1 / b 5 4 4 2 Fig 8 21 h/l f mode 3, S n o y it iv it s n e s s Dimensionles 0.1 0.1 0.09 0.09 0.08 0.08 0.07 0.07 0.06 0.06 0.05 7 0.05 10 8 6 6 L1 / b 5 4 4 2 Fig 9 22 h/l 23