Materials Science Forum Vols. 821-823 (2015) pp 524-527 © (2015) Trans Tech Publications, Switzerland doi:10.4028/www.scientific.net/MSF.821-823.524 Submitted: 2014-09-12 Revised: 2014-11-14 Accepted: 2015-01-29 Online: 2015-06-30 High-Speed Dicing of SiC Wafers by Femtosecond Pulsed Laser Akira Nakajima1, a *, Yosuke Tateishi3, Hiroshi Murakami1, Hidetomo Takahashi3, Michiharu Ota3, Ryoji Kosugi2, Takeshi Mitani2, Shin-ichi Nishizawa1 and Hiromichi Ohashi1 1 2 Energy Technology Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), Central 2, 1-1-1 Umezono, Tsukuba, Ibaraki 305-8568, JAPAN Advanced Power Electronics Research Center, National Institute of Advanced Industrial Science and Technology (AIST), Central 2, 1-1-1 Umezono, Tsukuba, Ibaraki 305-8568, JAPAN 3 Aisin Seiki Co., Ltd., 2-1 Asahi, Kariya, Aichi 448-8650, JAPAN a a-nakajima@aist.go.jp Keywords: SiC wafer, dicing, femtosecond pulsed laser Abstract. A novel dicing technology that utilizes femtosecond pulsed lasers (FSPLs) is demonstrated as a high-speed and cost-effective dicing process for SiC wafers. The developed dicing process consists of cleavage groove formation on a SiC wafer surface by the FSPL, followed by chip separation by pressing a cleavage blade. The effective FSPL scan speed on the SiC surfaces was 33 mm/s. Kerf loss is negligible in the developed FSPL dicing process. In addition, the residual lattice strain in the FSPL-diced SiC chips was comparably small to that of the conventional mechanical process using diamond saws, due to the absence of the lattice heating effect in femtosecond-laser processes. Introduction SiC power devices have been making big efforts for commercialization in the last decade and used in a number of applications, such as power converters for consumer electronics and social infrastructures. However, the commonly utilized dicing process, which uses diamond saws, is low in speed and high in cost due to the mechanical hardness and brittleness of wide-bandgap SiC (~9 on the Mohs scale). To expand the possible applications of SiC devices, novel dicing technologies for SiC wafers have been desired to produce a large number of SiC chips [1-3]. Recently, optical micromachining of SiC wafers has been presented using short-pulsed lasers [4-5]. In this paper, we demonstrate a high-speed SiC dicing technology that utilizes femtosecond pulsed lasers (FSPLs) and does not exhibit kerf loss. Experimental Fig. 1 shows the schematics of the developed SiC dicing process. After device fabrication on SiC wafers, cleavage grooves were formed on Fig. 1. Schematics of developed dicing processes of (a) groove formation by the FSPL, followed by (b) chip separation by pressing a cleavage blade from the backside. All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of Trans Tech Publications, www.ttp.net. (ID: 129.93.16.3, University of Nebraska-Lincoln, Lincoln, USA-16/09/15,08:06:20) Materials Science Forum Vols. 821-823 525 the wafer surfaces by the FSPL, as illustrated in Fig. 1(a). Then the wafers were flipped over and separated into individual SiC chips by pressing a cleavage blade into the wafer backside, as shown in Fig. 1(b). In this study, we utilized four-inch, 360-µm-thick 4H-SiC wafers with 600-V-rated Schottky barrier diodes (SBDs), as illustrated in Fig. 2(a). The anode electrodes have a 1594 × 1594-µm square shape. The distance between adjacent anode electrodes was 346 µm, as shown in Fig. 2(c). The wafers were diced into SiC chips by the developed FSPL process, and also by a conventional Fig. 2. (a) Schematic cross-sectional structure of mechanical dicing technique that used 4-inch SiC wafers with 600-V-rated SBDs and 50-µm-thick diamond saws. The FSPLs (b-c) top-view optical microscopy images. have a wavelength of 1045 nm, pulse width of 800 fs, repetition rate of 100 kHz, and pulse energy of 3.6 µJ. The laser scan speed on the SiC wafer surfaces was 100 mm/s using a motorized x-y-z translation stage. The laser scanned the surface three times to form a linear groove. Therefore effective scan speed was ~33 mm/s. Results and Discussion Fig. 3 shows SEM images of SiC chips diced by the FSPL process. Although debris was observed on the as-cleaved SiC chips, as seen in Fig. 3(b), the debris can be removed by using an organic solvent, as shown in Fig. 3(c). Fig. 4 shows the relationship between dicing yield and cutting center distance ∆x from the anode electrodes. In this study, the cutting center positions were changed from the street center position (∆x = 173 µm) to -7 µm in 20-µm steps. Here, the dicing yield was obtained Fig. 3. (a) SEM images of SiC chip by FSPL dicing and enlarged images at the corners of (b) as-cleaved and (c) cleaned SiC chips after FSPL dicing. 526 Silicon Carbide and Related Materials 2014 Fig. 4. Schematic drawings of dicing dimensions as a result of (a) FSPL and (b) conventional mechanical dicing processes. (c) Relationship between the cutting center position and the dicing yield. Fig. 5. Typical reverse leakage characteristics of the SiC-SBDs measured before and after (a) FSPL and (b) conventional mechanical dicing processes at ∆x = 13 µm. Fig. 6. (a) Schematic drawing of the measurement position on diced chips and (b) variations of the frequency shift of the FTO mode along <11–20> and (c) <1–100> directions. by comparing it to the reverse leakage current (VAC = -600 V) before and after the dicing process. Using the FSPL dicing process, we successfully obtained a 100% yield at a narrow ∆x value of 13 µm, with no effect on the reverse characteristics. Fig. 5 shows typical reverse leakage characteristics of the SiC-SBDs before and after the dicing processes at ∆x = 13 µm. These results indicate that kerf loss can be neglected in the FSPL dicing, and therefore the cutting street width can be reduced. The residual lattice strain distribution after the dicing process was evaluated by micro-Raman measurement. Scattered light was dispersed with a 1 m double monochromator with 1800 gr/mm gratings, and the 514.5 nm line of an Ar+ laser was used for the excitation source. We measured the Materials Science Forum Vols. 821-823 variation of the peak frequency of the FTO mode when making line scans on the (0001) surface from the cutting edges, as illustrated in Fig. 6(a). ∆ω (=ωd-ωv) corresponds to the difference in the peak frequencies between the diced chips (ωd) and a virgin epilayer (ωv). As shown in Figs. 6(b)–(c), the shifts to low frequencies in the diced chips were observed around the edges, which indicates that tensile stress remains. The residual lattice strain in the FSPL-diced SiC chips was comparably small to that of the conventional mechanical process due to the absence of the lattice heating effect in the femtosecond-laser ablation process. 527 Fig. 7. SEM image of SiC chip diced from 100-µm-thick SiC bare wafer by the FSPL process. Recently, SiC wafer-thinning technologies have been utilized in some commercially available SiC devices to minimize substrate resistance [6]. Thus, we have also diced thin 4H-SiC wafers using the developed FSPL process. Fig. 7 shows a SEM image of a SiC chip diced from a three-inch, 100-µm-thick SiC wafer. The developed dicing technology can also be utilized with such thin SiC wafers. Summary We demonstrated the high-speed SiC dicing technology utilized FSPLs. Kerf loss can be neglected in the FSPL dicing, and therefore the wafer area will be utilized more effectively. The residual lattice strain in the FSPL-diced SiC chips was evaluated by microscopic Raman spectroscopy, and was comparably small to that of the conventional mechanical process due to the femtosecond laser ablation properties with no heat damage to the surrounding SiC. The effective laser scan speed on the SiC wafer surfaces was 33 mm/s, which is one order of magnitude higher than that of conventional mechanical dicing. In addition, unlike the mechanical dicing process, the optical dicing process has no trade-off limitation between throughput time and cutting quality. Therefore further increments of the laser scan speed for productivity improvement could be made possible by increasing the laser output power in the future. References [1] D. Lewke, M. Koitzsch, M. Schellenberger, L. Pfitzner, H. Ryssel, H. Zühlke, Proc. Mater. Res. Soc. Symp. Vol. 1433 (2012) p. 25. [2] S. 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