Revised 2024, IA Datasheet No. 7.3 MOHAWK COLLEGE OF APPLIED ARTS AND TECHNOLOGY BUILDING AND CONSTRUCTION SCIENCES DEPARTMENT Concrete Mix Design by Trial and Error INTRODUCTION: The purpose of this laboratory procedure is to proportion a concrete mix of specified water/cement ratio and slump by a trial-and-error procedure. The student will also have an opportunity to practice performing slump tests, fresh density tests and casting cylinders for testing. This lab also demonstrates the concept of repeatability in measurements by requiring two cylinders per batch be cast. PROCEDURE: 1. Each group will be assigned a water-cement ratio: Group: 1 2 3 4 5 6 7 8 9 10 w/c: 0.40 0.43 0.45 0.47 0.50 0.53 0.55 0.57 0.60 0.63 SSD Mass of Cement: SSD Mass of Water: 2. In this procedure aggregates on the dry side of SSD will be used, since it is much easier to add water to achieve the SSD state than it is to adjust the cement. Obtain about 12.500 kg of each “air dried” aggregate and, after mixing separately, take a 500.0 g + 50.0 g moisture sample, weigh to 0.1 g and dry over a flame. Calculate the moisture correction factors C c and Cf and the equivalent SSD mass of the aggregate as outlined in Test Procedures and Formulae. If this is done correctly, the % Moisture Correction for both the CA and FA should be “negative” values. If it is not, re-check the calculation and check with the instructor. 3. Prior to weighing of aggregates and mixing of concrete, moisture calculations and “As Is” batch masses must be checked by instructor. 4. Add sufficient water to both the coarse and fine aggregate to bring them to the SSD condition and mix thoroughly (based on the moisture corrections, “Water to Add for SSD”). Weigh the containers with the aggregate in them and record this weight (Initial SSD Agg. + Pail). 5. Weigh out 4.500 kg of cement and enough water to yield the water-cement ratio assigned to your group. 1 6. After moistening the mixing pan and utensils, place the cement and water in the damp mixing pan and mix thoroughly to a smooth paste. 7. From the measured stock of SSD aggregate add CA and FA to achieve a slump of 70 ± 10 mm and an acceptable ratio of CA to FA. 8. Slump testing should be started while the mix is on the wet side so that the desired slump point will not be passed. The optimum ratio of CA to FA is not sharply defined. In general, the correct amount of sand to be used is that amount which will make enough mortar to fill the spaces between the CA and leave some excess for workability. This condition can best be detected by troweling. If a smooth, thin mortar surface can be obtained with three or four trowel strokes, then proportions are approximately correct. The addition of CA will have a much smaller effect on the slump than the addition of FA. It is better to keep the mix slightly oversanded as the required slump is approached. 9. When the mix is satisfactory, weigh the amounts of the SSD CA and FA (in their containers) remaining (Final SSD Agg. + Pail). Record the slump, perform a fresh density determination, and cast two cylinders for testing during the next laboratory session. CALCULATIONS: 1. The batch proportions are calculated by subtracting the FA and CA left over from the starting masses. 2. By referring to the Test Procedures and Formulae calculate: i) the fresh density, ii) the proportions per m3 of the mix, iii) the hardened density and iv) the compressive strength. Note: For the following lab session, Datasheet 7.3 should be completed except for the Hardened Density and Compressive Strength sections. There will be a “Class Data Collection Sheet” in the lab where each group will be required to record their information. After the lab session, the “Class Data” will be posted on MyCanvas to complete the lab report. REPORT: 1. The report should include a title page, the completed Report Form, two graphs as described below and the completed data sheet 7.3. The proportions per m3 of the mix should be reported. The masses should be based on SSD aggregates and the water to cement ratio should be calculated there from and be reported. 2 2. The above values should be available during (brought to) the subsequent laboratory session, as each group must record its results on the data collection sheet provided during the lab session in which the cylinders are tested. The values entered will be evaluated as part of the mark for the report. A summary of the class results in this same format will be posted on MyCanvas to enable the performance of the required analysis in the report and the production of the following graphs: a) compressive strength on the Y–axis and water-cement ratio on the X–axis. b) hardened density on the Y–axis and water-cement ratio on the X–axis. Note: Use the Excel Template from Lab 3 posted in MyCanvas to produce the graph. Note: Refer to Pages 11 to 15, Section 1.6 of the Policy and Procedures posted on MyCanvas with regards to Laboratory Reports. Note: Sample calculations not required! REFERENCES: (Posted in MyCanvas) MTO LABORATORY TESING MANUAL: 1. 2. 3. 4. Test Method LS-400: Method of Test for Dry Rodded Density of Coarse Aggregate Test Method LS-402: Method of Test for Slump of Portland Cement Concrete Test Method LS-405: Method of Test for Density Yield and Cementing Materials Factor of Plastic Concrete Test Method LS-406: Method of Capping Moulded Concrete Cylinders with Sulphur Mortar ASTM TEST PROCEDURES NOT AVAILABLE: 1. 2. 3. 4. 5. 6. 7. 8. C31 / C31 M – 12 Standard Practice for Making and Curing Concrete Test Specimens in the Field C39 / C39 M – 12a Standard Test Method for Compressive Strength of Cylindrical Concrete Specimens C94 / C94 M – 13a Standard Specification for Ready-Mixed Concrete1 C125 – 13a Standard Terminology Relating to Concrete and Concrete Aggregates C138 / C138 M – 13 Standard Test Method for Density (Unit Weight), Yield, and Air Content (Gravimetric) of Concrete 1 C143 / C143 M –12 Standard Test Method for Slump of Hydraulic-Cement Concrete1 C172 / C172 M – 10 Standard Practice for Sampling Freshly Mixed Concrete1 C192 / C192 M – 13 Standard Practice for Making and Curing Concrete Test Specimens in the Laboratory 1 3 9. C617 / C617 M – 12 Standard Practice for Capping Cylindrical Concrete Specimens1 10. C1064 / C1064 M – 12 Standard Test Method for Temperature of Freshly Mixed Hydraulic-Cement Concrete1 11. Manual of Aggregate and Concrete Testing1 CSA TEST METHODS NOT AVAILABLE: 1. CSA A 23.2 2C Making Concrete Mixes in the Laboratory 2. CSA A23.2 1C Sampling Plastic Concrete 3. CSA A23.2 5C Slump of Concrete 4. CSA A23.2 6C Density Yield and Cement Factor of Plastic Concrete 5. CSA A23.2 9C Compressive Strength of Cylindrical Concrete Specimens 4