What is F-D? Force object Deformation What properties can be studied? Hardness The force necessary to attain a given deformation Cohesiveness The strength of the internal bonds making up the body of the product Viscosity The rate of flow per unit time Springiness The rate at which a deformed material returns to its original condition after deforming force is removed Adhesiveness The work necessary to overcome the attractive forces between the surface of the food and the surface of other materials (tongue, teeth etc.) Fracturability The force at which material fractures Gumminess The energy required to disintegrate a semisolid food product to a state ready for swallowing Chewiness The energy required to masticate a solid food product to a state ready for swallowing. Examples- pasting properties of cooked rice • Back Extrusion test (BE) 5 F F orc e (kg) 4 3 2 1 0 0 40 80 120 Time (s) 160 200 How to measure visco-elastic nature of foods? • Instron texture analyzer Different Tools Shear Extrude Compression Fruits Vegetables Cooked Pasta Cubed Chicken Viscous Liquids Gels Puncture Fruits Vegetables Nuts Deformation TPA Bread Candy Cheese Gels Rolls Compression Shear Extrusion Fruits Vegetables Ground Meat Seafood Salad Viscous Liquids Gels Shear Extrusion Fruits Vegetables Viscous Liquids Gels Tension Raw Pasta Processed Meat Bend Snap Crackers Cookies Granola Bars Raw Pasta How to measure? hardness energy adhesion stickiness Single Kernel Hardness Measurement Example for various tests • Bakery • Fruit & Vegetables • Pasta, Noodles & Rice • Pet Food • Snack foods Bakery Viscosity 25mm. Ball Probes #Compress to limit and pull • Result = Positive (i.e. 'Hardness') • Result =negative (i.e. ‘Viscosity') Peak force values Hardness Viscoscity Bakery Margarine B • Magarine • Forward extrusion with 3mm extrusion disc • Containers are half filled with the margarine samples • Results = Average Force • Result = force plateau ('ease of extrusion') Margarine A Bakery • BISCUIT • 6 mm. cylinder probe Compress to limit • Results = maximum peak force ("Hardness") cylinder probe Sample Plunger Bakery/BREAD • BREAD • 36mm cylinder probe Compress to 40% strain • Results =compression force ('Firmness') at 25% compression 36mm cylinder probe Bread / Firmness Bakery/Cake • 36mm cylinder probe Compress to % strain and hold time 60 s. • Results = compression force (Firmness and Springiness) values at 25% compression: Fruit & Vegetables • Rice and Bean • Ottawa Cell Compression to limit and then weighed into 200g • Results = maximum peak force (Firmness) values, and Work of Extrusion values GRAPES • 2mm cylinder probe Compress to limit Being tested with a texture probe to determine the skin strength. Noodles • NOODLES • Spaghetti tensile grips • Dry noodles were placed in boiling water for 10 minutes and rinsed with cold water • After rinsing the samples and left to dry slightly for 15 minutes. • Results = Peak force values and Elongation Noodles Spaghetti tensile grips Rice • • • • • Hardness and Stickiness of four varieties of cooked rice 35mm cylinder probe compressed to 90% of their size the probe 200g of rice was weighed into a container Results = +Peak Force values ('Hardness') Results = - Peak Force ('Stickiness') Rice Hardness 35mm cylinder probe Stickiness Firmness of grain or cereal Pet Food • Hardness of Pellets by compression • 35mm cylinder probe Compress to limit • Results = Maximum peak force values ("Hardness") 35mm cylinder probe Wet Cat food • Ottawa Cell with Wide Blade Extrusion Plate • Compress to limit • Results = maximum peak force ("Firmness") • Results = area under the curve ("Work of Extrusion") Wide Blade Ottawa Texture Cell Fruits Vegetables Viscous Liquids Gels Test Mode Shear Extrusion Dog biscuit bending • 3 Point Bend Fixture • Compression to limit • Result = Peak Force (“Hardness”) Snack Foods • TORTILLA-TYPE SNACK FOOD • 1/4" Ball Probe and Support Ring ,Compress to limit • Results = Peak force 1/4" Ball Probe Support Ring Wafer to Fracture • 3-Point Bending Rig • Compress to limit • Results = Peak force value, the distance compressed before breaking Spreadability • • • • 45 degree cone probe Compress to limit Result = Peak force Result = Work of shear Toothpaste Firmness 'Force to Extrude' Hemispherical blade adjustable support length Compress to limit Result = Maximum extrusion force and work of extrusion' values Bending Force of lipsticks • • • • • • Lipstick Cantilever Rig Hemispherical blade Compress to Rupture Results = Maximum force Results = Distance at break Results = Modulus 10 0C 25 0C Full-Fat and Low-Fat Yoghurt by Back extrusion • YOGHURT • Back Extrusion Cell • Original yoghurt (150g) immediately after removal from storage at 5.0°C. • Compress to limit • Results = Peak force values and Area under the generated force YOGHURT Back Extrusion Cell ADHESIVE GUM • 4mm cylinder probe • Compress to limit (Distance2 mm) • Wide strips of adhesive (of approximately 4mm thickness) • Result = Positive (i.e. 'Hardness') • Result =negative (i.e. 'Stickiness') peak force values GUM ADHESIVE GUM 4mm cylinder probe Hardness Stickiness Warner-Bratzler Shear Food after different cooking times using Knife Blade • Knife Blade • Then cooked separately for the following times a) 0 mins, i.e. raw b) 1 min c) 2 mins d) 3 mins • Compress to limit • Results = Peak force Warner-Bratzler Shear a) 0 mins b) 1 min c) 2 mins d) 3 mins Warner-Bratzler Shear CHOCOLATE COATED WAFER BISCUITS • Knife Blade • Compress to limit • Results = The first peak force readings ( cutting of the first wafer layer) (“Hardness”) Graph CHOCOLATE COATED WAFER BISCUITS First Wafer layer Graph Hardness measurement of Biscuits by cutting Hardness Compression Strength of Fresh Eggs Compression to limit Results = Peak Load Kramer Shear cell • Fruits Vegetables Cooked Pasta Cubed Chicken Viscous Liquids Gels • Test Mode Shear Extrude Compression Compression Plate Bread Candy Cheese Gels Rolls Test Mode Deformation TPA Texture Profile Analysis 1, Initial step is begun at the first bite 2, Masticatory step is perceived during chewing 3, Residual step is perceived after the mastication and swallowing Textural Properties of Foods • Textural properties of food are those characteristics that are sensed by the feeling of touch, and are related to deformation, disintegration, and flow of food under the application of forces. • These properties can be measured objectively as function of force, distance, and time. • Textural properties of foods are greatly influenced by internal structure and other variables such as size, shape, moisture, and fat contents and their inter-relationships. Textural Characteristics • Hardness: the force (kg) necessary to attain a given deformation. • Cohesiveness: the strength of the internal bonds making up the body of the product (A1/A2). • Elasticity: the rate at which a deformed material goes back to its undeformed condition after the applied force is removed. • Adhesiveness: the work necessary to overcome the attractive force between the surface of the food and the other surface of contact (e.g., tongue, teeth, etc.) Textural Characteristics • Brittleness: the force with which the material fractures and was related to the primary parameters of hardness and cohesiveness. • Chewiness: the energy required to masticate a solid food product to a state ready for swallowing and was related to hardness, cohesiveness, and elasticity. • Gumminess: the force required to disintegrate a semisolid food to a state ready for swallowing and was related to hardness and cohesiveness. Example Textural Profile TPA Texture Profile Analysis • Hardness = Maximum force from First Stoke (N) • Fracturability or Brittleness = Maximum force of the first peak from First Stoke (N) TPA Hardness Fracturability Cohesiveness= A2/A1 A1 A2 TPA Springiness= L2 Springiness Index= L1/L2 L3 L1 L2 TPA TPA Application for Packaging • Tension Test • Compression Test • Peel Test • Tear Test • Friction Test • Dart Drop Impact Test VITAMIN BOTTLE SYRINGE PULL TAB CANNISTER FOOD BOX TOP CRACKER JACKS Compression Test Peeling Cup Universal Testing Machine