Construction and Building Materials 37 (2012) 738–745 Contents lists available at SciVerse ScienceDirect Construction and Building Materials journal homepage: www.elsevier.com/locate/conbuildmat Assessment of compressed earth blocks made in Spain: International durability tests Jaime Cid-Falceto a,⇑, Fernando R. Mazarrón b, Ignacio Cañas a a b Construction and Rural Roads Department, E.T.S.I. Agrónomos, Polytechnic University of Madrid, Avda. Complutense s/n, 28040 Madrid, Spain Rural Engineering Department, E.T.S.I. Agrónomos, Polytechnic University of Madrid, Avda. Complutense s/n, 28040 Madrid, Spain h i g h l i g h t s " We study the durability against rain of compressed earth blocks. " We analyze the usefulness of test procedures proposed in the international normative. " The lack of unified criteria in the tests produces differences in the results obtained. " Spanish CEB are fit for exterior and/or interior walls depending on stabilization. " This analysis could be a reference in the writing of future normative documents. a r t i c l e i n f o Article history: Received 20 December 2011 Received in revised form 25 July 2012 Accepted 11 August 2012 Available online 13 September 2012 Keywords: Compressed earth block Durability Erosion test Standards Construction material a b s t r a c t This research studies the durability against rain of the most industrialized construction material based on unbaked earth: compressed earth blocks (CEBs). The test procedures will be those ones proposed in the international normative (44 normative documents studied), analyzing the usefulness of these tests. The lack of unified criteria in the tests produces differences in the results obtained depending on the method used. Spanish stabilized CEB are fit for both interior faces and exterior walls, while non-stabilized CEB are just adequate to be used in exterior walls by applying a protection. This analysis could be a reference in the writing of future normative documents for all the world. Ó 2012 Elsevier Ltd. All rights reserved. 1. Introduction 1.1. Compressed earth blocks Constructions based on unbaked earth date back since more than 9000 years ago [1]. Compressed earth block (CEB) has become more common in the last few years as an earth construction system [2], proving to be an industrialized material, besides its traditional value as an element of self-construction. CEB includes all the variations of this product, whether or not the earth is stabilized [3]. Although throughout the literature different designations are used, all refer to the same products: compressed earth block [4], pressed brick [5–7], pressed block [8], compressed stabilized earth block – CSEB [9–12], soil cement solid bricks [13–24], soil–cement block [25], ground blocks cements ⇑ Corresponding author. Tel.: +34 913365767; fax: +34 913363688. E-mail addresses: jaime.cid@upm.es (J. Cid-Falceto), f.ruiz@upm.es (F.R. Mazarrón), ignacio.canas@upm.es (I. Cañas). 0950-0618/$ - see front matter Ó 2012 Elsevier Ltd. All rights reserved. http://dx.doi.org/10.1016/j.conbuildmat.2012.08.019 [26], compressed earth brick [8] or stabilized soil blocks [27]. The most common format is a rectangular parallelepiped (or prismatic) formal with a length ‘‘l’’, a width ‘‘w’’ and a height ‘‘h’’, obtained from static or dynamic compression of wet earth, followed by an immediate stripping, and that may contain stabilizers or additives to achieve or develop the particular features of the products [4,26]. In Fig. 1, it compiles the sizes of the CEB accepted in the official normative of the countries that have a standard of compressed earth block. However, in the Spanish standard UNE 41410 [4], NMAC 14.7.4 [28] or the American regulation published by ASTM International [8], sizes and tolerance of the blocks are not specified, allowing some liberty in the making of these earth materials. It can define the CEB as the product obtained by compression of wet earth, followed by a stripping, and that may contain stabilizers or additives to achieve certain properties and which dry compressive strength equals or is more than 2 MPa. Mechanic compression improves the physical properties of these blocks. Benefits of using earth in this manner include improved strength and durability as compared with adobe [29]. 739 J. Cid-Falceto et al. / Construction and Building Materials 37 (2012) 738–745 Fig. 1. Sizes of blocks (length, width, height) in international normative (CEB). Besides, the advantages of these CEB are that they do not need the high temperature curing as required by fired clay bricks [30] and the optimum compression level is reached by hydraulic presses. 1.2. Standards for compressed earth block The number of normative documents on compressed earth block (CEB) that were identified and used in this article are forty four. The totality of international norms in reference to the CEB are: The norm IS 1725 [25] from India, twelve norms NBR [13–24] from Brazil, fourteen norms ARS [31–44] from African Regions, two norms NT [45,46] from Tunisia, three norms NZS [5–7] from New Zealand, one norm KS 02-1070 [27] from Kenya, one norm XP P13-901 [47] from France, one norm NTC 5324 [26] from Colombia, one norm UNE 41410 [4] from Spain, one norm ASTM E2392M-10 [8] from the American Society for Testing and Materials, and lastly, one norm NMAC 147.4 [28] from New Mexico. In addition to these, three normative documents of great international prestige are EBAA 2001 [48], HB 195 [49] and Bulletin 5 [9]. In this normative about compressed earth blocks, the application field in 85% of the analyzed standards and regulations contemplates the stabilization of the blocks. In the rest of the documents it contemplates blocks with or without stabilizers always that mechanical specifications referred in the document are accomplished. This is the case of the first European normative [4], which limits the amount of stabilizers and additives to 15%. A compressed earth block is considered valid if the proposed mechanical specifications are complied, needing a minimum value of compression (dry and wet values). The amount of moisture of the block influences the values of compression [50], so that a dry value is obtained when the CEB is tested when the weight is constant after two consecutive loads; or a wet value if the test is performed on the block previously submerged in water. In most of the international standards, it considers CEB those blocks that have a compression value in dry that is equal to or more than 2 MPa; case of the Brazilian standards [13], Colombian standard [26], Indian standard [25] or the experimental French standard [47]. 1.3. Typologies of CEB: standards The typologies of compressed earth blocks, which are defined in the standards and regulations, are classified according to different properties: Table 1 Drip and spray erosion test, international normative. Technical documents Reference IS 1725 NZS SAZS 724 SLS 1382 UNE 41410 ASTM E2395M-10 EBAA 2001 HB 195 Bulletin 5 [25] [5–7] [65] [10–12] [4] [8] [48] [49] [9] Drip erosion Spray erosion Technical X X X X X X b a, c b b a, a, a, a, X X X X X X X X (a) Adobe; (b) compressed earth block; (c) rammed earth. Fig. 2. Minimum values of dry and wet compressive strength in all international standards (CEB). b, c b, b, b, b, c c c c 740 J. Cid-Falceto et al. / Construction and Building Materials 37 (2012) 738–745 Table 2 Specifications of spray erosion test, according to International standards. Technical documents Sample Tested face Number of samples Exposed area (area £ mm) Spray time (min) Observations (min) Application distance (mm) Pressure (kPa) Outlet nozzle (£ mm) Erosion rate (mm/min) Evaluation system Maximum impact velocity (m/s) Maximun rain rate (mm/h) Drop diameter (£ mm) IS 1725 NZS SLS 1382 ASTM E2395M10 EBAA 2001 HB 195 Bulletin 5 Whole block Table of block 3 – 120 – 180 147 100 No Yes 6.5 15–30 2–4 Whole block Table of block – 150 60 15 470 0–50 153 Yes Yes – – – Whole block Orientation as intended in wall construction 3 150 60 15 500 50 – – Yes – – – Whole block Table of block Whole block Table of block 5 70–150 60 15 470 0–50 – Yes No – – – Whole block Table of block 5 70–150 60 15 470 0–50 – Yes Yes – – – Whole block Table of block 1 150 60 15 470 0–50 – Yes Yes – – – – According to the total volume of holes, two kinds of blocks are defined: the solid block in which the total apparent volume (Vt) is more than 85%; and the hollow block, in which the Vt is less than 85% [26,16]. – According to the aspect or texture: ordinary blocks that will be coated; face blocks that are to be used without render [4,26]. – Mechanic specifications, complying with the African regulations [31–44], or from Tunisia [45,46], are classified in three categories: category 1, structural elements which are not load-bearing and structural elements capable of withstanding limited external loads; category 2, structural elements capable of withstanding important external loads; category 3, structural elements capable of withstanding high external loads. A summary of minimum values of dry and wet compressive strength needed by the CEB, are detailed in Fig. 2. – According to their capillarity specifications: weak capillarity (index of absorption by capillarity, Cb 6 20); little capillarity (Cb 6 40) [26,47]. – According to the environment where they are, it divides in three categories: dry, wet with aggression of the water by lateral sprinkling or wet with vertical penetration [31,45,46]. 2. Durability of earth blocks in normative documents Durability of the earth materials is one of the main aspects that must be considered when characterizing a material based on unbaked earth, since its affinity for water is one of the main drawbacks of this material [51]. There are many authors [52–56] that propose different laboratory tests for the study and analysis of water erosion on the unbaked earth materials, getting dispersed results due to the variability of their technical test specifications. 2.1. Standards of durability with erosion test After studying the normative international panorama [57], all regulations, standards or normative documents regarding the durability of the earth systems opposite to the erosion of water are analyzed. The tests currently used to check the effect of water on this kind of material are the spray erosion test and the drip erosion test. Table 1 shows normative documents in which any of these two kinds of existing erosion tests are mentioned. Indicating the constructive technique to which the proposed test is applied. These tests have been proposed in numerous documents and are the object of study of many authors [58–64]. Both are considered empirical. The ‘‘spray erosion test’’ is referred to by some authors as a direct replica of the erosion originated by rain water [58] – 150 60 15 470 0–50 153 Yes Yes – – – studying its application on real conditions. The ‘‘drip erosion test’’ is a good cheap test for testing bricks in areas of little rain [63]. 2.2. International normative to CEB: specifications to erosion test Spray erosion test is an empirical test developed by Commonwealth Scientific and Industrial Research Organization (CSIRO). The drip erosion test was developed by the University of Technology of Swinburne, Australia, which is currently known as Swinburne accelerated erosion test. The drip erosion test is used in the Spanish standard UNE 41410:2008 [4]. These tests are sometimes applicable to several construction techniques with earth as it is the case of the New Zealand standard [6] or to one technique only, as it is the case of Zimbabwe [65]. This study focuses on the test methods applied internationally to CEB. All the tests are based on the same ground of subjecting a test tube to a pressure spray for a certain amount of time or until specimen is penetrated (spray erosion), or else to a constant water fall for a certain amount of time (drip erosion), in order to evaluate afterwards the damage caused in both cases. In the spray erosion test the following parameters are defined: sample, tested face, number of samples to be tested, exposed area, spray time, observations, application distance (nozzle-specimen), pressure, etc., Table 2 contains the explanations of the ‘‘spray erosion test’’ procedures for the compressed earth blocks. For the cases of the drip erosion test the height of the water fall or the inclination of the sample to be tested are indicated. For the interpretation of the evaluation criteria regarding the validity or invalidity of the sample, the erodibility indexes are established (Table 3), case of the New Zealand standards [5–7]. Furthermore, the norm NZS 4299 [7], introduces a map with wind zones limiting the materials according to the erodibility index (Table 3), for which the criteria of acceptability of all materials is to have an erodibility index inferior to five or a depth of erosion inferior to 120 mm (D120mm). Other standards limit the erosion of the block, to less than 10 mm, like in the standards IS 1725 [25] or SLS 1382 [10]. Differently, in the Australian documents EBAA 2001 [48] and HB 195 [49], the test is proposed and described, but no criteria are offered for its evaluation. 3. Research objectives The objective of this research, in addition to that of analyzing the Spanish products, is to analyze the usefulness of the international tests as a reference in the writing of future standards. J. Cid-Falceto et al. / Construction and Building Materials 37 (2012) 738–745 741 Fig. 5. CEB type 1 after 30 min in spray erosion test, with two different areas. These tests help us to better know the applicability of the earth products and to propose a series of modifications to obtain more homogeneous results, allowing us to establish levels of quality and safety of the products, characterize the materials and facilitate comparative analysis between products. The present article studies sole three Spanish products in industrial format that have these features. 4. Materials Three kind of CEB are used that cover the present market in Spain, all of them solid blocks. These are identified as type 1 (non-stabilized block) and as type 2 and type 3 (stabilized blocks). The purpose of stabilizing earth-based materials is to improve their resistance to the detrimental effects of water, both blocks are stabilized with cement at the 6% (block type 2), and cement–quicklime at the 8% (block type 3). Fig. 3 shows the orientation of the compression of each one of the blocks made in Spain. The CEB were analyzed to determine its characteristics. A granulometric analysis was developed to determine proportion of different sized particles in the soil, expressing the quantity as the percentages which passed through the different sieves according to UNE 103101 [66] and Atterberg Limits and group index of the soil according to UNE 103103 [67] and UNE 103104 [68] (see Table 4). For the application of international test, it develops two prototypes that have great versatility in the system allowing the validation of all the technical specifications proposed in the analyzed normative documents. In the spray erosion test, pressures, distances of application and/or area of the exposed zone can be changed (Fig. 4). In the drip erosion test it can change the height of application and/or the quantity of water. 0.05 MPa of pressure and an area of application of 0.150 m of diameter. It will indicate whether it is suitable (D < 120 mm) or not according to the criteria established by the New Zealand standard and in the case where the analyzed CEB is suitable, which erodibility index it corresponds to. 5.1.1.2. Procedure B. This method, complying with standard SLS 1282 [10–12]. It keeps the same conditions than with procedure A. It modifies the distance of application to 0.500 m. According to the criteria of evaluation of this test procedure, the perforations performed after the application of the spray erosion test must not be more than 10 mm deep. 5.1.1.3. Procedure C. This method, complying with standard IS 1725 [25]. It increases the pressure of application up to 0.15 MPa and the distance of application is reduced to 0.180 m. According to the criteria of evaluation of this procedure, the CEB must not suffer a weight loss higher than 5%. 5.1.2. Drip erosion test The test procedure specified in diverse normative documents will be applied, UNE 41410 [4], HB 195 [49] y EBAA [48]. 5.1.2.1. Procedure D. This method, complying with standard UNE 41410 [4]. For 10 min a quantity of 500 ml of water is applied. It tests two samples of each type of CEB and it applies the criteria of evaluation of the standard, if the hole is equal or less than 10 mm, the CEB is apt, while if it is more than 10 mm, it will not pass the criteria of the test. The test method indicates that the height of the water fall must be 1 m, the time of test 10 min and the positioning of the sample 27° respect of the horizontal. 5.2. Tested faced in CEB to erosion tests 5. Experimental work: methods For this part of the present work, two different tests were programmed: the spray erosion test and the drip erosion test. Initially the testing procedures are applied (procedure A–D) and afterwards it is analyzed whether testing one side or another of the block influences the erosion tests. 5.1. Erosion test: procedures The different procedures used in this work are: procedure A (spray erosion test according to standards NZS), procedure B (spray erosion test according to standards SLS), procedure C (spray erosion test according to standard IS) and procedure D (drip erosion test according to standard IS). 5.1.1. Spray erosion test In the case of this test, it will develop the same test on each type of block, with three different procedures according to the analyzed international regulations. That is, it will test nine samples in each one of the procedures detailed below. 5.1.1.1. Procedure A. Complying with the standard NZS [5–7] and the Australian normative documents. Duration of the test, 60 min (interruption of the test every 15 min to observe and analyze the sample); a distance of application of 0.470 m; This section of the investigation consists in analyzing whether the tested face influences the results of the erosion. Both the spray erosion test and the drip erosion test will be applied over both sides and faces of each one of the three blocks. 5.2.1. Spray erosion test Three kinds of CEB will be tested on both sides and faces according to the three procedures indicated by international norms. For each one of these procedures (A– C) 12 blocks are tested. 5.2.2. Drip erosion test Three kinds of CEB are tested on both sides and faces according to the procedure indicated in the first non-experimental European norm UNE 41410. For the study of these three types of blocks, twelve blocks have to be tested according to the procedure D. 6. Results and discussion The first step consists of the analysis of the study of the tested face and, based on the results, the procedures of testing here described will be applied. 742 J. Cid-Falceto et al. / Construction and Building Materials 37 (2012) 738–745 Table 3 Erodibility indexes from spray erosion test, NZS 4298. Erodibility index Criteria (mm) Result 1 2 3 4 5 0 6 D < 20 20 6 D < 50 50 6 D < 90 90 6 D < 120 D P 120 Pass Pass Pass Pass Fail 6.1. Study of the tested faces Firstly, the results obtained when applying the ‘‘spray erosion test’’ to the three kinds of compressed earth blocks are analyzed (procedures A–C). When applying the three procedures of the test to the sides and faces of block 1, the first results were negative (fail), a rupture and a disgregation having been produced in every case. Block 1 does not meet any of the criteria of evaluation of the three procedures at hand. In the case of blocks 2 and 3 a positive evaluation is obtained (pass) when applying the three testing procedures. The application of the specifications of the three testing procedures (procedure A, B, and C), do not produce an erosion on the side or face of the three blocks that were analyzed. This means that the position of the block for this test does not influence the final result, according to the criterias of evaluation proposed by the procedures A–C. Secondly, a drip erosion test is applied (procedure D). All blocks (blocks 1–3) meet the requirements of procedure D. In spite of differences in erosion having been found in block 1 when tested on the side a (erosion 5 mm) or on side b (erosion 9 mm), while that on their faces the same erosion is obtained on both cases (face a and face b have a depth of erosion of 4 mm). Fig. 3. Orientation of the compression, in CEB made in Spain. Acknowledging this, it is recommended that the drip erosion test is used for CEB 1 (procedure D) for side a, side b, and for one of the two faces of each sample. The value of erosion of the block to be selected will be the highest figure of erosion provided by any of these. For the rest of the blocks it is recommended to test in all cases the ‘‘face a’’ of the corresponding block, since no differences between the sets of results have appeared. 6.2. Study of the testing procedures In each of the three kinds of CEB made in Spain, the four test procedures described in the previous section were performed, three of them are specifically of the spray erosion test and the procedure D is the drip erosion test specified in the CEB Spanish standard [4]. The results of the tests performed are shown in Table 5. 6.2.1. Spray erosion test When applying this test, all CEB stabilized, block type 2 and block type 3, are apt according to the technical specifications of the different methods. Instead, block type 1 (unstabilized block), does not pass the conformity criteria. Comparing the different test procedures, procedure C is a more aggressive method than the rest of test procedures (processes A Fig. 4. Spray erosion test, UPM model. Table 4 Results of the granulometric analysis, Attemberg limits and size of the CEB. CEB type 1 CEB type 2 CEB type 3 Percent passing (%) Atterberg limits UNE sieve designation Liquid limit (%) Plastic limit (%) Plastic index (%) a (mm) b (mm) c (mm) 20.3 20.2 28.3 14.1 18.5 19.2 6.2 1.7 9.1 306 295 290 166 140 145 103 90 95 10 6.3 5 2 0.5 0.32 0.08 98.6 100 100 98.3 99.6 100 98.3 99.4 100 93.9 86.9 92.4 75.3 48.2 57.1 59.1 31.2 45.5 14.4 11.4 18.8 Size Table 15 Pass 4 mm Pass – mm Pass – mm Faila Pass – mm Pass – mm Faila Pass – mm Pass – mm 743 and B). However, this difference does not affect the results according to their criteria of evaluation. Furthermore, as for what the area of application is concerned, many of the studied standards appoint the area in a circular surface of 0.150 m of diameter, but if it analyzes the size of the CEB currently made all over the world (Fig. 1), in a great number of them, the area of exposure is bigger than the faces of the tested CEB. This also happens with the CEB made in Spain. To solve this problem, it proposes to modify the area of application into a circular area of 125 mm of diameter, an area that covers the face of the CEB made in Spain (Fig. 5). Different results are obtained depending on the stabilization of the blocks: Edge b 14 Pass 9 mm Pass – mm Pass – mm 9 8 Edge a 13 Pass 5 mm Pass – mm Pass – mm – For the non-stabilized CEB (type 1), the erosion degree decreases considerably if a smaller exposed area is used (125 mm of diameter). And the penetration of water is less than when the area of application does not cover the table of the block, as seen on the edge of the tested CEB. If the surface affected by the applied stream of water being applied is adjusted to the tested face of the block, the erosion produced will be inferior (g < f), see Fig. 5. In the same way the shaded area shows the advance of humidity over the block, being inferior if the surface where it is applied is the same as the face being tested. – In stabilized CEB, decreasing the area exposed according to the geometry of the tested CEB does not affect the results obtained. 6.2.2. Drip erosion test All the analyzed CEB are apt for their use in construction, according to the trial procedures analyzed at the international level. In the non-stabilized CEB, the media depth of the erosion is 6 mm deep 10 min after it is tested. On the other hand, for the stabilized blocks the erosion depth is practically zero. The maximum erosion produced on the blocks that were not stabilized (block 1) is not produced due to the direct fall of the drop of water but rather by the runoff that takes place, resulting in a greater loss due to this effect. It is recommendable to use a criteria of evaluation relating the blocḱs loss of mass, around 5% of the maximum loss of weight, as has been proposed in other articles on the subject of international norms of erosion [25]. Table 12 Pass 4 mm Pass – mm Pass – mm Faila Pass – mm Pass – mm Faila Pass – mm Pass – mm Faila Pass – mm Pass – mm Faila Pass – mm Pass – mm 7 6 5 Proc. B (deep in mm) 4 Proc. C (deep in mm) J. Cid-Falceto et al. / Construction and Building Materials 37 (2012) 738–745 Edge b 11 Pass 9 mm Pass – mm Pass – mm Rupture of the block. Edge a 10 Pass 5 mm Pass – mm Pass – mm This article presents an analysis of the durability properties when exposed to water of the three kinds of CEB made in Spain to be used as construction material. It has been tested according to the test procedures of international standards for construction materials with earth, specifically for compressed earth blocks. Both tests (spray and drip erosion tests) have been applied to the products made in Spain, reaching the following conclusions, which can serve as a base for the normalization of the durability test: a Type test Samples Block 1 Block 2 Block 3 Faila Pass I.E 1 Pass I.E 1 Block 1 Block 2 Block 3 Drip test Faila Pass I.E 1 Pass I.E 1 Faila Pass I.E 1 Pass I.E 1 1 Samples Proc. D (deep in mm) 3 2 Spray test Proc. A (deep in mm) Type Test Table 5 Results of the spray and drip erosion tests in all CEB. 7. Conclusions – The criteria of evaluation in the spray erosion test are varied making it difficult to carry out the comparison between these two criteria. There is a need to unify the procedures in a single test. – Spray erosion test is a method applicable to the stabilized CEB (types 2 and 3), while for non-stabilized blocks (type 1) it is too aggressive. Those blocks that are not suitable must be rendered if they are to be used in exterior, or they must be used mainly for interior faces. – Performing the spray erosion test with procedures A, B and C do not show differences in the results for the CEB types 2 and 3 since the content of the stabilizer increases the CEB́s capacity of resistance to erosion. – In the case of the CEB analyzed in this study (CEB made in Spain), it has been proven that the erosion results (spray erosion test) do not vary depending on which face of the object 744 J. Cid-Falceto et al. / Construction and Building Materials 37 (2012) 738–745 is tested. However, if a testing method for a ‘‘spray erosion test’’ is developed for a new regulation, it is necessary to indicate which is the tested face. It is because of this that it is recommendable to initially test one or the other faces or sides of the object at random, and in the case of obtaining different results, the value of the erosion should come to be considered that of the most unfavorable result. – To decrease the area exposed in the spray erosion test affects only affects non-stabilized CEB, thus, it is advised to keep the following ratio: e<a where ‘‘a’’ is the width of the CEB and ‘‘e’’ the diameter of the circular area of application (Fig. 5). – After evaluating the three procedures (A–C) of the spray erosion test, the procedure B is considered the most recommendable due to its methodology and the system of evaluation it applies. – Drip erosion test is a valid method for not-stabilized CEB, whilst for stabilized Spanish blocks, not quantifiable differences are found in their results. – It is concluded that the criteria of evaluation of the ‘‘drip erosion test’’ should be modified. The criteria of evaluation must be related to the loss of weight of the CEB (loss of weight >5– 10%) and not to the depth of the erosion produced at that moment. Applying these durability tests to the CEB made in Spain, it confirms that all the stabilized CEB tested in this article are apt for constructions with earth, since they comply with the specifications of international standards. The use of non-stabilized CEB is valid for interior faces and exterior walls by rendering them or applying a similar protection. Acknowledgements This study has been carried out as part of the BIA2006-099170 research project ‘‘Development of earth-based material to rural construction: adobe, compressed earth blocks, rammed earth and poured earth as sustainable construction systems’’, funded by the Spanish Ministry of Science and Innovation. References [1] Minke G. Manual de construcción en tierra. 1994 ed. Montevideo-Uruguay: Editorial Nordan-comunidad; 2001. [2] Reddy BW, Lal R, Rao KSN. 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