Soil Testing Methods

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Soil Testing Methods
Chapter 8
Three approaches

Observations in the field

On-site measurements

Laboratory measurements
Soil Analysis Ch 8
2
Field Observations

Field observations of properties which can be observed after digging
a soil pit

Semi-quantitative assessments of properties rather than direct
measurements.
Soil Analysis Ch 8
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Field Measurements

On-site measurements using equipment inserted into soil, without
significant disturbance of the soil.

This approach applies particularly to soil water studies.
Soil Analysis Ch 8
4
Laboratory Analysis

Measurements made in the laboratory on soil samples taken from
the field.

Sub-sampling down to an analytical sample also occurs
Soil Analysis Ch 8
5
Soil Survey Reports

what kinds of soil exist in an area

described in terms of location, profile characteristics, relationship to
each other, suitability for various uses, and needs for particular
kinds of management

two major parts in a soil survey report:

the soil map

the narrative
Soil Analysis Ch 8
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SALIS

NSW soil survey database

Soil And Land Information Service

run by Dept of Natural Resources

http://www.dnr.nsw.gov.au/soils/about_salis.shtml
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Field Analysis of Soils
How can we Analyse Soil in the Field?
Field investigation

soil pits
 expose the soil profile and horizons
 allow field testing of parameters that would be destroyed by
cores
 in-situ testing devices
 semi-quantitative assessments

field data minimises sampling error

does not guarantee reliable or even consistent data

soils have very poor homogeneity
Soil Analysis Ch 8
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Soil Pit
from www.drm.gov.au
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Choosing Sites for Soil Pits
Avoid

areas close to gateways, paths and tracks

headlands of arable fields (the outer 10 m)

sites where straw or fertiliser have been stored

sites used for localised burning of crop residues or hedge trimmings

old field boundaries where a hedge or bank has been removed and
the land levelled
Soil Analysis Ch 8
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Choosing Sites for Soil Pits

soil varies spatially (from one place to another)

some properties vary in time


eg nutrient levels, moisture
others are more permanent

horizon depth, texture, stone content and ion exchange capacity
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How do we Sample Soil?
Is it just digging holes?
Sampling questions

How many samples do I take?

Do we composite lots of sub samples?

How deep do we take the samples?

Do we replicate the sampling?

What quality control do we need?

What tools do I need?

How do we transport, store and prepare the samples?
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Information we need to know

Why are we analysing the soil?
 Surveys, chemical analysis etc.

How large is the area of interest?
 Large areas require lots of sampling

Do we now the soil profile at all?
 If we don’t, how deep do we sample?

What are we analysing the soil for?
 Physical, chemical or biological parameters
Soil Analysis Ch 8
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Amount of sample

depends upon;
 Time constraints
 Topography
 Cost factors
 Reasons for sampling
 There are no specific guidelines
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Soil Sampling

undisturbed stratification:


remove a core with all horizon information retained, eg with
auger
disturbed stratification

no attempt to keep the vertical connection between horizons, eg
with a shovel
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Soil Sampling

How many samples do we take?


At least 20 single samples per 10 000m2 must be taken with an earth
boring tool (or spade) and combined to a mixed sample.
To what depth do we sample?

The usual sampling depth is up to 20 cm in arable land or 10cm in
pasture. Undisturbed soil samples are obtained with a cutting cylinder
with minimum capacity of 100cm3 .
Soil Analysis Ch 8
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How do we sample?
random
diagonal line
Soil Analysis Ch 8
cross line
test lot
19
Sampling using Augers

pressed and rotated into the soil to take samples from depth
increments of between 15 and 20cm.

samples are 'disturbed' to varying degrees

observations that can be made on the samples will be restricted

colour, texture, stones, roots and horizon depth can be recorded

soil structure cannot

special coring equipment is required to obtain 'undisturbed' samples
Soil Analysis Ch 8
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Sampling for lab testing

normal sampling depth for horticultural and tree crops is 0-15 cm

deep sampling down to 60-100 cm may be necessary to better assess
soil salinity, acidity, S, and mineral N status

sampling depth must be recorded

protocols relevant to important crop and soil tests should be
followed

usually involves making a composite from around 15 to 30 subsamples from the area in question
Soil Analysis Ch 8
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Transportation, preparation
and storage of samples
Now that you have your soil samples, what do you do with
them?
Laboratory Preparation of Samples

should be kept cool or cold between during transport

may be air-dried remote from the laboratory (max. 40C) when
moisture content is not required

breaking up any large cores or peds on a clean surface

remove rocks by hand or sieving

retain a representative portion in a sealed polyethylene bag or
'moisture container' for moisture determination

sample size reduction: coning and quartering or riffler
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Laboratory Preparation of Samples
Soil Analysis Ch 8
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Laboratory Preparation of Samples

Next spread the soil samples on drying trays (if applicable) and airdry at up to 40C.

When the soil is thoroughly air-dry, mix, roll, and/or grind.

Retain the <2mm fraction, preferably in an air-tight plastic or inert
container, for subsequent laboratory analyses.
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Laboratory Preparation of Samples

When required, determine the weight percentage (oven-dry basis) of the
residual >2-20 mm size fraction.

When fine grinding is specified, take a representative sub-sample (usually
around 30g) from the <2 mm portion.

Pass the entire sub-sample through the required mill and store in a small
air-tight container.
Soil Analysis Ch 8
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Coning & quartering
Soil Analysis Ch 8
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Riffling
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